Creep of Mechanically-Alloyed NiAl Containing 13 Vol % Mo or Mo2C Dispersoids

1998 ◽  
Vol 552 ◽  
Author(s):  
A. Lakki ◽  
D. C. Dunand
Keyword(s):  
Mechanical Alloying ◽  
Nickel Aluminide ◽  
Metallic Phase ◽  
Creep Mechanism ◽  
Diffusional Creep ◽  
Mechanically Alloyed ◽  
Ceramic Phase ◽  
Creep Properties ◽  
Reactive Mechanical Alloying

ABSTRACTDispersion-strengthened nickel aluminide NiAl was synthesized by reactive mechanical alloying from elemental powders. The microstructure and creep properties of these materials was compared for two cases: (i) NiAl-Mo, where dispersoids are in the form of a ductile, metallic phase and (ii) NiAl- Mo2C, where the dispersoids are a brittle, ceramic phase. Also, the effect of annealing treatments which coarsened both matrix grains and dispersoids was investigated. Inhibited diffusional creep is identified as the rate-controlling creep mechanism.

Microstructure of mechanically alloyed and hot-pressed Al5CuZr2

1990 ◽  
Vol 48 (4) ◽  
pp. 970-971
Author(s):  
T. E. Mitchell ◽  
P. B. Desch ◽  
R. B. Schwarz
Keyword(s):  
Mechanical Alloying ◽  
Vickers Hardness ◽  
Hot Pressing ◽  
Rapid Quenching ◽  
Hardened Steel ◽  
Alloyed Powder ◽  
Ion Milling ◽  
Mechanical Grinding ◽  
Mechanically Alloyed ◽  
Steel Container

Al3Zr has the highest melting temperature (1580°C) among the tri-aluminide intermetal1ics. When prepared by casting, Al3Zr forms in the tetragonal DO23 structure but by rapid quenching or by mechanical alloying (MA) it can also be prepared in the metastable cubic L12 structure. The L12 structure can be stabilized to at least 1300°C by the addition of copper and other elements. We report a TEM study of the microstructure of bulk Al5CuZr2 prepared by hot pressing mechanically alloyed powder.MA was performed in a Spex 800 mixer using a hardened steel container and balls and adding hexane as a surfactant. Between 1.4 and 2.4 wt.% of the hexane decomposed during MA and was incorporated into the alloy. The mechanically alloyed powders were degassed in vacuum at 900°C. They were compacted in a ram press at 900°C into fully dense samples having Vickers hardness of 1025. TEM specimens were prepared by mechanical grinding followed by ion milling at 120 K. TEM was performed on a Philips CM30 at 300kV.

New Fe-Ni Based Metal-Metalloid Glassy Alloys Prepared by Mechanical Alloying and Rapid Solidification

1996 ◽  
Vol 455 ◽  
Author(s):  
J. J. Suñol ◽  
M. T. Clavaguera-Mora ◽  
N. Clavaguera ◽  
T. Pradell
Keyword(s):  
Mechanical Alloying ◽  
Rapid Solidification ◽  
Melt Spinning ◽  
Magnetic Interaction ◽  
Processing Route ◽  
Mechanically Alloyed ◽  
Scanning Calorimetry ◽  
Glassy Alloys ◽  
Rapidly Solidified ◽  
Thermal Stability Of

ABSTRACTMechanical alloying and rapid solidification are two important routes to obtain glassy alloys. New Fe-Ni based metal-metalloid (P-Si) alloys prepared by these two different processing routes were studied by differential scanning calorimetry and transmission Mössbauer spectroscopy. Mechanical alloyed samples were prepared with elemental precursors, and different nominal compositions. Rapidly solidified alloys were obtained by melt-spinning. The structural analyses show that, independent of the composition, the materials obtained by mechanical alloying are not completely disordered whereas fully amorphous alloys were obtained by rapid solidification. Consequently, the thermal stability of mechanically alloyed samples is lower than that of the analogous material prepared by rapid solidification. The P/Si ratio controls the magnetic interaction of the glassy ribbons obtained by rapid solidification. The experimental results are discussed in terms of the degree of amorphization and crystallization versus processing route and P/Si ratio content.

scholarly journals Effect of Milling Parameters on the Development of a Nanostructured FCC–TiNb15Mn Alloy via High-Energy Ball Milling

Metals ◽  
2021 ◽  
Vol 11 (8) ◽  
pp. 1225
Author(s):  
Cristina García-Garrido ◽  
Ranier Sepúlveda Sepúlveda Ferrer ◽  
Christopher Salvo ◽  
Lucía García-Domínguez ◽  
Luis Pérez-Pozo ◽  
...  
Keyword(s):  
Mechanical Alloying ◽  
Ball Mill ◽  
Milling Time ◽  
High Energy ◽  
Planetary Mill ◽  
Nominal Composition ◽  
Mechanically Alloyed ◽  
Milling Parameters ◽  
Energy Ball ◽  
Full Conversion

In this work, a blend of Ti, Nb, and Mn powders, with a nominal composition of 15 wt.% of Mn, and balanced Ti and Nb wt.%, was selected to be mechanically alloyed by the following two alternative high-energy milling devices: a vibratory 8000D mixer/mill® and a PM400 Retsch® planetary ball mill. Two ball-to-powder ratio (BPR) conditions (10:1 and 20:1) were applied, to study the evolution of the synthesized phases under each of the two mechanical alloying conditions. The main findings observed include the following: (1) the sequence conversion evolved from raw elements to a transitory bcc-TiNbMn alloy, and subsequently to an fcc-TiNb15Mn alloy, independent of the milling conditions; (2) the total full conversion to the fcc-TiNb15Mn alloy was only reached by the planetary mill at a minimum of 12 h of milling time, for either of the BPR employed; (3) the planetary mill produced a non-negligible Fe contamination from the milling media, when the highest BPR and milling time were applied; and (4) the final fcc-TiNb15Mn alloy synthesized presents a nanocrystalline nature and a partial degree of amorphization.

Synthesis of Nanocrystalline Cubic Hafnium Nitride by Reactive Mechanical Alloying

2010 ◽  
Vol 27 (8) ◽  
pp. 086106 ◽  
Author(s):  
Ding Zhan-Hui ◽  
Qiu Li-Xia ◽  
Yao Bin ◽  
Zhao Xu-Dong ◽  
Lu Feng-Guo ◽  
...  
Keyword(s):  
Mechanical Alloying ◽  
Hafnium Nitride ◽  
Reactive Mechanical Alloying

scholarly journals Formation and Properties of the Ta-Y2O3, Ta-ZrO2, and Ta-TaC Nanocomposites

2018 ◽  
Vol 2018 ◽  
pp. 1-12
Author(s):  
J. Jakubowicz ◽  
M. Sopata ◽  
G. Adamek ◽  
P. Siwak ◽  
T. Kachlicki
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Mechanical Alloying ◽  
Young’S Modulus ◽  
Young's Modulus ◽  
Ceramic Composites ◽  
Ceramic Phase ◽  
Plasma Sintering ◽  
Average Grain Size ◽  
Bulk Nanocrystalline

The nanocrystalline tantalum-ceramic composites were made using mechanical alloying followed by pulse plasma sintering (PPS). The tantalum acts as a matrix, to which the ceramic reinforced phase in the concentration of 5, 10, 20, and 40 wt.% was introduced. Oxides (Y2O3 and ZrO2) and carbides (TaC) were used as the ceramic phase. The mechanical alloying results in the formation of nanocrystalline grains. The subsequent hot pressing in the mode of PPS results in the consolidation of powders and formation of bulk nanocomposites. All the bulk composites have the average grain size from 40 nm to 100 nm, whereas, for comparison, the bulk nanocrystalline pure tantalum has the average grain size of approximately 170 nm. The ceramic phase refines the grain size in the Ta nanocomposites. The mechanical properties were studied using the nanoindentation tests. The nanocomposites exhibit uniform load-displacement curves indicating good integrity and homogeneity of the samples. Out of the investigated components, the Ta-10 wt.% TaC one has the highest hardness and a very high Young’s modulus (1398 HV and 336 GPa, resp.). For the Ta-oxide composites, Ta-20 wt.% Y2O3 has the highest mechanical properties (1165 HV hardness and 231 GPa Young’s modulus).

Development of Mechanically Alloyed and Sintered W-1 wt.% Ni Matrix Composites Reinforced with TiB2

2012 ◽  
Vol 194 ◽  
pp. 194-198 ◽  
Author(s):  
Duygu Ağaoğulları ◽  
Özge Balci ◽  
Ö. Utku Demirkan ◽  
Hasan Gökçe ◽  
Aziz Genç ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Mechanical Alloying ◽  
Relative Density ◽  
Physical And Mechanical Properties ◽  
Matrix Composites ◽  
Combined Method ◽  
Mechanically Alloyed ◽  
Activated Sintering ◽  
Sintering Aid ◽  
Reinforcing Agent

Due to improve the physical and mechanical properties of Ni activated W compacts, TiB2 was added to the W-Ni matrix as reinforcing agent. W-Ni matrix composites were fabricated by using a combined method of mechanical alloying (MA), cold pressing and activated sintering. The amount of activated sintering aid (Ni) was kept constant as 1 wt.%. The effects of TiB2 content and mechanical alloying duration on the physical, microstructural and mechanical properties of activated sintered W-Ni compacts were investigated. The results showed that TiB2 particles have a significant effect on the density and microhardness values of the sintered samples. After MA and sintering, formation of W2B and NiTi intermetallic compounds were observed because of the decomposition of TiB2. The relative density value of 91.21 % and microhardness value of 4.08±0.28 GPa of W-1 wt.% Ni samples respectively increased to 94.88 % and 5.64±0.28 GPa with the addition of 2 wt.% TiB2.

scholarly journals Three-Dimensional Finite Element Modeling of Thermomechanical Problems in Functionally Graded Hydroxyapatite/Titanium Plate

2014 ◽  
Vol 2014 ◽  
pp. 1-20 ◽  
Author(s):  
S. N. S. Jamaludin ◽  
S. Basri ◽  
Ahmad Hussain ◽  
Dheya Shujaa Al-Othmany ◽  
F. Mustapha ◽  
...  
Keyword(s):  
Thermal Stresses ◽  
Three Dimensional ◽  
Metallic Phase ◽  
Functionally Graded ◽  
Thermomechanical Model ◽  
Graded Materials ◽  
Ceramic Phase ◽  
Fg Plates ◽  
Dimensional Finite Element ◽  
Three Dimensional Finite Element

The composition of hydroxyapatite (HA) as the ceramic phase and titanium (Ti) as the metallic phase in HA/Ti functionally graded materials (FGMs) shows an excellent combination of high biocompatibility and high mechanical properties in a structure. Because the gradation of these properties is one of the factors that affects the response of the functionally graded (FG) plates, this paper is presented to show the domination of the grading parameter on the displacement and stress distribution of the plates. A three-dimensional (3D) thermomechanical model of a 20-node brick quadratic element is used in the simulation of the thermoelastic behaviors of HA/Ti FG plates subjected to constant and functional thermal, mechanical, and thermomechanical loadings. The convergence properties of the present results are examined thoroughly in order to assess the accuracy of the theory applied and to compare them with the established research results. Instead of the grading parameter, this study reveals that the loading field distribution can be another factor that reflects the thermoelastic properties of the HA/Ti FG plates. The FG structure is found to be able to withstand the thermal stresses while preserving the high toughness properties and thus shows its ability to operate at high temperature.

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