scholarly journals Effect of calcium carbonate filler and alkali treatment on physical and elastic properties of jute mat reinforced polyester resin composites

2020 ◽  
Vol 26 (2) ◽  
pp. 61-68
Author(s):  
Rahima Nasrin ◽  
Salma Begum ◽  
MA Gafur ◽  
AH Bhuiyan ◽  
AH Bhuiyan

Polyester resin-jute mat reinforced composites with different wt% of calcium carbonate (CaCO3) filler were fabricated using a simple cold press molding method. The effects of CaCO3 filler and alkali (NaOH) treatment on various physical and elastic properties were evaluated. Water absorption (WA) increases with the increase of soaking time and load. The maximum WA was observed for 5 wt% addition of CaCO3 and for more CaCO3, WA decreases. The ultimate tensile strength (UTS) and flexural strength (FS) decreases with the addition of CaCO3 for 0.5 wt% NaOH treated composites but for 5 wt% NaOH treated composites UTS and FS increases with the addition of CaCO3 filler. The optimum filler addition is about 5 wt% CaCO3. With the addition of CaCO3, tangent modulus increases for 0.5 wt% NaOH treated composites and for 5 wt% NaOH treated composites it increases up to a maximum value and then decreases. The effect of load on tensile and flexural properties is also discussed. Bangladesh Journal of Physics, 26(2), 61-68, December 2019

2021 ◽  
Vol 20 (1) ◽  
pp. 1
Author(s):  
Muhammad Ghozali ◽  
Dody Ariawan ◽  
Eko Surojo

<p>Natural fiber reinforced composites is one materials potentially developing in Indonesia. One of biggest problem with composites specimen is its void. One properties to find out void of composites is composites density value. The objective of research is to investigate the effect of fiber alkali (NaOH) treatment and microcrystalline cellulose (MCC) addition on density value of cantala fiber reinforced unsaturated polyester composites. Firstly, cantala fibers was submerged into alkali (NaOH) 6% solution for 0, 3, 6, 9, and 12 hours. Furthermore, the fiber was washed using acetid acid and then using clean water to reach pH 7. Thereafter, cantala fiber was dried in the oven for 10 hours at temperature 60<sup>0</sup>C. Composites was composed of cantala fiber, unsaturated polyester polymer matrix, and microcrystalline cellulose according to the composition with volume fraction 30%. Composites was casted using compression molding method with compressive strength of 10 MPa for 12 hours. All specimens of composites undertake post cure for 2 hours at 60<sup>0</sup>C. Density test was conducted using densimeter by calculating the density of composites in the air and the water. The result of research showed that the longer the alkali treatment time and the more addition of microcrystalline cellulose (MCC) filler, the higher is the composites density. The higher density value of cantala fiber reinforced unsaturated polyester is alkali treatment 6 hours, which was 1.223 gr/cm<sup>3</sup>.</p>


2010 ◽  
Vol 7 (4) ◽  
pp. 1400-1409
Author(s):  
Baghdad Science Journal

This study is attempt to improve thermal isolation through measuring thermal conductivity composite of on polyester resin with fillers of (TiO2, ZnO, Acrylonitril, wood flour Coconut (Wf). The grain size of the fillers is 200 µm. The number of samples is (16) in addition to the virgin sample; these samples are prepared by cast molding method for polyester with filler volume fractions (5%, 10%, 15% and 20%). Shore hardness tests were used to measure the hardness and Lee disk method for thermal conductivity. The experimental results showed that the (20% ZnO) sample has the maximum value of thermal conductivity where (20% w.f) has minimum thermal conductivity .on the other hand (15% ZnO) sample give the maximum value of hardness where (20% w.f) sample gave the minimum value of hardness. From this study there is an important factor that should be observed that is the relationship between hardness and thermal conductivity. The study prove that the experimental results satisfy the theoretical assumptions in that the additive material (fillers) of metals base increase thermal conductivity where the material of cellulose base decrease the thermal conductivity and give good thermal isolation but with low hardness and all the result above the refry sample .


2021 ◽  
Vol 12 (5) ◽  
pp. 6148-6163

Oil palm empty fruit bunch (OPEFB) single fibers and reinforced composites were comprehensively characterized through tensile tests to assess their performance as potential reinforcing materials in polymer composites. The performances of OPEFB single fibers and reinforced composites with untreated and treated fibers conditions were compared. The fibers were variously treated with 3% sodium hydroxide, 2% silane, 3% sodium hydroxide mixed with 2% silane, and 3% sodium hydroxide prior to 2% silane for 2 hours soaking time. The highest toughness of the single fibers test was then selected to proceed with composites fabrication. The OPEFB composites were fabricated in 90:10, 80:20, 70:30, and 60:40 epoxy-fibre fractions. The result shows that the selected treated fiber composite exhibits better performance. The selected treated fiber composite increased the highest ultimate tensile strength by 145.3% for the 90:10 fraction. The highest Young’s Modulus was increased by about 166.7% for 70:30 fraction. Next, the highest toughness was increased by 389.5% for the 30:70 fraction. The treated fibers provided a better interlocking mechanism between the matrix and fibers in reinforced composites, thus improving their interfacial bonding.


2011 ◽  
Vol 8 (2) ◽  
pp. 551-560
Author(s):  
Baghdad Science Journal

In this study, composite materials were prepared using unsaturated polyester resin as binder with two types of fillers (sawdust and chopped reeds). The molding method is used to prepare sheets of UPE / sawdust composite and UPE / chopped reeds composite. The mechanical properties were studied including flexural strength and Young's modulus for the samples at normal conditions (N.C). The Commercial wood, UPE and its composite samples were immersed in water for about 30 days to find the weight gain (Mt%) of water for the samples, also to find the effect of water on their flexural strength and Young's modulus. The results showed that the samples of UPE / chopped reeds composite gained highest values of flexural strength (24.5 MPa) and Young's modulus (5.1 GPa) as compared with other composites at (N.C). The results showed that the wet samples of sawdust composite have lowest values of weight gain (Mt %) of water (0.043%) as compared with other composites after immersion. Also it’s showed a slight decrease in values of Young's modulus for all the samples after immersion as compared with the samples at (N.C). Finally it’s showed a slight decrease in values of flexural strength for all the samples except for the composite material formed from UPE / chopped reeds which showed an increase in the value of flexural strength after immersion, where the wet samples of UPE / chopped reeds composite gained (29 MPa) as compared with the samples at (N.C).


2018 ◽  
Vol 32 (9) ◽  
pp. 1190-1203 ◽  
Author(s):  
Xuping Yang ◽  
Wenbin Yang ◽  
Jinghui Fan ◽  
Juying Wu ◽  
Kai Zhang

Thermally conductive and electrically insulating polyamide 6 (PA6) matrix quaternary composites were prepared by hot press molding and injection molding, respectively. The quaternary composites were composed of zero-dimensional aluminum oxide particle, one-dimensional silicon carbide whisker, two-dimensional flake graphite, and PA6 resin matrix. Morphology, structure, density, thermal conductivity, volume electrical resistivity, and tensile strength of two types of composites were characterized by scanning electron microscopy, X-ray diffractometer, thermal conductivity tester, high resistance micro-current tester, and tensile tester. The results showed that crystallinity, thermal conductivity, density, and tensile strength of hot press molding samples were superior to those of samples made by injection molding method. This is due to that hot press molding method can provide higher molding pressure and longer annealing time than injection molding. The mechanism could be explained that the performances of the composites were promoted by increasing molding pressure and annealing time.


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