Characterization of the Composition, Structure, and Mechanical Properties of Endocarp Biomass

2022 ◽  
Vol 65 (1) ◽  
pp. 67-74
Author(s):  
Makua C. Vin-Nnajiofor ◽  
Wenqi Li ◽  
Seth Debolt ◽  
Yang-Tse Cheng ◽  
Jian Shi

HighlightsEndocarps have higher lignin content, cellular and bulk density, and hardness than typical biomass feedstocks.The impacts of lignin content, bulk density, and mechanical properties on energy consumption are discussed.Endocarps can be a potential feedstock for a biorefinery coproducing biofuel and bioproducts.Abstract. Lignin is an abundant biopolymer and a promising source of feedstock for high-value chemicals and materials. This study aims to characterize the lignin-rich endocarp biomass and identify features of this unique feedstock that are relevant to feedstock preprocessing and logistics. The chemical composition and cellular structure of walnut and peach endocarps were characterized using HPLC and scanning electron microscopy (SEM) imaging. Mechanical properties of the endocarps were investigated using nanoindentation. Mechanical tests revealed hardness values of up to 0.48 and 0.40 GPa for walnut and peach endocarps, respectively. With screen sizes of 1 and 2 mm, the specific energy consumption was 9.21 and 1.86 MJ kg-1 for walnut and 12.6 and 2.72 MJ kg-1 for peach, respectively, as determined using a knife mill. Milling energy consumption was correlated to screen size, lignin content, bulk density, and mechanical properties. This study provides critical information on feedstock supply logistics necessary to implement a novel feedstock in biorefineries and evaluate the economic feasibility for coproduction of biofuels and lignin-derived products. Keywords: Biomass feedstock, Lignin, Mechanical properties, Nanoindentation, Size reduction.

2020 ◽  
Vol 986 ◽  
pp. 41-49
Author(s):  
Radka Pernicova ◽  
Tomas Kolomaznik

This document explains and demonstrates the influence of plasticizing additives on concrete – wet cured concrete with aggregate based on silicon carbide specifically. These special products have been designed for the foundry industry and have specific requirements for treatment in their early curing stage. The paper deals with the optimization of the currently used formula in order to increase their mechanical and surface properties by adding several different types of plasticizing additives and/or combinations thereof. Indicators of the measured characteristics have been mechanical tests, surface properties, and bulk density, which represented the SiC indicator of the mixture. With regard to the measured data, it can be stated that the effect of the plasticizing additive on special concrete with SiC aggregate have been considerable and depended very much on the type of additive used and its dosage, as the resulting mechanical properties differed by up to 40%.


2019 ◽  
Vol 14 (1) ◽  
pp. 110
Author(s):  
Assiss. Prof. Dr. Sabiha Mahdi Mahdi ◽  
Dr. Firas Abd K. Abd K.

Aim: The aimed study was to evaluate the influence of silver nitrate on surfacehardness and tensile strength of acrylic resins.Materials and methods: A total of 60 specimens were made from heat polymerizingresins. Two mechanical tests were utilized (surface hardness and tensile strength)and 4 experimental groups according to the concentration of silver nitrate used.The specimens without the use of silver nitrate were considered as control. Fortensile strength, all specimens were subjected to force till fracture. For surfacehardness, the specimens were tested via a durometer hardness tester. Allspecimens data were analyzed via ANOVA and Tukey tests.Results: The addition of silver nitrate to acrylic resins reduced significantly thetensile strength. Statistically, highly significant differences were found among allgroups (P≤0.001). Also, the difference between control and experimental groupswas highly significant (P≤0.001). For surface hardness, the silver nitrate improvedthe surface hardness of acrylics. Highly significant differences were statisticallyobserved between control and 900 ppm group (P≤0.001); and among all groups(P≤0.001)with exception that no significant differences between control and150ppm; and between 150ppm and 900ppm groups(P>0.05).Conclusion: The addition of silver nitrate to acrylics reduced significantly the tensilestrength and improved slightly the surface hardness.


1970 ◽  
Vol 26 (1) ◽  
pp. 16 ◽  
Author(s):  
S Balasubramanian ◽  
Rajkumar Rajkumar ◽  
K K Singh

Experiment to identify ambient grinding conditions and energy consumed was conducted for fenugreek. Fenugreek seeds at three moisture content (5.1%, 11.5% and 17.3%, d.b.) were ground using a micro pulverizer hammer mill with different grinding screen openings (0.5, 1.0 and 1.5 mm) and feed rate (8, 16 and 24 kg h-1) at 3000 rpm. Physical properties of fenugreek seeds were also determined. Specific energy consumptions were found to decrease from 204.67 to 23.09 kJ kg-1 for increasing levels of feed rate and grinder screen openings. On the other hand specific energy consumption increased with increasing moisture content. The highest specific energy consumption was recorded for 17.3% moisture content and 8 kg h-1 feed rate with 0.5 mm screen opening. Average particle size decreased from 1.06 to 0.39 mm with increase of moisture content and grinder screen opening. It has been observed that the average particle size was minimum at 0.5 mm screen opening and 8 kg h-1 feed rate at lower moisture content. Bond’s work index and Kick’s constant were found to increase from 8.97 to 950.92 kWh kg-1 and 0.932 to 78.851 kWh kg-1 with the increase of moisture content, feed rate and grinder screen opening, respectively. Size reduction ratio and grinding effectiveness of fenugreek seed were found to decrease from 4.11 to 1.61 and 0.0118 to 0.0018 with the increase of moisture content, feed rate and grinder screen opening, respectively. The loose and compact bulk densities varied from 219.2 to 719.4 kg m-3 and 137.3 to 736.2 kg m-3, respectively.  


Author(s):  
Georgel MIHU ◽  
Claudia Veronica UNGUREANU ◽  
Vasile BRIA ◽  
Marina BUNEA ◽  
Rodica CHIHAI PEȚU ◽  
...  

Epoxy resins have been presenting a lot of scientific and technical interests and organic modified epoxy resins have recently receiving a great deal of attention. For obtaining the composite materials with good mechanical proprieties, a large variety of organic modification agents were used. For this study gluten and gelatin had been used as modifying agents thinking that their dispersion inside the polymer could increase the polymer biocompatibility. Equal amounts of the proteins were milled together and the obtained compound was used to form 1 to 5% weight ratios organic agents modified epoxy materials. To highlight the effect of these proteins in epoxy matrix mechanical tests as three-point bending and compression were performed.


2021 ◽  
Vol 13 (10) ◽  
pp. 5617
Author(s):  
Raman Kumar ◽  
Sehijpal Singh ◽  
Ardamanbir Singh Sidhu ◽  
Catalin I. Pruncu

This paper’s persistence is to make an inclusive analysis of 268 documents about specific energy consumption (SEC) in machining operations from 2001 to 2020 in the Scopus database. A systematic approach collects information on SEC documents’ primary data; their types, publications, citations, and predictions are presented. The VOSviewer 1.1.16 and Biblioshiny 2.0 software are used for visualization analysis to show the progress standing of SEC publications. The selection criteria of documents are set for citation analysis. The ranks are assigned to the most prolific and dominant authors, sources, articles, countries, and organizations based on the total citations, number of documents, average total citation, and total link strength. The author-keywords, index-keywords, and text data content analysis has been conducted to find the hotspots and progress trend in SEC in machining operations. The most prolific and dominant article, source, author, organization, and country are Anderson et al. “Laser-assisted machining of Inconel 718 with an economic analysis”, the Int J Mach Tools Manuf, Shin Y.C., form Purdue University Singapore, and United States, respectively, based on total citations as per defined criteria. The author keywords “specific cutting energy” and “surface roughness” dominate the machining operations SEC. SEC’s implication in machining operations review and bibliometric analysis is to deliver an inclusive perception for the scholars working in this field. It is the primary paper that utilizes bibliometric research to analyze the SEC in machining operations publications expansively. It is valuable for scholars to grasp the hotspots in this field in time and help the researchers in the SEC exploration arena rapidly comprehend the expansion status and trend.


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