scholarly journals Analisis Pertumbuhan Fase Superkonduktor BSCCO-2212 dan BPSCCO-2212 Akibat Variasi Suhu Sintering Menggunakan Metode Pencampuran Basah

2021 ◽  
Vol 2 (4) ◽  
pp. 86-95
Author(s):  
Pulung Karo Karo ◽  
◽  
Risky Putra Ramadhan ◽  
Suprihatin Suprihatin ◽  
Yanti Yulianti
Keyword(s):  
Volume Fraction ◽  
Sintering Temperature ◽  
Superconducting Phase ◽  
Phase Purity ◽  
Optimum Point ◽  
Purity Level ◽  
Degree Of Orientation ◽  
Mixing Method

The research was conducted to determine the effect of sintering temperature on the level of purity of the superconducting phase BSCCO-2212 and BPSCCO-2212 using the wet mixing method. Sintering was carried out for 20 hours with variations in sintering temperature: 825, 830, 835 and 840°C. XRD results showed that the phase purity level increased until it reached the optimum point at 835°C sintering temperature and then decreased at 840°C. The highest volume fraction of the BSCCO-2212 sample was obtained at a sintering temperature of 835°C at 71.09% and the highest degree of orientation was obtained at a sintering temperature of 830°C at 26.44%. In the BPSCCO-2212 sample, the highest volume fraction was obtained at a sintering temperature of 835°C at 52.59% and the highest degree of orientation at a sintering temperature of 830°C at 43.49%. The results of the comparison of BSCCO-2212 and BPSCCO-2212 samples showed that the BPSCCO-2212 sample had a higher level of phase purity than BSCCO-2212.

scholarly journals Sintesis Superkonduktor BSCCO-2223 dengan Variasi Waktu Sintering pada Kadar Ca=2,10 Menggunakan Metode Pencampuran Basah

2019 ◽  
Vol 7 (2) ◽  
pp. 139-144
Author(s):  
Siti Istikomah ◽  
◽  
Suprihatin Suprihatin ◽  
Agus Riyanto ◽  
◽  
...  
Keyword(s):  
Volume Fraction ◽  
Orientation Degree ◽  
Phase Purity ◽  
Sintering Time ◽  
Purity Level ◽  
Degree Of Orientation ◽  
Mixing Method

Research about the effect of sintering time on the phase purity level of superconductor BSCCO-2223 at the level of Ca 2,10 has been synthesized using the wet-mixing method. Sample dissolved is slowly with HNO3 and aquades, then drying gradually temperature of 300, 400, 600 °C. The sample was calcined for 10 hours at 800 °C and sintered using variations of time 10, 20, 30, and 40 hours at 865°C. Variations were carried out to determine the effect of sintering time on the purification of the superconductor. XRD results show that sintering time has an effect on the volume fraction value of BSCCO-2223. Volume fraction that is relatively high at 30 hours sintering time is 79,17 % with an orientation degree value of 37.94%. While the lowest was obtained at the time of sintering for 10 hours with the volume fraction of 38.47% with a degree of orientation of 15.27%. the SEM results show that all samples have layers oriented and have relatively little space between the plates (voids).

scholarly journals Pengaruh Variasi Waktu Sintering Terhadap Pertumbuhan Fase Bahan Superkonduktor BSCCO-2212 dengan Kadar Ca=1,10 Menggunakan Metode Pencampuran Basah

2020 ◽  
Vol 1 (1) ◽  
pp. 7-11
Author(s):  
Karlina Rahmah ◽  
◽  
Suprihatin Suprihatin ◽  
Pulung Karo Karo ◽  
◽  
...  
Keyword(s):  
Volume Fraction ◽  
High Volume ◽  
Superconducting Phase ◽  
High Volume Fraction ◽  
Orientation Degree ◽  
Phase Purity ◽  
Characterization Result ◽  
Sintering Time ◽  
Mixing Method ◽  
High Orientation

This research was conducted to determine the effect of sintering time on the formation of the superconducting phase BSCCO-2212 by calculating the level of purity of the phases formed and looking at the microstructure. The variation of sintering time was 10, 20, 30 and 40 hours using the wet mixing method. The sample was calcinated with 800 °C for 10 hours and sintered with 830 °C. The XRD’s characterization result shows a decrease in phase purity with increasing the sintering time. The relative high volume fraction of the BSCCO-2212/ts10 sample is 90,48% while, the lowest volume fraction of BSCCO-2212/tc40 is 50,74%. The relative high orientation degree of BSCCO-2212/ts20 is 18,47% and the lowest orientation degree of BSCCO-2212/ts10 is 8,4%. The SEM’s characterization result shows of all samples have been oriented and have relatively little space between slabs (voids).

scholarly journals Pengaruh Variasi Kadar CaCO3 terhadap Pertumbuhan Fase Superkonduktor BPSCCO–2212 Menggunakan Metode Pencampuran Basah

2021 ◽  
Vol 2 (1) ◽  
pp. 17-22
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Volume Fraction ◽  
Superconducting Phase ◽  
Maximum Point ◽  
X Ray Diffraction ◽  
X Ray ◽  
Degree Of Orientation ◽  
Mixing Method ◽  
Scanning Electron

This research was conducted to determine the effect of CaCO3 levels on the formation of superconducting phase BPSCCO - 2212 by calculating the level of purity of the phases formed and looking at the microstructure. The variation of CaCO3 was 0.95, 1.00, 1.05 and 1.10 mole using the wet mixing method. The samples were calcined at 800 ° C for 10 hours, and sintered at 820 ° C for 20 hours. Synthesized samples were characterized using X-Ray Diffraction (XRD) and Scanning Electron Microscopy (SEM). The XRD’s chacterization results show that the level of purity of the formed phases increases with increasing Ca levels with maximum point at BPSCCO-2212/1.10 mole. The highest volume fraction was 79,06% in the BPSCCO-2212/1.10 sample. While the lowest volume fraction was 72.10% in the BPSCCO-2212/0.95 sample. Meanwhile, the highest degree of orientation was 20.59% at BPSCCO-2212/0.95. The lowest degree of orientation was 8.46% at BPSCCO-2212/1.10. SEM’s chacterization results show of all samples have been oriented altought not perfect yet and have relatively little space between slabs (voids).

scholarly journals Pengaruh Variasi Suhu Sintering Menggunakan Metode Pencampuran Basah

2020 ◽  
Vol 1 (2) ◽  
pp. 53-57
Author(s):  
M Muntamijayati ◽  
◽  
Suprihatin Suprihatin ◽  
Yanti Yanti ◽  
Simon Sembiring ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Volume Fraction ◽  
Sintering Temperature ◽  
X Ray Diffraction ◽  
X Ray ◽  
A Value ◽  
Degree Of Orientation ◽  
Mixing Method ◽  
Scanning Electron

The superconducting material BPSCCO-2212 with doping Pb = 0,2 has been synthesized by the wet mixing method. Calculation is caried out at 800 °C for 10 hours. While sintering is done at 825 °C, 830 °C, 835 °C and 840 °C for 20 hours. The synthesis result were characterized by XRD X-Ray Diffraction) and SEM (Scanning Electron Microscopy). The XRD spectrum analysis results that have been processed using celref, show that in general the samples produced have formed the BPSCCO-2212 phase (indicated the presence of Bi-2212 peaks) and have been oriented (indicated the existence of peaks with h = k = 0, l even number). For the calculation result obtanced the highest volume fraction value at 830 °C sintering temperature with a value FV = 66,97 % and the highest degree of orientation at 825 °C with a value of P = 76,54 %. The results of the SEM photo recorder generally show that the crystals formed are oriented.

scholarly journals Pengaruh Suhu Sintering Terhadap Pembentukan Fase Superkonduktor BSCCO-2223 dengan Kadar Ca = 2,10 Menggunakan Metode Pencampuran Basah

2019 ◽  
Vol 7 (2) ◽  
pp. 133-138
Author(s):  
Komala Dewi ◽  
◽  
Suprihatin Suprihatin ◽  
Syafriad Syafriad ◽  
◽  
...  
Keyword(s):  
Volume Fraction ◽  
Sintering Temperature ◽  
Empty Space ◽  
Temperature Variations ◽  
Orientation Degree ◽  
Mixing Method ◽  
Materials Used

This study was conducted to determine the effect of sintering temperature on the formation of BSCCO-2223 superconductor phase with levels of Ca = 2,10 using the wet mixing method. The materials used were Bi2O3, SrCO3, CaCO3, CuO, HNO3 and aquades. Synthesis is carried out by dissolving the materials using HNO3 and aquades slowly then the solution is dried for 40 hours at a temperature of 300, 400 and 600 °C gradually. The samples were calcined at 800 ° C for 10 hours and each was sintered with temperature variations of 850, 855, 860 and 865 °C for 20 hours. The XRD result shows that the sintering temperature has an effect on the formation of BSCCO-2223 superconductor phase, with volume fraction value which tends to increase with increasing sintering temperature. The highest volume fraction was obtained in the BSCCO-2223 sample with sintering temperature of 865 °C which is 79,49%. SEM result shows that all samples have arranged layers (oriented) with relatively small empty space between the plaques (void). The highest orientation degree is in the BSCCO-2223 sample with sintering temperature of 860 °C which is 23,77%.

STABILIZATION OF Bi(2223) SUPERCONDUCTING PHASE BY VANADIUM OXIDE ADDITION

1993 ◽  
Vol 07 (01n03) ◽  
pp. 157-161 ◽  
Author(s):  
D. SURESH BABU ◽  
G. NARSING RAO ◽  
L. BROHAN ◽  
M. GANNE
Keyword(s):  
Critical Current Density ◽  
Current Density ◽  
Flux Pinning ◽  
Volume Fraction ◽  
Ac Susceptibility ◽  
Superconducting Phase ◽  
Nominal Composition ◽  
Oxide Addition ◽  
Probable Role

We report on the ac susceptibility, microwave absorption and dc magnetization of Bi 2− x V x Sr 2 Ca 2 Cu 3 O y (nominal composition). The low T c (2212) phase ( T c = 85 K ) dominates in the x = 0 sample with extremly weak flux pinning. In x = 0.4 sample, both flux pinning and volume fraction of the high T c (2223) phase ( T c = 105 K ) were increased. The intragrain critical current density of the sample with x = 0.4 was estimated and found to be comparable with that of Pb doped Bi 2 Sr 2 Ca 2 Cu 3 O y superconductor. The data suggest that addition of V 2 O 5 in Bi 2 Sr 2 Ca 2 Cu 3 O y system increases the volume fraction of the high T c phase. Probable role of vanadium in enhancing the high T c (2223) phase in Bi-V-Sr-Ca-Cu-O system is discussed.

Microstructure and Mechanical Properties of In Situ TiB2/6061 Composites

2012 ◽  
Vol 535-537 ◽  
pp. 14-17
Author(s):  
Long Hua Zhong ◽  
Yu Tao Zhao ◽  
Song Li Zhang ◽  
Rong Wen
Keyword(s):  
Master Alloy ◽  
Volume Fraction ◽  
X Ray Diffraction ◽  
Melt Mixing ◽  
X Ray ◽  
Mixing Method ◽  
Particulate Volume Fraction ◽  
Ti Powder ◽  
Particulate Volume

In situ TiB2/6061 composites have been successfully synthesized through chemical reaction between 6061 master alloy, Al-3B master alloy and Ti powder. The composites fabricated by direct melt mixing method was investigated by Scanning Electron Microscope (SEM), Energy Dispersive x-ray Spectroscopy (EDS) and X-Ray Diffraction (XRD), The results shown the existence of TiB2particles. The size of most TiB2particles were just in micron level, and even reached to sub-micron level. The increase in microhardness and tensile strength for the as-prepared composites with 5% particulate volume fraction (PVF) are up to 26.8% and 51.2% respectively.

Structure and Morphology Properties of Nanosized La0.75K0.05Ba0.05Sr0.15MnO3 Manganite

2020 ◽  
Vol 860 ◽  
pp. 106-111
Author(s):  
Dhawud Sabilur Razaq ◽  
Budhy Kurniawan ◽  
Ikhwan Nur Rahman ◽  
Dicky Rezky Munazat
Keyword(s):  
Bond Length ◽  
Crystallite Size ◽  
Sintering Temperature ◽  
Bond Angle ◽  
Sol Gel ◽  
Rhombohedral Structure ◽  
Phase Purity ◽  
X Ray ◽  
Structure And Morphology ◽  
Scanning Electron

Nanosized La0.75K0.05Ba0.05Sr0.15MnO3 manganite have been synthesized using sol-gel method. Afterwards, the samples were sintered at eight different temperature ranging from 650 to 1000 °C. Phase purity, crystal structure and the morphology of the sample have been examined using X-Ray Diffractometer (XRD) and Scanning Electron Microscope. It has been found that different higher sintering temperature greatly affect the phase purity and crystallite size of the sample. Regardless of the sintering temperature, all the samples crystallized in rhombohedral structure with R-3c space group. The crystallite size of the samples is found to increase from 41.59 nm up to 73.42 nm as the sintering temperature increases. Further analysis from XRD result shows that sintering temperature also affect the average Mn-O bond length and Mn-O-Mn bond angle of the sample. The average Mn-O bond length is found to increase while the average Mn-O-Mn bond angle tends to decrease as sintering temperature increases. SEM measurement shows that various grain size ranging from ~100 nm up to ~ 350 nm exists in all the sample regardless the sintering temperature.

Explorative Synthesis of Magnetic Ca-Fe-O Compounds by Mixing Precipitated CaCO3 from Limestone and Iron Sand Extracted – Fe2O3.H2O

2015 ◽  
Vol 827 ◽  
pp. 203-207 ◽  
Author(s):  
Mastuki ◽  
Malik Anjelh Baqiya ◽  
Darminto
Keyword(s):  
Calcium Carbonate ◽  
Sintering Temperature ◽  
Raw Material ◽  
Phase Content ◽  
Precipitated Calcium Carbonate ◽  
Mixing Method

Synthesis of Ca-Fe-O using solution mixing method employing CaCO3 and Fe2O3•H2O has been conducted. Extraction of limestone as the raw material of precipitated calcium carbonate (PCC) and iron sands as that of Fe2O3•H2O was prepared to explore various compound of C-Fe-O, where the CaFe4O7 phase is mainly expected. The PCC and Fe2O3•H2O each are dissolved in 1 M HNO3 and mixed to be most homogeneous. The results of the synthesis are characterized by DTA/GTA and then sintered at temperatures of 800°C, 900°C and 1000°C.The sintered samples were characterized by XRD, FTIR, and VSM. The sintering temperature at 800°C, 900°C and 1000°C gave result the phase content of CaFe4O7 being respectively 55.42%, 44.55% and 36.39%. Other major phases in the Ca-Fe-O samples consist of Ca2Fe9O13 and Ca4Fe14O25. The remanence value of the corresponding samples is 2.11, 1.28, and 1.74 emu/g respectively.

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