scholarly journals INVESTIGATION OF SURFACE FUNCTIONALIZATION AND COATINGS FOR BIOMEDICAL APPLICATIONS BY ZETA POTENTIAL AND ADSORPTION MEASUREMENTS ON SOLID SURFACES

Author(s):  
SILVIA SPRIANO ◽  
SARA FERRARIS ◽  
MARTINA CAZZOLA ◽  
VERONICA PERETTI
2021 ◽  
pp. 096739112110384
Author(s):  
Christian Chapa González ◽  
Javier Ulises Navarro Arriaga ◽  
Perla Elvia García Casillas

The physicochemical properties of the nanoparticle surface determine the performance of nanocomposites in biomedical applications such as their biodistribution and pharmacokinetics. The physicochemical properties of chitosan, such as apparent charge density and solubility, are pH dependent. Similarly, Fe3O4 nanoparticles are susceptible to variations in their physicochemical properties due to changes in pH. In this work, we evaluated the physicochemical properties of chitosan–magnetite nanocomposites that were suspended at pH 7.0, 9.0, and 11.0 to determinate the effect on particle size, zeta potential, and mass percentage of the polymeric coating, in addition to the crystalline phase and magnetic properties of magnetite phase. X-ray diffraction results exposed that the present phase was magnetite with no other phases present and that the crystallite size was between 10.8 and 14.1 nm. Fourier transform infrared verified the chitosan functional groups in treated samples while the percentage of mass determined by TGA found to be nearly 9%. Scanning electron microscopy micrographs corroborated the spherical shape of the bare and chitosan-coated nanoparticles. Dynamic light scattering results showed that chitosan coating modifies the zeta potential, going from a potential of −11.8 mV for bare particles to −3.0 mV (pH 11). Besides, vibrating sample magnetometer measurements showed that coercivity remained very low, which is desirable in biomedical applications.


2014 ◽  
Vol 24 (33) ◽  
pp. 5269-5276 ◽  
Author(s):  
Christian Peters ◽  
Olgaç Ergeneman ◽  
Pedro D. Wendel García ◽  
Michelle Müller ◽  
Salvador Pané ◽  
...  

2013 ◽  
Vol 25 (26) ◽  
pp. 3616-3616 ◽  
Author(s):  
Weiwei Gao ◽  
Che-Ming J. Hu ◽  
Ronnie H. Fang ◽  
Brian T. Luk ◽  
Jing Su ◽  
...  

2006 ◽  
Vol 314 ◽  
pp. 19-24 ◽  
Author(s):  
Cornelia Bellmann ◽  
Anja Caspari

The process of electrophoretic deposition depends strongly on the electrokinetic properties and with it the surface properties of the material that will be processed. Different additives, conditioners but also the suspending liquid influence the surface of the applied material by adsorption. Electrokinetic investigations reflect changes in properties at the outermost solid surface very sensitive. Streaming potential measurements are especially suited for studying such changes of surface chemistry at solids with different shapes. Two approaches are applicable: 1. The adsorption process was done before measuring. The result of this process should be shown. In this case it will be interesting to see differences in the functionality of the solid surface. The zeta potential will be measured versus different pH value. 2. The adsorption process will be studied directly. The zeta potential will be determined versus the concentration of the adsorptive. The second approach can be used for investigation of adsorption of multicomponent mixtures. Competing adsorption processes are detectable.


2020 ◽  
Vol 39 (3) ◽  
Author(s):  
U.M. Badeggi ◽  
B.A. Lawal ◽  
A.O. Akinfenwa ◽  
Y.O. Ayipo ◽  
Y. Azeh ◽  
...  

In the present study, Pelargonium sidoides (PS) extract was used in the green synthesis of AuNPs that was characterized by UV-Vis, TEM, SAED, EDS, XRD, FTIR, and DLS. UV-Vis showed a surface plasmon resonance (SPR) at λmax of 532 nm while TEM shows that the particles are predominantly spherical and monodispersed. DLS measurement indicated the particle size and the zeta potential to be 27.20 nm and -24.0 mV respectively. The in vitro stability of the hybrid particles in different solutions and buffers (pH 7 and 9) confirmed that the particles are stable over a given period. The method employed is simple, environmentally friendly, and inexpensive. Our studies suggest that the Pelargonium sidoides-gold nanoparticles (PS-AuNPs) may be safely used in biomedical applications such as drug delivery. Keywords: Pelargonium sidoides; biosynthesis; biomedicals; capping agent; zeta potential


Polimery ◽  
2021 ◽  
Vol 66 (9) ◽  
pp. 451-458
Author(s):  
Nur Fathin Amirah Shafie ◽  
Mohd Yusof Hamzah ◽  
Roshafima Rasit Ali

The influence of 2-(dimethylamino)ethyl methacrylate (DMAEMA) concentration on the temperature sensitivity of nanogels based on N-isopropylacrylamide (NIPAAM), poly(vinylpyrrolidone) (PVP), poly(ethylene glycol) diacrylate (PEGDA) by gamma radiation induced polymerization was investigated. Dynamic light scattering (DLS) and zeta potential measurements were used to characterize the nanogels. Temperature has been found to cause the nanogel particles to swell and shirnkage, allowing controlled dosing of the drug contained in capsules. The developed nanogels are promising materials with great potential for biomedical applications.


2021 ◽  
Author(s):  
Reddhy Mahle ◽  
Partha Kumbhakar ◽  
Divya Nayar ◽  
Tharangattu N. Narayanan ◽  
Kishor Kumar Sadasivuni ◽  
...  

Recent progress in the bio-mediated preparation of quantum dots as a greener and efficacious approach towards their surface functionalization in light of their varied applications is summarised.


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