scholarly journals Pengaruh Konsentrasi Ekstrak Metanol Babadotan (Ageratum conyzoides L.) terhadap Pertumbuhan Beberapa Jenis Gulma

2020 ◽  
Vol 3 (4) ◽  
pp. 85-95
Author(s):  
Ilham Iwan Tona ◽  
Gina Erida ◽  
Hasanuddin Hasanuddin

Abstrak.  Gulma merupakan tumbuhan yang tidak dikehendaki keberadaannya atau tumbuhan yang tumbuh liar pada lahan budidaya yang dapat menimbulkan kerugian sehingga perlu dikendalikan. Penelitian ini bertujuan Untuk mengetahui konsentrasi yang efektif dari ekstrak methanol babadotan dalam menghambat pertumbuhan gulma bayam duri, teki dan rumput kembang goyang. Penelitian dilaksanakan di Laboratorium Ilmu Gulma Jurusan Agroteknologi, Laboratorium Analisis Pangan Jurusan Teknologi Hasil Pertanian Fakultas Pertanian, Laboratorium Kimia Organik Fakultas Keguruan Ilmu Pendidikan, Laboratorium Analisis Kimia Fakultas Matematikan dan Ilmu Pengetahuan Alam serta Kebun Percobaan Fakultas Pertanian Universitas Syiah Kuala, Darussalam Banda Aceh sejak Juli - November 2017. Rancangan yang digunakan dalam penelitian ini adalah Rancangan Acak Lengkap (RAL) pola Non Faktorial,  yaitu dengan menggunakan 3 jenis gulma  A : bayam duri , B : teki, C : rumput kembang goyang dan ekstrak daun babadotan pada masing-masing gulma yaitu 0%, 10%, 20%, 30%, 40%, serta terdapat kontrol (herbisida 2,4D). Setiap perlakuan diulang sebanyak  3 kali dengan 3 tanaman indikator sehingga terdapat 54  satuan percobaan dan setiap satuan percobaan terdiri dari 4 unit gulma, sehingga terdapat 216 unit percobaan.  Hasil Penelitian menunjukkan ekstrak metanol babadotan dengan konsentrasi 10 dan 20% mampu mengendalikan gulma bayam duri pada 7 HSA sebesar 93,75%  dan pada 14 HSA sebesar 100%. Sedangkan pada rumput kembang goyang konsentrasi 20% pada 7 HSA mampu mengendalikan gulma sebesar 82,50% dan pada 14 HSA sebesar 93,33%.  Ekstrak metanol babadotan berdasarkan uji fitokimia ditemukan senyawa steroid dan saponin, sedangkan hasil analisis Kromatografi Gas dan Spektometri Massa ditemukan 6 senyawa mayor terdiri dari senyawa 2H-1-Benzopyran, 7-(1,1-dimethylethyl)-2,3-dihydro-3,3-dimethyl, 3,7,11,15-Tetramethyl-2-hexadecen-1-ol, 9-Eicosyne, 9-Eicosyne dan Methyl Ester. The Effect of Whiteweed Methanol Extract ( Ageratum conyzoides L.) to Growth of some WeedsAbstract.  Weeds are plants that are not desired for their existence or plants that grow wild on cultivated land that can cause harm so that need to be controlled. This study aims to determine the effective concentration of whiteweed methanol extract in inhibiting the growth of spiny amaranth, nutgrass and rocking grass. This research was conducted in Weed Science Laboratory and Experimental Garden Department of Agrotechnology, Food Analysis Laboratory Department of Food technology Faculty of Agriculture, Chemical Organic Department of Education Faculty, Chemical Analysis Mathematics and Natural Science faculty,  University of Syiah Kuala, Darussalam Banda Aceh, from July to November 2017. This research using Randomized Completely Design with Non Factorial pattern, using 3 types of weeds, A : whiteweed, B : nutgrass, C : rocking grass and whiteweed leaves solvent for each weeds is 0%, 10%, 20%, and 40%,and has control (herbicide 2,4D). Each tretment has 3 replication with 3 indicator plants so that has 54 experimental units., each experimental unit consists of 4 weed units, so there are 216 experimental units.The results showed that whiteweed methanol extract with a concentration of 10 and 20% was able to control spinach weed in 7 HSA at 93.75% and at 14 HSA at 100%. Whereas on the rocking grass, the concentration of 20% in 7 HSA was able to control weeds by 82.50% and at 14 HSA by 93.33%. Whiteweed methanol extract based on phytochemical test found steroid and saponin compounds, while the results of Gas Chromatography and Mass Spectrometry analysis found 6 major compounds consisting of compounds: 2H-1-Benzopyran, 7-(1,1-dimethylethyl)-2,3-dihydro-3,3-dimethyl, 3,7,11,15-Tetramethyl-2-hexadecen-1-ol, 9-Eicosyne, 9-Eicosyne and Methyl Ester.  

2018 ◽  
Vol 55 (No. 1) ◽  
pp. 23-30
Author(s):  
Aoki Yoshinao ◽  
Trung Nguyen Van ◽  
Suzuki Shunji

Methanol extract of Piper betle leaves exhibited an inhibitory effect on grape downy mildew. This extract might contain more than two compounds which have different polarities that suppress grape downy mildew. Gas chromatograph-tandem mass spectrometry analysis identified 4-allylpyrocatechol, eugenol, α-pinene, and β-pinene in the methanol extract. Neither of the compounds suppressed grape downy mildew by single treatment. On the other hand, treatment with a combination of 4-allylpyrocatechol with eugenol, α-pinene or β-pinene enhanced the inhibitory effects on grape downy mildew and perfectly suppressed it. The complex extracted from P. betle leaves may be used in organic agriculture as an alternative to chemical fungicides in viticulture.


2011 ◽  
Vol 6 (9) ◽  
pp. 1934578X1100600 ◽  
Author(s):  
Barbara Szajwaj ◽  
Jaroslaw Moldoch ◽  
Milena Masullo ◽  
Sonia Piacente ◽  
Wieslaw Oleszek ◽  
...  

Two new derivatives of phenylpropenoic acids, N-trans-feruloyl-L-DOPA and O-trans-caffeoylmalic acid dimethyl ester, along with four known N-trans-caffeoyl-L-DOPA (clovamide), N-trans-caffeoyl-L-DOPA-methyl ester, O-trans-caffeoylmalic acid, O-trans-feruloyl-malic acid and quercetin 3- O-β-D-glucopyranoside were isolated from the aerial parts of Trifolium pallidum. Their structures were elucidated by extensive spectroscopic methods including 1D- (1H, 13C) and 2D-NMR (DQF-COSY, HSQC, HMBC) experiments as well as mass spectrometry analysis.


Author(s):  
PRIYADHARISINI J

Objective: Garcinia cambogia fruit commonly known as Malabar tamarind, belongs to the family Clusiaceae, is said to show varied medicinal effects including antiobesity, antiviral, antimicrobial, anti-inflammatory, and anticancer. Hence, the present study deals with the determination of phytochemical constituents present in the chloroform extract of G. cambogia fruits and determination of bioactive compounds using the gas chromatography and mass spectrometry analysis (GC-MS) technique. Methods: The phytochemical constituents present in the chloroform extract of G. cambogia fruits were tested by qualitative analysis, and bioactive compounds were investigated using the GC-MS technique. The analysis was carried out on a JOEL GC MATERI system with a column packed with a column HP5MS (5% phenyl, methylpolysiloxane) fused capillary column (30 × 0.25 μm ID × 0.25 μm df). The compounds are separated using helium as a carrier gas at a constant flow 1 ml/min. The mass spectra of the known compounds in the fruit extract were matched with the known components stored in the National Institute of Standard and technology library. Results: The phytochemical test revealed the presence of xanthones, flavonoids, phlobatannins, terpenoids steroids, phenolic compounds saponins, and anthraquinones. The GC-MS analysis provided peaks of 13 different bioactive compounds, namely 3,7,11,15-tetramethyl-2-hexadecenol (37.1%), pentadecanoic acid 14-methyl-, methylester (100%), hexadecanoic acid 15 methyl-, methyl ester (100%), 9,12-octadecadienoic acid methyl ester (42.6%), docosanoic acid (100%), docosanoic acid methyl ester (37.3%), phenol, 2,4,bis1,1-dimethylethyl) (100%), 9, hexadecanoic acid methyl ester (99.2%), 10-octadecenoic acid methylester (100%), 11 eicosenoic acid methyl ester (53.1%), heptadecanoic acid 9 methyl-, methyl ester (100%), eicosenoic acid methyl ester (56.9%), and 5, 12d ethanofuro oxepino[2,3,4-mn] (2,3,4-ed) anthrace2-one 9,12-dilol 6 methyl,2a 3,4,4a,5,6,7,8a‑octahydro (19%) were reported. Conclusion: The phytochemical investigation and determination of bioactive compounds will be considered for pharmacological activities, and further isolation of individual components would however help to find new drugs.


Author(s):  
C. Prabhu ◽  
V. Rajasekar ◽  
T. Prakash

In the present work, a detailed investigation of the physio-chemical characteristics of grapeseed methyl ester (GSME) obtained from winery biomass waste has been carried out to evaluate its suitability as an energy alternate, for CI engines. GSME was subjected to Gas chromatography and mass spectrometry analysis from which fatty acids compositions were determined followed by other interpretations such as carbon number, number of double bonds, etc. Two different predictive correlations were identified from the literature for predicting the properties that are considered important, for using GSME as a fuel. The predicted properties of GSME are compared with the experimental results obtained through standard ASTM procedures, for diesel, neat grapeseed oil (GSO) and GSME, respectively. Further, the influence of the structural and compositional characteristics of GSME on the physicochemical properties like density, kinematic viscosity, lower calorific value, etc. has been evaluated and found to be closer to diesel.


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