Do We Need Higher Dose Scale Inhibitors to Inhibit Scale under Turbulent Conditions? Insight into Mechanisms and New Test Methodology

2014 ◽  
Author(s):  
Tao Chen ◽  
Ping Chen ◽  
Harry Montgomerie ◽  
Thomas Hagen ◽  
Ronald Benvie ◽  
...  
Keyword(s):  
Reynolds Number ◽  
Turbulent Flow ◽  
Growth Inhibitor ◽  
Test Method ◽  
Bulk Precipitation ◽  
Scale Inhibitor ◽  
Surface Deposition ◽  
Test Methodology ◽  
The Relationship ◽  
Scale Deposition

Abstract Turbulent flow, especially around chokes, downhole safety valves and inflow control devices, favors scale deposition potentially leading to severe loss of production. Recently, scale formation under turbulent conditions has been studied and progressed, focused on the bulk precipitation (SPE164070) and a small bore valve loop test (SPE 155428). However, bulk precipitation is not fully representative the surface deposition in the fields and the Reynolds number of modified loop is unknown. The relationship between a measured Reynolds number and surface deposition up until this study has not been addressed. A newly developed test methodology with rotating cylinder has been applied to generate high shear rate and evaluate surface deposition with Reynolds numbers up to ~41000. The relationship between Reynolds number and surface deposition is addressed. Using this highly representable test method for BaSO4 scale deposition, several different generic types of inhibitor chemistries, including polymers and phosphonates, were assessed under different levels of turbulence to evaluate their performance on surface deposition. The results showed it is not always true that higher turbulence results in higher dose of inhibitor being required to control scale. It is inhibitor chemistry and mechanisms dependent. The scale inhibitorscan be classified as three types when evaluating the trend of mass deposition versus Reynolds number and the morphology of the crystals deposited on the metal surface. ➢ Type 1: Crytal growth inhibitors. The mass of surface deposition increases with the increase of turbulence, along with smaller crystals.➢ Type 2: Dispersion and crystal growth inhibitor. The higher the turbulence, the less mass deposition, along with smaller crystals.➢ Type 3: Dispersion scale inhibitors. The higher the turbulence, the less mass deposition. The size of the crystals has no major change. This paper gives a comprehensive study of the effect of flow condition on the scale surface deposition and inhibition mechanisms. In addition, it details how this methodology and new environmentally acceptable inhibitor chemistry can be coupled to develop a chemical technology toolbox that also includes techniques for advanced scale inhibitor analysis and improved scale inhibitor retention, to design optimum scale squeeze packages for the harsh scaling conditions associated with turbulent flow conditions.

The Impact of Pre-flush Additives on Scale Squeeze Treatments - Application of Modelling and New Test Methodologies to Understand Mechanisms of Retention and Optimise Field Treatment Designs

2014 ◽  
Author(s):  
O.. Vazquez ◽  
T.. Chen ◽  
L.. Crombie ◽  
P.. Chen ◽  
S.. Heath ◽  
...  
Keyword(s):  
Computer Modelling ◽  
Scale Inhibitor ◽  
Retention Mechanisms ◽  
Test Methodology ◽  
Production Stages ◽  
Modelling Techniques ◽  
Treatment Designs ◽  
The Impact ◽  
Scale Deposition ◽  
Modelling Data

Abstract One of the most common methods to prevent scale deposition in the near wellbore area is through the application of squeeze treatments which conventionally consist of pre-flush, main treatment, overflush, shut-in and back production stages. The use of additives such as polyamino acids and polyquaternary amines has often been successfully applied as part of the pre-flush stage of squeeze treatments to improve treatment lifetimes (Chen et al., 2006, Vazquez et al., 2011, Heat et al., 2012). However, although this technology has been successful applied in the field, there is still a lack of understanding of the prevalent retention mechanisms with different scale inhibitors and also a suitable test methodology and modelling techniques to optimize field treatment designs and lifetimes. A new sand pack methodology which provides a better simulation of field squeeze treatments than traditional corefloods has been designed to provide a better understanding of the scale inhibitor retention mechanisms when polyquaternary amines are applied in pre-flush treatments. This has enabled improved treatment modelling and the impact of these additives to be understood in field treatments. The performance of the polyquaternary amine is dependent upon scale inhibitor chemistry and the mechanisms of retention are addressed for both polymeric and phosphonate scale inhibitors. The adsorption isotherms were derived and compared in the absence/presence of the polyquaternary amine using specialized software, and applied to predict squeeze lifetime in field scenarios. This paper provides an understanding on the effects of polyquaternary amines on squeeze lifetime for both phosphonate and polymeric scale inhibitors supported by the application of a newly developed test methodology and computer modelling techniques. In addition, the combination of laboratory and computer modelling data coupled with field experience and a better understanding of the retention mechanisms involved now provides the ability to improve and optimize field squeeze treatment designs with polyquaternary amine pre-flush additives.

An evaluation of ECT sample height for small flute board grades and Box Manufacturer’s Certification compliance

TAPPI Journal ◽  
2009 ◽  
Vol 8 (6) ◽  
pp. 24-28
Author(s):  
CORY JAY WILSON ◽  
BENJAMIN FRANK
Keyword(s):  
Compressive Strength ◽  
Compressive Load ◽  
Test Sample ◽  
Test Methods ◽  
Test Method ◽  
Initial Development ◽  
Sample Height ◽  
Relationship Of ◽  
The Relationship ◽  
Corrugated Fiberboard

TAPPI test T811 is the specified method to ascertain ECT relative to box manufacturer’s certification compliance of corrugated fiberboard under Rule 41/ Alternate Item 222. T811 test sample heights were derived from typical board constructions at the time of the test method’s initial development. New, smaller flute sizes have since been developed, and the use of lighter weight boards has become more common. The T811 test method includes sample specifications for typical A-flute, B-flute, and C-flute singlewall (and doublewall and triplewall) structures, but not for newer thinner E-flute or F-flute structures. This research explores the relationship of ECT sample height to measured compressive load, in an effort to determine valid E-flute and F-flute ECT sample heights for use with the T811 method. Through this process, it identifies challenges present in our use of current ECT test methods as a measure of intrinsic compressive strength for smaller flute structures. The data does not support the use of TAPPI T 811 for ECT measurement for E and F flute structures, and demonstrates inconsistencies with current height specifi-cations for some lightweight B flute.

Tire Treadwear — A Comprehensive Evaluation of the Factors: Generic Type, Aspect Ratio, Tread Pattern, and Tread Composition Part I: Introduction and Details on the Organization of the Program

1986 ◽  
Vol 14 (4) ◽  
pp. 201-218 ◽  
Author(s):  
A. G. Veith
Keyword(s):  
Aspect Ratio ◽  
Comprehensive Evaluation ◽  
Test Method ◽  
Interactive Effects ◽  
Data Analyses ◽  
Main Effect ◽  
Systematic Determination ◽  
Relationship Of ◽  
The Relationship

Abstract This four-part series of papers addresses the problem of systematic determination of the influence of several tire factors on tire treadwear. Both the main effect of each factor and some of their interactive effects are included. The program was also structured to evaluate the influence of some external-to-tire conditions on the relationship of tire factors to treadwear. Part I describes the experimental design used to evaluate the effects on treadwear of generic tire type, aspect ratio, tread pattern (groove or void level), type of pattern (straight rib or block), and tread compound. Construction procedures and precautions used to obtain a valid and functional test method are included. Two guiding principles to be used in the data analyses of Parts II and III are discussed. These are the fractional groove and void concept, to characterize tread pattern geometry, and a demonstration of the equivalence of wear rate for identical compounds on whole tread or multi-section tread tires.

Evaluation of the Resistance of Individual Si Die to Cracking

1998 ◽  
Author(s):  
R. Berriche ◽  
R.K. Lowry ◽  
M.I. Rosenfield
Keyword(s):  
Thermal Cycling ◽  
Hardness Test ◽  
Mechanical Stresses ◽  
Test Method ◽  
Processing Conditions ◽  
Micro Hardness ◽  
Test Methodology ◽  
Vickers Micro Hardness

Abstract The present work investigated the use of the Vickers micro-hardness test method to determine the resistance of individual die to cracking. The results are used as an indicator of resistance to failure under the thermal and mechanical stresses of packaging and subsequent thermal cycling. Indentation measurements on die back surfaces are used to determine how changes in wafer backside processing conditions affect cracks that form around impressions produced at different loads. Test methodology and results obtained at different processing conditions are discussed.

Numerical and Experimental Analysis of Turbulent Flow in Corrugated Pipes

2010 ◽  
Vol 132 (7) ◽  
Author(s):  
Henrique Stel ◽  
Rigoberto E. M. Morales ◽  
Admilson T. Franco ◽  
Silvio L. M. Junqueira ◽  
Raul H. Erthal ◽  
...  
Keyword(s):  
Reynolds Number ◽  
Pressure Drop ◽  
Turbulent Flow ◽  
Friction Factor ◽  
Turbulence Models ◽  
Reynolds Numbers ◽  
Velocity Magnitude ◽  
Geometric Configurations ◽  
Corrugated Surfaces ◽  
Friction Factors

This article describes a numerical and experimental investigation of turbulent flow in pipes with periodic “d-type” corrugations. Four geometric configurations of d-type corrugated surfaces with different groove heights and lengths are evaluated, and calculations for Reynolds numbers ranging from 5000 to 100,000 are performed. The numerical analysis is carried out using computational fluid dynamics, and two turbulence models are considered: the two-equation, low-Reynolds-number Chen–Kim k-ε turbulence model, for which several flow properties such as friction factor, Reynolds stress, and turbulence kinetic energy are computed, and the algebraic LVEL model, used only to compute the friction factors and a velocity magnitude profile for comparison. An experimental loop is designed to perform pressure-drop measurements of turbulent water flow in corrugated pipes for the different geometric configurations. Pressure-drop values are correlated with the friction factor to validate the numerical results. These show that, in general, the magnitudes of all the flow quantities analyzed increase near the corrugated wall and that this increase tends to be more significant for higher Reynolds numbers as well as for larger grooves. According to previous studies, these results may be related to enhanced momentum transfer between the groove and core flow as the Reynolds number and groove length increase. Numerical friction factors for both the Chen–Kim k-ε and LVEL turbulence models show good agreement with the experimental measurements.

Determination of Steady-State Adhesive Wear Rate

2005 ◽  
Author(s):  
L. J. Yang
Keyword(s):  
Steady State ◽  
Wear Rate ◽  
Wear Test ◽  
Standard Test ◽  
Test Method ◽  
Testing Time ◽  
Wear Coefficient ◽  
Wear Rates ◽  
Test Methodology

Wear rates obtained from different investigators could vary significantly due to lack of a standard test method. A test methodology is therefore proposed in this paper to enable the steady-state wear rate to be determined more accurately, consistently, and efficiently. The wear test will be divided into four stages: (i) to conduct the transient wear test; (ii) to predict the steady-state wear coefficient with the required sliding distance based on the transient wear data by using Yang’s second wear coefficient equation; (iii) to conduct confirmation runs to obtain the measured steady-state wear coefficient value; and (iv) to convert the steady-state wear coefficient value into a steady-state wear rate. The proposed methodology is supported by wear data obtained previously on aluminium based matrix composite materials. It is capable of giving more accurate steady-state wear coefficient and wear rate values, as well as saving a lot of testing time and labour, by reducing the number of trial runs required to achieve the steady-state wear condition.

The Relationship Between Frictional Resistance and Roughness for Surfaces Smoothed by Sanding

2002 ◽  
Vol 124 (2) ◽  
pp. 492-499 ◽  
Author(s):  
Michael P. Schultz
Keyword(s):  
Reynolds Number ◽  
Frictional Resistance ◽  
Resistance Coefficient ◽  
Polished Surface ◽  
Average Height ◽  
Freestream Velocity ◽  
Number Range ◽  
Test Fixture ◽  
Plate Length ◽  
The Relationship

An experimental investigation has been carried out to document and relate the frictional resistance and roughness texture of painted surfaces smoothed by sanding. Hydrodynamic tests were carried out in a towing tank using a flat plate test fixture towed at a Reynolds number ReL range of 2.8×106−5.5×106 based on the plate length and freestream velocity. Results indicate an increase in frictional resistance coefficient CF of up to 7.3% for an unsanded, as-sprayed paint surface compared to a sanded, polished surface. Significant increases in CF were also noted on surfaces sanded with sandpaper as fine as 600-grit as compared to the polished surface. The results show that, for the present surfaces, the centerline average height Ra is sufficient to explain a large majority of the variance in the roughness function ΔU+ in this Reynolds number range.

Turbulent flow between concentric rotating cylinders at large Reynolds number

1992 ◽  
Vol 68 (10) ◽  
pp. 1515-1518 ◽  
Author(s):  
Daniel P. Lathrop ◽  
Jay Fineberg ◽  
Harry L. Swinney
Keyword(s):  
Reynolds Number ◽  
Turbulent Flow ◽  
Large Reynolds Number ◽  
Rotating Cylinders
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