Adhesive Cementation Promotes Higher Fatigue Resistance to Zirconia Crowns

2017 ◽  
Vol 42 (2) ◽  
pp. 215-224 ◽  
Author(s):  
F Campos ◽  
LF Valandro ◽  
SA Feitosa ◽  
CJ Kleverlaan ◽  
AJ Feilzer ◽  
...  
Keyword(s):  
Fatigue Resistance ◽  
Mean Value ◽  
Resin Cement ◽  
Surface Pretreatment ◽  
Inner Surface ◽  
Computer Aided ◽  
Mode Of Failure ◽  
Zirconia Crowns ◽  
Adhesive Cementation ◽  
Number Of Cycles

SUMMARY Objective: The aim of this study was to investigate the influence of the cementation strategy on the fatigue resistance of zirconia crowns. The null hypothesis was that the cementation strategy would not affect the fatigue resistance of the crowns. Methods and Materials: Seventy-five simplified molar tooth crown preparations were machined in glass fiber–filled epoxy resin. Zirconia crowns were designed (thickness=0.7 mm), milled by computer-aided design/computer-aided manufacturing, and sintered, as recommended. Crowns were cemented onto the resin preparations using five cementation strategies (n=15): ZP, luting with zinc phosphate cement; PN, luting with Panavia F resin cement; AL, air particle abrasion with alumina particles (125 μm) as the crown inner surface pretreatment + Panavia F; CJ, tribochemical silica coating as crown inner surface pretreatment + Panavia F; and GL, application of a thin layer of porcelain glaze followed by etching with hydrofluoric acid and silanization as crown inner surface pretreatment + Panavia F. Resin cement was activated for 30 seconds for each surface. Specimens were tested until fracture in a stepwise stress fatigue test (10,000 cycles in each step, 600 to 1400 N, frequency of 1.4 Hz). The mode of failure was analyzed by stereomicroscopy and scanning electron microscopy. Data were analyzed by Kaplan-Meier and Mantel-Cox (log rank) tests and a pairwise comparison (p<0.05) and by Weibull analysis. Results: The CJ group had the highest load mean value for failure (1200 N), followed by the PN (1026 N), AL (1026 N), and GL (1013 N) groups, while the ZP group had the lowest mean value (706 N). Adhesively cemented groups (CJ, AL, PN, and GL) needed a higher number of cycles for failure than the group ZP did. The groups' Weibull moduli (CJ=5.9; AL=4.4; GL=3.9; PN=3.7; ZP=2.1) were different, considering the number of cycles for failure data. The predominant mode of failure was a fracture that initiated in the cement/zirconia layer. Finite element analysis showed the different stress distribution for the two models. Conclusion: Adhesive cementation of zirconia crowns improves fatigue resistance.

Fatigue Failure Load of a Bonded Simplified Monolithic Feldspathic Ceramic: Influence of Hydrofluoric Acid Etching and Thermocycling

2020 ◽  
Vol 45 (1) ◽  
pp. E21-E31 ◽  
Author(s):  
LF Guilardi ◽  
GKR Pereira ◽  
AS Vallau ◽  
IA Silva ◽  
JC Giordani ◽  
...  
Keyword(s):  
Fatigue Failure ◽  
Fatigue Resistance ◽  
Hydrofluoric Acid ◽  
Failure Load ◽  
Statistical Tests ◽  
Resin Cement ◽  
Ceramic Surface ◽  
Adhesive Cementation ◽  
Ceramic Restorations ◽  
O 10

SUMMARY Objective: To evaluate the effect of hydrofluoric acid (HF) etching and thermocycling (Tc) on fatigue failure load of feldspathic ceramic restorations cemented with two resin cements. Methods: Disc-shaped feldspathic ceramic (Vitablocs Mark II; Ø=10 mm, 1.0-mm thick) and G10 epoxy resin (Ø=10 mm, 2.5-mm thick) specimens were made and randomly allocated considering three factors: ceramic etching (ie, with vs without 10% HF plus silane application), resin cement (ie, self-adhesive [RelyX U200; U200] or conventional [Multilink Automix; MA]), and Tc (ie, with vs without 5-55°C/12,000 cycles). Adhesive cementation followed each manufacturer's instructions. The fatigue test (n=20) was based on the staircase approach (250,000 cycles; 20 Hz). Contact angle, surface topography, and fractography analysis were also executed. Specific statistical tests were employed for each outcome (α=0.05). Results: The interaction of HF and Tc factors decreased the fatigue resistance for both cements (U200 542.63>U200/HF-Tc 495.00; MA 544.47>MA/HF-Tc 506.84). Comparing the cements associated with HF or Tc, there was statistical superiority for MA (U200-Tc 537.37<MA-Tc 561.32; U200/HF 535.79<MA/HF 557.11), and no statistical difference was detected when only cement type or its association with HF-Tc was compared (U200 542.63=MA 544.47; U200/HF-Tc 495.00=MA/HF-Tc 506.84). The fracture always originated from defects at the ceramic-intaglio surface as radial cracks. Conclusion: HF etching plus silane agent increased the ceramic surface free energy and its wettability, but it did not provide better results in terms of fatigue resistance compared with silane agent application only. The association of HF etching and aging significantly reduced the fatigue resistance of the material, regardless of the resin cement used.

scholarly journals Influence of Hydrofluoric and Nitric Acid Pre-Treatment and Type of Adhesive Cement on Retention of Zirconia Crowns

Materials ◽  
2021 ◽  
Vol 14 (4) ◽  
pp. 960
Author(s):  
Osama Harb ◽  
Walid Al-Zordk ◽  
Mutlu Özcan ◽  
Amal Abdelsamad Sakrana
Keyword(s):  
Nitric Acid ◽  
Mean Value ◽  
Cement Type ◽  
Main Mode ◽  
Mode Of Failure ◽  
Zirconia Crowns ◽  
Pre Treatment ◽  
The Impact ◽  
Adhesive Cement ◽  
Retention Strength

Background: The aim of this study was to test the impact of hot acids etching and two types of adhesive cement on the retention of zirconia crowns. Methods: Forty maxillary premolars were prepared, and zirconia crowns were designed and fabricated with proximal extensions, then divided into 4 groups (n = 10). Group AP; the crowns were air-abraded and cemented using Panavia SA Cement. Group AL; the crowns were air- abraded and cemented using GC LinkForce. Group AHP; the crowns were air-abraded, etched with the hot acids (48% hydrofluoric acid and 69% nitric acid), and cemented using Panavia SA Cement. Group AHL; the crowns were air-abraded, etched with the hot acids, and cemented using GC LinkForce. Each zirconia crown was pre-treated and bonded to its corresponding tooth. After thermocycling (5–55 °C/10,000), the retention test was performed and the load required to dislodge the crown was reported in Newton (N), and mode of failure was recorded. The retention strength (MPa) was calculated for each tested variable and statistically analyzed. Results: Group AHP showed the highest mean value of the retention strength, followed by group AP then group AHL. Group AL showed the lowest value. A statistically significant effect (p = 0.001) of the hot acids etching on the retention of zirconia crown was found. Also, there was a significant effect (p = 0.000) of the cement type. The interaction between surface treatment and the cement type has no significant impact (p = 0.882). The main mode of failure for Panavia SA Cement is mixed mode of failure, while for G-CEM LinkForce is adhesive failure. Conclusions: Hot acid etching pre-treatment improved the retention of zirconia crown. Usage of Panavia SA Cement with hot acids etching is effective can be used for adhesive cementation of zirconia crown.

Influence of CAD/CAM Fabrication and Sintering Procedures on the Fracture Load of Full-Contour Monolithic Zirconia Crowns as a Function of Material Thickness

2020 ◽  
Vol 45 (2) ◽  
pp. 219-226 ◽  
Author(s):  
M Zimmermann ◽  
A Ender ◽  
A Mehl
Keyword(s):  
Computer Aided Design ◽  
Mean Value ◽  
Fracture Load ◽  
Significance Level ◽  
Material Thickness ◽  
Computer Aided ◽  
Cad Cam ◽  
Zirconia Crowns ◽  
Monolithic Zirconia

Summary Objective: The purpose of this in vitro study was to analyze the effect of computer-aided design/computer-aided manufacturing (CAD/CAM) fabrication and sintering procedures on the fracture load of monolithic zirconia crowns with different material thicknesses adhesively seated to methacrylate dies fabricated with stereolithography technology. Method: Monolithic zirconia crowns were fabricated from inCoris TZI C material with a chairside CAD/CAM system (CEREC MCXL) comprising three material thicknesses (0.5/1.0/1.5 mm, n=8 each). Two CAD/CAM fabrication procedures (milling, MI; grinding, GR), two chairside sintering procedures (superspeed, SS; speedfire sintering, SF), and one labside sintering procedure (classic, CL) were evaluated. In total, 144 crowns were fabricated. Restorations were adhesively seated to methacrylate dies fabricated with SLA technology. Thermomechanical cycling (TCML) was performed before fracture testing. Loading forces until fracture were registered and statistically analyzed with one-way analysis of variance (ANOVA), post hoc Scheffé test, and three-way ANOVA (α=0.05). Results: Test groups showed statistically significant differences (p<0.05). The highest mean value was found for 1.5-mm crowns of group GR_SF with 3678.6 ± 363.9 N. The lowest mean value was found for group 0.5-mm crowns of group MI_SF with 382.4 ± 30.7 N. There was a significant three-way interaction effect between thickness, sintering, and processing [F(4,126)=9.542; p<0.001; three-way ANOVA, significance level α=0.05]. Conclusions: CAD/CAM fabrication and sintering procedures influence the maximum loading force of monolithic zirconia crowns with different material thicknesses. A material thickness of 0.5 mm should be considered as a critical thickness for monolithic zirconia crown restorations.

scholarly journals Novel Electronic Device to Quantify the Cyclic Fatigue Resistance of Endodontic Reciprocating Files after Using and Sterilization

2020 ◽  
Vol 10 (14) ◽  
pp. 4962 ◽  
Author(s):  
Álvaro Zubizarreta-Macho ◽  
Óscar Alonso-Ezpeleta ◽  
Alberto Albaladejo Martínez ◽  
Vicente Faus Matoses ◽  
Javier Caviedes Brucheli ◽  
...  
Keyword(s):  
Fatigue Resistance ◽  
Computer Aided Design ◽  
Electronic Device ◽  
Light Emitting Diode ◽  
Study Groups ◽  
Cyclic Fatigue ◽  
Time To Failure ◽  
Cyclic Resistance ◽  
Computer Aided ◽  
Number Of Cycles

Background: The aim of this study was to analyze the effects of the time of use (TU) and sterilization cycles (SC) of endodontic reciprocating files on cyclic fatigue resistance. Methods: One-hundred-and-twenty (120) Procodile NiTi endodontic reciprocating instruments were selected at random and distributed into the following study groups: A: 0 sterilization cycles/0s time of use (n = 10); B: 0/60 (n = 10); C: 0/120 (n = 10); D: 1/0 (n = 10); E: 1/60 (n = 10); F: 1/120 (n = 10); G: 5/0 (n = 10); H: 5/60 (n = 10); I: 5/120 (n = 10); J: 10/0 (n = 10); K: 10/60 (n = 10); and L: 10/120 (n = 10). A dynamic cyclic fatigue device was designed using computer-aided design/computer-aided engineering (CAD/CAE) technology and created with a 3D printer to simulate the pecking motion performed by the clinician. Failure of the endodontic rotary instrument was detected by a light-emitting diode-light-dependent resistor (LED-LDR) system controlled by an Arduino driver complex and management software. The results were analyzed using the ANOVA test. Results: All pairwise comparisons presented statistically significant differences between the time to failure, number of cycles to failure and number of cycles of in-and-out movement for the time of use study groups (p < 0.001), but not in the number of sterilization cycles (p > 0.05). Conclusions: The time of use of NiTi endodontic reciprocating files negatively affects dynamic cyclic fatigue resistance. Dynamic cyclic resistance is not affected by the number of sterilization cycles.

scholarly journals Influence of the Pecking Motion Frequency on the Cyclic Fatigue Resistance of Endodontic Rotary Files

2019 ◽  
Vol 9 (1) ◽  
pp. 45 ◽  
Author(s):  
Álvaro Zubizarreta-Macho ◽  
Jesús Mena Álvarez ◽  
Alberto Albaladejo Martínez ◽  
Juan José Segura-Egea ◽  
Javier Caviedes Brucheli ◽  
...  
Keyword(s):  
Fatigue Resistance ◽  
Computer Aided Design ◽  
Electrical Discharge Machining ◽  
Light Emitting Diode ◽  
Cyclic Fatigue ◽  
Distribution Parameter ◽  
Weibull Statistics ◽  
Shape Distribution ◽  
Computer Aided ◽  
Number Of Cycles

Purpose: To analyze the influence of the pecking motion frequency on the cyclic fatigue resistance of endodontic rotary files. Material and Methods: Sixty PlexV 25.06 endodontic rotary files were selected and distributed into three groups: 30 movements/min (n = 20), 60 movements/min (n = 20), and 120 movements/min (n = 20). A dynamic cyclic fatigue device was designed using Computer Aided Design/ Computer Aided Engineering (CAD/CAE) technology and manufactured by 3D impressions to simulate the pecking motion performed by an operator. Failures of the endodontic rotary files were detected by a Light-Emitting Diode (LED)/Light-Dependent Resistor (LDR) system controlled by an Arduino-Driver complex and management software. Endodontic rotary files were tested on an artificial root canal manufactured by wire electrical discharge machining (EDM), with similar dimensions to those of the instrument under examination. Endodontic rotary files were used following the manufacturer’s recommendations. The results were analyzed by ANOVA and Weibull statistics. Results: All pairwise comparisons revealed statistically significant differences in all three variables, except for the difference in the number of cycles between the groups with 60 and 120 movements/min (p = 0.298). The scale distribution parameter of Weibull statistics showed statistically significant differences in all three variables, except for the differences in the number of cycles between groups with 30 and 60 movements/min (p = 0.0722). No statistically significant differences in the three variables were observed for the shape distribution parameter. Conclusion: A low frequency of pecking motion is recommended to reduce the risk of failure of endodontic rotary files associated with cyclic fatigue.

scholarly journals Adhesion to Zirconia: A Systematic Review of Surface Pretreatments and Resin Cements

Materials ◽  
2021 ◽  
Vol 14 (11) ◽  
pp. 2751
Author(s):  
Rubén Comino-Garayoa ◽  
Jesús Peláez ◽  
Celia Tobar ◽  
Verónica Rodríguez ◽  
María Jesús Suárez
Keyword(s):  
Systematic Review ◽  
Artificial Aging ◽  
Meta Analysis ◽  
Resin Cement ◽  
Air Abrasion ◽  
Surface Pretreatment ◽  
Adhesive Cementation ◽  
The One ◽  
Focus Question ◽  
Adhesive Cement

This systematic review aims to evaluate the different pretreatments of the zirconia surface and resin cement in order to determine a valid operative protocol for adhesive cementation. Methodologies conducted for this study followed the Prisma (Preferred Reporting Items for Systematic Reviews and Meta-Analysis) guidelines. An electronic search was performed in four databases. The established focus question was: “What type of surface conditioning method is the one that obtains the best adhesion values to zirconia over time by applying a resin cement?” Forty-five relevant papers were found to qualify for final inclusion. In total, 260 different surface pretreatment methods, mainly combinations of air-abrasion protocols and adhesive promoters, were investigated. Altogether, the use of two artificial aging methods, three types of cement and four testing methods was reported. The results showed that mechanicochemical surface pretreatments offered the best adhesive results. Self-adhesive cement and those containing 10-MDP obtained the best results in adhesion to zirconia. Artificial aging reduced adhesion, so storage in water for 30 days or thermocycling for 5000 cycles is recommended. A standardized adhesive protocol has not been established due to a lack of evidence

scholarly journals Influence of Different Surface Pretreatments on Shear Bond Strength of an Adhesive Resin Cement to Various Zirconia Ceramics

Materials ◽  
2020 ◽  
Vol 13 (3) ◽  
pp. 652 ◽  
Author(s):  
Marco Colombo ◽  
Simone Gallo ◽  
Sara Padovan ◽  
Marco Chiesa ◽  
Claudio Poggio ◽  
...  
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Tetragonal Zirconia ◽  
Resin Cement ◽  
Zirconia Ceramic ◽  
Adhesive Resin ◽  
Surface Pretreatment ◽  
Significant Difference ◽  
Computer Aided ◽  
Adhesive Resin Cement

The aim of this in vitro study was to assess the influence of surface pretreatment on shear bond strength (SBS) of an adhesive resin cement (G-CEM Link Force TM, GC Corporation, Tokyo, Japan) to three different yttria-stabilized tetragonal zirconia polycrystalline (Y-TZP) ceramics: (1) Copran Zirconia Monolith HT, COP; (2) Katana ML Zirconia, KAT; and (3) Metoxit Z-CAD HTL Zirconia, MET. In total, 45 cylinders (5 mm in diameter, 1 mm height) for each type of zirconia ceramic were prepared used a computer-aided design and computer-aided manufacturing (CAD/CAM) machine (software CEREC 4.2). Each type of zirconia was subdivided into three groups and each group received a different surface pretreatment; 15 samples were not conditioned as control (groups COP 1, KAT 1, MET 1), 15 samples were air-borne particle abraded with aluminum dioxide particles of 50-μm size at 0.3 MPa for 20 s (groups COP 2, KAT 2, MET 2), and 15 samples were hot-etched with a solution of hydrochloric acid and ferric chloride (groups COP 3, KAT 3, MET 3). After specimen fabrication, the adhesive cement–ceramic interface was analyzed using an SBS test. Subsequently, the adhesive remnant index (ARI) was measured. Data were submitted to statistical analysis. Air-borne particle abraded specimens showed the highest SBS values for COP and KAT groups. For MET, no significant difference was reported between air-borne particle abraded specimens and untreated controls. The lowest values were detected for acid-etched groups. A higher frequency of ARI = “1” and ARI = “2” was reported in control and air-borne particle abraded groups, whereas ARI = “3” was detected in hot-etched groups. No correlation was found between ARI score and shear bond strength. Air-borne particle abrasion is considered the best treatment for Zirconia Copran and Zirconia Katana ML, if it is followed by using dual-curing resin cement.

scholarly journals Shaping and Centering Ability, Cyclic Fatigue Resistance and Fractographic Analysis of Three Thermally Treated NiTi Endodontic Instrument Systems

Materials ◽  
2020 ◽  
Vol 13 (24) ◽  
pp. 5823
Author(s):  
Saulius Drukteinis ◽  
Vytaute Peciuliene ◽  
Ruta Bendinskaite ◽  
Vilma Brukiene ◽  
Rasmute Maneliene ◽  
...  
Keyword(s):  
Fatigue Resistance ◽  
Cyclic Fatigue ◽  
Fractographic Analysis ◽  
Significance Level ◽  
Root Canals ◽  
Topographic Features ◽  
New Instrument ◽  
Before And After ◽  
Number Of Cycles ◽  
Thermally Treated

The better understanding of the clinically important behavioral features of new instrument systems has an important significance for the clinical endodontics. This study aimed to investigate the shaping and centering ability as well as cyclic fatigue resistance of HyFlex CM (CM), HyFlex EDM (EDM) and EdgeFile (EF) thermally treated nickel–titanium (NiTi) endodontic instrument systems. Sixty curved root canals of the mesial roots of mandibular molars were randomly assigned into three groups (n = 20) and shaped using CM, EDM and EF files up to the size 40 and taper 04 of the instruments. µCT scanning of the specimens before and after preparation was performed and the morphometric 2D and 3D parameters were evaluated in the apical, middle and coronal thirds of root canals. In each group, 40.04 instruments (n = 20) were subjected to the cyclic fatigue resistance test in artificial root canals at 37 °C temperature until fractures occurred, and the number of cycles to failure (NCF) was calculated. The fractographic analysis was performed using a scanning electron microscope, evaluating topographic features and surface profiles of the separated instruments. The one-way analysis of variance with post hoc Tuckey’s test was used for statistical analysis of the data; the significance level was set at 5%. All systems prepared the comparable percentage of root canal surface with the similar magnitude of canal transportation in all root thirds (p > 0.05), but demonstrated significantly different resistance to cyclic fatigue (p < 0.05). The most resistant to fracture was EF, followed by EDM and CM. The length of the fractured fragments was not significantly different between the groups, and fractographic analysis by SEM detected the typical topographic features of separated thermally treated NiTi instrument surfaces.

scholarly journals Cyclic fatigue resistance of 2Shape, Twisted File and EndoSequence Xpress nickel-titanium rotary files at intracanal temperature

2018 ◽  
Vol 12 (4) ◽  
pp. 283-287 ◽  
Author(s):  
Gülşah Uslu ◽  
Taha Özyürek ◽  
Mustafa Gündoğar ◽  
Koray Yılmaz
Keyword(s):  
Fatigue Resistance ◽  
Statistical Significance ◽  
Cyclic Fatigue ◽  
Nickel Titanium ◽  
Bonferroni Correction ◽  
Significant Difference ◽  
Inner Diameter ◽  
The Difference ◽  
Number Of Cycles ◽  
Analyze Data

Background. The aim of this study was to compare the cyclic fatigue resistance of 2Shape, Twisted File (TF) and EndoSequence Xpress (ESX) nickel-titanium rotary files at intracanal temperature (35°C). Methods. Twenty 2Shape TS1 (25/.04), 20 TF (25/.04) and 20 ESX (25/.04) files were tested for cyclic fatigue at intracanal temperature (35°C). All the instruments were rotated in artificial canals which were made of stainless steel with an inner diameter of 1.5 mm, 60° angle of curvature and a radius curvature of 5 mm until fracture occurred; the time to fracture was recorded in seconds using a digital chronometer and the number of cycles to fracture (NCF) for each file was calculated. Kruskal-Wallis test with Bonferroni correction was performed to statistically analyze data using SPSS 21.0. Statistical significance was set at P<0.05. Results. NCF values revealed that the 2Shape had significantly the highest cyclic fatigue resistance, followed by TF and ESX at intracanal temperature (P<0.05). The difference was significant between the TF and ESX groups (P<0.05). There was no significant difference among the 2Shape, TF and ESX files with respect to the lengths of the fractured file fragments (P>.05). Conclusion. Within the limitations of present study, it was concluded that the cyclic fatigue resistance of 2Shape files at the intracanal temperature is higher than that of TF and ESX files.

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