scholarly journals Influence of cavo superficial enamel acid-etching on the microtensile bond strength of low-shrinkage composite resin

2020 ◽  
Vol 49 ◽  
Author(s):  
Raquel Devisate BORGHI ◽  
Erick Kamiya COPPINI ◽  
Josué Junior Araújo PIEROTE ◽  
João Victor Frazão CÂMARA ◽  
Luis Alexandre Maffei Sartini PAULILLO
Keyword(s):  
Bond Strength ◽  
Testing Machine ◽  
Adhesive System ◽  
Composite Resins ◽  
Acid Etching ◽  
Microtensile Bond Strength ◽  
Posterior Teeth ◽  
Cutting Machine ◽  
Universal Testing ◽  
Significant Difference

Abstract Introduction To prevent the shrinkage stresses produced during polymerization, composite resins of low polymerization shrinkage were developed. Objective To evaluate the microtensile bond strength in class I cavities restored by acid-etching the cavosurface angle and with composite resins indicated for posterior teeth. Material and method 48 healthy molars were selected and divided into six groups (n = 8), considering that the cavosurface enamel of three groups was etched with 35% phosphoric acid. The teeth were restored with the Clearfil SE Bond adhesive system and Filtek Z350 XT, Empress Direct, and Charisma Diamond composite resins, which were light-cured for 40 seconds. After 24 hours, the teeth were taken to a cutting machine, which produced sections in the buccolingual and mesiodistal directions. This resulted in toothpicks of 0.9×0.9 mm that were taken to the universal testing machine for the microtensile bond strength test. Statistical analysis was performed with ANOVA and Tukey’s test (p < 0.05). Result There was no statistically significant difference between the groups evaluated. Conclusion Acid-etching the cavosurface angle did not affect the performance of restorations, probably due to the adhesive system used.

The effect of caries detector dyes and a cavity cleansing agent on composite resin bonding to enamel and dentin

2001 ◽  
Vol 25 (1) ◽  
pp. 57-63 ◽  
Author(s):  
Azza El-Housseiny ◽  
Hana Jamjoum
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Composite Resin ◽  
Testing Machine ◽  
Group Iv ◽  
Acid Etching ◽  
Group V ◽  
Universal Testing ◽  
Group I ◽  
Significant Difference

This study was undertaken to evaluate the effect of caries detector dyes and/or cavity cleanser on composite bonding and etching patterns of enamel and dentin. One hundred and eight non-carious premolars were divided into six groups according to the enamel and dentin pretreatment investigated. The different pretreatment were as follows: Group I: teeth with prophylaxis only, Group II: Sable seek caries detector dye,Groups III: chlorhexidine cavity cleanser,Group IV: the caries detectors dye followed by prophylaxis, Group V: the cavity cleanser followed by the caries detector dye, and Group IV: Snoop caries detector dye. The shear bond strength of composite resin bonded to enamel and dentin was evaluated by the Instron Universal testing machine while, the topographic details of enamel and dentin were examined by the SEM following the different pretreatment and acid etching. Results of the shear bond strength showed no statistically significant difference among the six groups, with no substantial differences in SEM results. It is concluded that using the caries detector dyes and/or chlorhexidine cavity cleanser before acid etching does not significantly affect composite bonding to enamel and dentin.

scholarly journals Polymerization Shrinkage of Bulk Fill Composites and its Correlation with Bond Strength

2018 ◽  
Vol 29 (3) ◽  
pp. 261-267 ◽  
Author(s):  
Lauber Jose dos Santos Almeida Junior ◽  
Estevam Carlos de Oliveira Lula ◽  
Karla Janilee de Souza Penha ◽  
Vinicius Souza Correia ◽  
Fernando Augusto Cintra Magalhães ◽  
...  
Keyword(s):  
Bond Strength ◽  
Testing Machine ◽  
Class I ◽  
Third Molars ◽  
Microtensile Bond Strength ◽  
Polymerization Shrinkage ◽  
Universal Testing ◽  
Significant Difference ◽  
Light Curing ◽  
Factor C

Abstract The present study aimed to evaluates polymerization shrinkage (PS) using microcomputed tomography (μCT) and microtensile bond strength (μTBS) in bulk fill composites (BFC) and conventional class I restorations as well as the correlation between these factors. Class I cavities (4 x 5 x 4 mm), factor-C = 4.2, were created in third molars that were free of caries, which were randomly divided in 4 groups (n = 6): XTI (Filtek Supreme XTE: incremental technique); XTB (Filtek Supreme XTE: single fill technique); TBF (Tetric Bulk Fill); and SF (SonicFill). Each tooth was scanned twice in μCT: T0 was after filling the cavity with composite, and T1 was after light curing. The data were analyzed by subtracting the composite volume for each time (T1 - T0). After 1 week, the teeth were sectioned crosswise in the buccolingual and mesiodistal directions to obtain specimens with approximately 1 mm² thickness and fixed in a universal testing machine to perform μTBS. The Kruskal-Wallis and Dunn tests showed a statistically significant difference for shrinkage in µCT among the XTI and XTB and between the SF and XTB. Regarding the μTBS, all the groups differed from XTB. Bulk fill composites type presents a PS similar to that of the conventional nanoparticulate composite inserted using the incremental technique, but the bond strength was higher for the incremental group, which presented a lower number of pre-test failures when compared to BFC. No correlation was observed between the polymerization shrinkage and bond strength in the studied composites.

scholarly journals Effect of Different Bonding Strategies on Adhesion to Deep and Superficial Permanent Dentin

2010 ◽  
Vol 04 (02) ◽  
pp. 110-117 ◽  
Author(s):  
Rafael Eduardo Fernandes Pegado ◽  
Flávia Lucisano Botelho do Amaral ◽  
Flávia Martão Flório ◽  
Roberta Tarkany Basting
Keyword(s):  
Bond Strength ◽  
Composite Resin ◽  
Testing Machine ◽  
Adhesive System ◽  
Single Bond ◽  
Adhesive Systems ◽  
Microtensile Bond Strength ◽  
Universal Testing ◽  
One Step ◽  
The One

Objectives: To evaluate the effect of different bonding strategies on the microtensile bond strength to deep and superficial permanent dentin.Methods: Forty-eight teeth were randomly flattened according to the dentin depth: superficial dentin (SD) and deep dentin (DD). Subsequently, three adhesive systems were applied (n=8): an etchand- rinse (Adper Single Bond 2 - SB), a “mild” two-step self-etching (Clearfil SE Bond - SE) and a one-step self-etching adhesive system (Futurabond – FB). Each specimen was restored with a composite resin and sectioned into 1.0-mm2 thick slabs. After 24 hours, resin-dentin sticks were submitted to tensile stress in a universal testing machine (0.5 mm/min). Data were submitted to two-way ANOVA and Tukey’s test at a level of 0.05%.Results: Superficial dentin showed the highest microtensile bond strength values, which differed statistically from those obtained in the deep dentin, irrespective of the adhesive system used. FB yielded the highest bond strength values, which were statistically similar to the bond strength values of SE, but statistically different from those obtained when the SB adhesive was used.Conclusions: Bond strength obtained in superficial dentin was significantly higher than in deep dentin, for all adhesive systems tested. Adhesion was affected by the different bonding strategies: the one-step, low pH, acetone-based self-etching adhesive promoted the higher bond strength values, which were statistically similar to those obtained with the two-step, water-based self-etching adhesive. (Eur J Dent 2010;4:110-117)

scholarly journals Effects of Fluorosis and Self Etching Primers on Shear Bond Strengths of Orthodontic Brackets

2009 ◽  
Vol 03 (03) ◽  
pp. 173-177 ◽  
Author(s):  
Ahmet Yalcin Gungor ◽  
Hakan Turkkahraman ◽  
Necdet Adanir ◽  
Huseyin Alkis
Keyword(s):  
Bond Strength ◽  
Testing Machine ◽  
Orthodontic Brackets ◽  
Universal Testing ◽  
Adhesive Remnant Index ◽  
Halogen Light ◽  
Significant Difference ◽  
Bond Strengths ◽  
Group Ii ◽  
Clinical Changes

ABSTRACTObjectives: To evaluate the effects fluorosis and self etching primers (SEP) on shear bond strengths (SBS) of orthodontic brackets.Methods: A total of 48 (24 fluorosed and 24 non-fluorosed) non-carious freshly extracted human permanent premolar teeth were used in this study. Fluorosed teeth were selected according to the modified Thylstrup and Fejerskov index (TFI), which is based on the clinical changes in fluorosed teeth. Fluorosed and non-fluorosed teeth were randomly assigned to 4 groups of 12 each. In groups I (non-fluorosed teeth) and II (fluorosed teeth), standard etching protocol was used and brackets were bonded with Light Bond. In groups III (non-fluorosed teeth) and IV (fluorosed teeth), Transbond Plus SEP was used and brackets were bonded with Transbond XT Light Cure Adhesive. All specimens were cured with a halogen light. After bonding, SBS of the brackets were tested with Universal testing machine. After debonding, all teeth and brackets in the test groups were examined under 10x magnifications. Any adhesive remained after debonding was assessed and scored according to the modified Adhesive Remnant Index (ARI).Results: ANOVA indicated a significant difference between groups (P<.001). SBS in group II (Light Bond+Fluorosis) were significantly lower than other groups. ARI scores of the groups were also significantly different (P<.001). There was a greater frequency of ARI scores of 1,2 and 3 in group II (Light Bond+Fluorosis).Conclusions: When standard etching protocol was used enamel fluorosis significantly decreased the bond strength of orthodontic brackets. Satisfactory bond strengths were obtained when SEP was used for bonding brackets to the fluorosed teeth. (Eur J Dent 2009;3:173-177)

scholarly journals Microtensile Bond Strength of Methacrylate and Silorane Resins to Enamel and Dentin

2014 ◽  
Vol 25 (4) ◽  
pp. 327-331 ◽  
Author(s):  
Gisele Rodrigues da Silva ◽  
Isabela Sousa Araújo ◽  
Rodrigo Dantas Pereira ◽  
Bruno de Castro Ferreira Barreto ◽  
Célio Jesus do Prado ◽  
...  
Keyword(s):  
Bond Strength ◽  
Aging Time ◽  
Storage Time ◽  
Composite Resin ◽  
Glass Plate ◽  
Composite Resins ◽  
Microtensile Bond Strength ◽  
Bonding Interaction ◽  
Significant Difference ◽  
And Storage

The aim of this study was to evaluate the microtensile bond strength (µTBS) of two substrates (enamel and dentin) considering two study factors: type of composite resin [methacrylate-based (Filtek Supreme) or silorane-based (Filtek LS)] and aging time (24 h or 3 months). Twenty human molars were selected and divided into 2 groups (n=10) considering two dental substrates, enamel or dentin. The enamel and dentin of each tooth was divided into two halves separated by a glass plate. Each tooth was restored using both tested composite resins following the manufacturer's instructions. The samples were sectioned, producing 4 sticks for each composite resin. Half of them were tested after 24 h and half after 3 months. µTBS testing was carried out at 0.05 mm/s. Data were analyzed by three-way ANOVA and Tukey's HSD tests at α=0.05. Significant differences between composite resins and substrates were found (p<0.05), but no statistically significant difference was found for aging time and interactions among study factors. The methacrylate-based resin showed higher µTBS than the silorane-based resin. The µTBS for enamel was significantly higher than for dentin, irrespective of the composite resin and storage time. Three months of storage was not sufficient time to cause degradation of the bonding interaction of either of the composite resins to enamel and dentin.

scholarly journals Bond strength to dentin of total-etch and self-etch adhesive systems

2014 ◽  
Vol 62 (4) ◽  
pp. 365-370 ◽  
Author(s):  
Ricardo Alves dos SANTOS ◽  
Eliane Alves de LIMA ◽  
Mônica Maria de Albuquerque PONTES ◽  
Alexandre Batista Lopes do NASCIMENTO ◽  
Marcos Antônio Japiassú Resende MONTES ◽  
...  
Keyword(s):  
Bond Strength ◽  
Testing Machine ◽  
Adhesive System ◽  
Single Bond ◽  
Adhesive Systems ◽  
Healthy Human ◽  
Universal Testing ◽  
Stereo Microscope ◽  
Diamond Disc ◽  
Self Etch

OBJECTIVE: To assess the bond strength to dentin of the Single Bond (3M ESPE) and XP Bond (Dentsply) total-etch and Adper SE Plus (3M ESPE) self-etch adhesive systems. METHODS: Fifteen healthy human third molars were randomly allocated across three different groups of five teeth each according to the adhesive system. The occlusal portion of each tooth was removed under refrigeration using a flexible diamond disc (EXTEC, Enfield, CT, USA) down to an area of dentin that did not reveal enamel, as confirmed under a 40X stereo microscope (Ramsor, São Paulo, Brazil). A standardized smear layer was created with #600 grit silicon-carbide paper. The adhesive systems were applied as per manufacturer recommendations, with the exception of the Adper SE Plus system, which was triple-polymerized. Composite resin blocks (5 mm) were placed on the dentin surface. The specimens were stored in distilled water for 24 hours at 37ºC. Using a flexible diamond disc (EXTEC, Enfield, CT, USA), toothpick-like specimens with an adhesive area of less than 1 mm² were obtained. A microtensile bond test was then carried out using a universal testing machine (KRATOS) with a crosshead speed of 0.5 mm/min. Analysis of variance (ANOVA) and Tukey's test were used for comparisons. RESULTS: The bond strength values obtained with each adhesive system were as follows: XP Bond, 96.24 MPa; Adper Single Bond, 72.39 MPa; Adper SE Plus, 49.91 MPa. CONCLUSION: In terms of bond strength to dentin, conventional adhesives outperform self-etching systems.

scholarly journals Shear bond strength of bulk-fill and nano-restorative materials to dentin

2016 ◽  
Vol 10 (01) ◽  
pp. 040-045 ◽  
Author(s):  
Hakan Colak ◽  
Ertugrul Ercan ◽  
Mehmet Mustafa Hamidi
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Clinical Success ◽  
Testing Machine ◽  
Group Iv ◽  
Composite Resins ◽  
Group Iii ◽  
Bonding System ◽  
Group I ◽  
Significant Difference

ABSTRACT Objectives: Bulk-fill composite materials are being developed for preparation depths of up to 4 mm in an effort to simplify and improve the placement of direct composite posterior restorations. The aim of our study was to compare shear-bond strength of bulk-fill and conventional posterior composite resins. Materials and Methods: In this study, 60 caries free extracted human molars were used and sectioned parallel to occlusal surface to expose midcoronal dentin. The specimens were randomly divided into four groups. Total-etch dentine bonding system (Adper Scotchbond 1XT, 3M ESPE) was applied to dentin surface in all the groups to reduce variability in results. Then, dentine surfaces covered by following materials. Group I: SonicFill Bulk-Fill, Group II: Tetric EvoCeram (TBF), Group III: Herculite XRV Ultra, and Group IV: TBF Bulk-Fill, 2 mm × 3 mm cylindrical restorations were prepared by using application apparatus. Shear bond testing was measured by using a universal testing machine. Kruskal–Wallis and Mann–Whitney U-tests were performed to evaluate the data. Results: The highest value was observed in Group III (14.42 ± 4.34) and the lowest value was observed in Group IV (11.16 ± 2.76) and there is a statistically significant difference between these groups (P = 0.046). However, there is no statistically significant difference between the values of other groups. In this study, Group III was showed higher strength values. Conclusion: There is a need for future studies about long-term bond strength and clinical success of these adhesive and bulk-fill systems.

scholarly journals Influence of Air Abrasion and Sonic Technique on Microtensile Bond Strength of One-Step Self-Etch Adhesive on Human Dentin

2015 ◽  
Vol 2015 ◽  
pp. 1-6 ◽  
Author(s):  
Baraba Anja ◽  
Dukić Walter ◽  
Chieffi Nicoletta ◽  
Ferrari Marco ◽  
Sonja Pezelj Ribarić ◽  
...  
Keyword(s):  
Bond Strength ◽  
Testing Machine ◽  
Control Group ◽  
Air Abrasion ◽  
Microtensile Bond Strength ◽  
Dentin Surface ◽  
Significant Difference ◽  
Human Dentin ◽  
One Step ◽  
Self Etch

The purpose of thisin vitrostudy was to evaluate the microtensile bond strength of one-step self-etch adhesive to human dentin surface modified with air abrasion and sonic technique and to assess the morphological characteristics of the pretreated dentin surface. The occlusal enamel was removed to obtain a flat dentin surface for thirty-six human molar teeth. The teeth were randomly divided into three experimental groups (n= 12 per group), according to the pretreatment of the dentin: (1) control group, (2) air abrasion group, and (3) sonic preparation group. Microtensile bond strength test was performed on a universal testing machine. Two specimens from each experimental group were subjected to SEM examination. There was no statistically significant difference in bond strength between the three experimental groups (P> 0.05). Mean microtensile bond strength (MPa) values were 35.3 ± 12.8 for control group, 35.8 ± 13.5 for air abrasion group, and 37.7 ± 12.0 for sonic preparation group. The use of air abrasion and sonic preparation with one-step self-etch adhesive does not appear to enhance or impair microtensile bond strength in dentin.

scholarly journals Effect of beverages on surface properties of resin-based sealants

2017 ◽  
Vol 16 ◽  
pp. 1-7
Author(s):  
Bruna Genari ◽  
Vicente Castelo Branco Leitune ◽  
João Henrique Macedo Saucedo ◽  
Susana Maria Werner Samuel ◽  
Fabrício Mezzomo Collares
Keyword(s):  
Bond Strength ◽  
Testing Machine ◽  
Resin Cement ◽  
Control Group ◽  
Resin Cements ◽  
Universal Testing ◽  
Halogen Light ◽  
Significant Difference ◽  
Tooth Surfaces ◽  
Light Curing

Self-adhesive, dual-polymerizing resin cements require no treatment to the prepared tooth surfaces before cementation. Aim: The aim of this study was to evaluate the influence of curing mode on bond strength (BS) of three cementing systems to bovine dentin. Methods: The buccal enamel surfaces of 50 bovine incisors were removed to expose dentin and to flat the surface. The teeth were divided into five groups (n=10), which consisted of two resin cements (Multilink and Clearfil SA Cement) that were tested in dual- (halogen light for 40 s) and self-cured modes, and a control (RelyX ARC). Two cylinders of resin cements (1.0 mm X 0.75 mm) were prepared on each bonded dentin surface. After 24h at 37oC, resin cylinders were subjected to micro-shear testing in a universal testing machine (4411/Instron - 0.5 mm/min). Data were statistically analyzed by two-way ANOVA, Tukey and Dunnett`s test (5%). Results: Multilink showed higher BS than those observed on Clearfil SA. Light-curing resulted in higher BS for both Multilink and Clearfil SA. When Multilink was light-cured, no significant difference on BS was demonstrated between it and RelyX ARC. Conclusions: The highest BS values were obtained in control group and light-cured Multilink resin cement.

scholarly journals Perbedaan Kekuatan Geser Reparasi Gigi Tiruan Cekat dengan Resin Komposit Packable dan Flowable (Uji Laboratoris pada permukaan logam NiCr)

2012 ◽  
Vol 19 (2) ◽  
pp. 102
Author(s):  
Endang Wahyuningtyas ◽  
Suparyono Saleh ◽  
Sri Budi Barunawati
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Composite Resin ◽  
Testing Machine ◽  
Composite Resins ◽  
Distilled Water ◽  
Research Subjects ◽  
Flowable Composite ◽  
Diamond Bur ◽  
Universal Testing

Latar Belakang. Resin komposit merupakan bahan pilihan untuk reparasi Gigi Tiruan Cekat porcelain fused to metal (PFM) Karena estetis baik dan manipulasi mudah. Tujuan penelitian ini adalah mengetahui perbedaan kekuatan geser perlekatan resin komposit pada permukaan logam Gigi Tiruan Cekat dengan menggunakan resin komposit jenis packable dan jenis flowable. Metode penelitian. Subjek penelitian berupa logam NiCr (Noritake, Japan) berbentuk silinder dengan diameter 10 mm dan tinggi 3 mm. Penelitian dibagi menjadi dua kelompok, masing-masing terdiri dari 10 subjek. Kelompok pertama reparasi dengan resin komposit packable (Z250™ 3M ESPE, USA) dan kelompok kedua reparasi dengan resin komposit flowable (Dyad flow, Kerr, USA). Permukaan subjek dikasari dengan wheel diamond bur, dietsa dengan asam fosfat 37 % (Scotchbond™, 3M ESPE, USA) kemudian dicuci dan dikeringkan, selanjutnya diaplikasikan silan (Rely X™ Ceramic Primer, 3M ESPE, USA) dan bonding (Adper™ Single Bond, 3M ESPE, USA). Permukaan kemudian dilapisi dengan resin komposit packable dan flowable, disinari selama 40 detik. Subjek penelitian direndam di dalam distilled water dan dimasukkan ke dalam incubator dengan suhu 37°C selama 7 hari. Uji kekuatan geser dilakukan dengan menggunakan Universal Testing Machine. Data dianalisis dengan uji t. hasil uji t menunjukkan terdapat perbedaan bermakna kekuatan geser reparasi gigi tiruan cekat pada permukaan logam (p<0,05). Kesimpulan penelitian ini adalah kekuatan geser reparasi pada permukaan logam dengan menggunakan resin komposit flowable yang mengandung bahan coupling agent lebih tinggi dibandingkan reparasi pada permukaan porselen dengan menggunakan resin komposit packable. Background. One of selected material by repairing the fixed partial denture was composite resin because of its good aesthetics and low manipulation. The aim. This research was aimed at identifying the differences of shear bond strength of composite resin on metal surface by using different composite resins, namely packable and flowable composite resins. Method. The research subjects were cylinders with 10 mm in diameter and 3 mm in height. The research subjects with metal material of NiCr (Noritke, Japan) involved two groups. The first group comprising 10 repair subjects with composite packable (Z250™, 3M ESPE, USA) and 10 repair subjects with flowable composite (Dyad flow, Kerr, USA). The surface of the subjects were roughned with wheel diamond bur and etched with 37% phosphate acid (Scotbond™, 3M ESPE, USA) were applied. The surface was then coated with packable and flowable composite resins and light-cured for 40 seconds. The research subjects were immersed in distilled water and put into the incubator at temperature of 37°C for 7 days. The shear bond strength test was conducted using the Universal Testing Machine. Data were analyzed using t-test. The result. The research result showed that there were differences of shear bond strength of repair between packable and flowable composite resins. The result of t-test indicated significant diffrences on metal surface (p<0,05). The conclusion of this research is that shear bond strength of repair with flowable composite which contain coupling agent has higher shear bond strength than that of packable composite resin.

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