scholarly journals Tensile Characterizations of Oil Palm Empty Fruit Bunch (OPEFB) Fibres Reinforced Composites in Various Epoxy/Fibre Fractions

2021 ◽  
Vol 12 (5) ◽  
pp. 6148-6163
Keyword(s):  
Sodium Hydroxide ◽  
Oil Palm ◽  
Fiber Composite ◽  
Tensile Tests ◽  
Empty Fruit Bunch ◽  
Reinforced Composites ◽  
Soaking Time ◽  
Single Fibers ◽  
The Matrix ◽  
Treated Fiber

Oil palm empty fruit bunch (OPEFB) single fibers and reinforced composites were comprehensively characterized through tensile tests to assess their performance as potential reinforcing materials in polymer composites. The performances of OPEFB single fibers and reinforced composites with untreated and treated fibers conditions were compared. The fibers were variously treated with 3% sodium hydroxide, 2% silane, 3% sodium hydroxide mixed with 2% silane, and 3% sodium hydroxide prior to 2% silane for 2 hours soaking time. The highest toughness of the single fibers test was then selected to proceed with composites fabrication. The OPEFB composites were fabricated in 90:10, 80:20, 70:30, and 60:40 epoxy-fibre fractions. The result shows that the selected treated fiber composite exhibits better performance. The selected treated fiber composite increased the highest ultimate tensile strength by 145.3% for the 90:10 fraction. The highest Young’s Modulus was increased by about 166.7% for 70:30 fraction. Next, the highest toughness was increased by 389.5% for the 30:70 fraction. The treated fibers provided a better interlocking mechanism between the matrix and fibers in reinforced composites, thus improving their interfacial bonding.

scholarly journals A review of oil palm fruit fiber reinforced composites

2022 ◽  
Vol 1212 (1) ◽  
pp. 012050
Author(s):  
B Bakri ◽  
Naharuddin ◽  
Mustafa ◽  
A Medi ◽  
L Padang
Keyword(s):  
Mechanical Properties ◽  
Chemical Composition ◽  
Surface Treatment ◽  
Oil Palm ◽  
Superheated Steam ◽  
Fiber Composite ◽  
Fiber Reinforced Composites ◽  
Empty Fruit Bunch ◽  
Reinforced Composites ◽  
Palm Fruit

Abstract Oil palm fibers have been developed as reinforcement in the composite. These fibers can be produced from fruit, trunk, and frond of oil palm. In this review, the oil palm fruit fiber for reinforcing composite was focused. Oil palm fruit fibers consist of empty fruit bunch (EFB) and mesocarp fruit (MF) fibers. The chemical composition and characteristics of oil palm fruit fiber are described. Furthermore, the mechanical properties of the composite are reported to be related to the surface treatment of EFB and MF fibers. Applications of such fiber composite are included in this review. From some researches, the surface treatment methods for MF and EFB fibers as reinforcement composite was conducted with using alkali, silane, acryilic acid, acetic anhydride, hydogen peroxide, microwave, and superheated steam. The effect of these surface treatments on oil palm EFB and MF fibers displayed the improvement of the mechanical properties (tensile, flexural and impact strengths) of the composite due to enhance the interface adhesion between fiber and matrix after treatment of fibers.

scholarly journals Sodium Hydroxide-Steam Explosion Treated Oil Palm Empty Fruit Bunch: Ethanol Production and Co-Fermentation with Cane Molasses

BioResources ◽  
2016 ◽  
Vol 11 (3) ◽  
Author(s):  
Trinset Weeraphan ◽  
Vasana Tolieng Tolieng ◽  
Vichien Kitpreechavanich ◽  
Somboon Tanasupawat ◽  
Ancharida Akaracharanya
Keyword(s):  
Ethanol Production ◽  
Sodium Hydroxide ◽  
Oil Palm ◽  
Steam Explosion ◽  
Empty Fruit Bunch ◽  
Cane Molasses

scholarly journals Mechanical Characterization of Epoxy Filled with Seed Shells as Reinforcement

2019 ◽  
Vol 8 (4) ◽  
pp. 6972-6977
Keyword(s):  
Mechanical Properties ◽  
Flexural Strength ◽  
Sodium Hydroxide ◽  
Natural Fiber ◽  
Fiber Composite ◽  
Flexural Modulus ◽  
Natural Fibers ◽  
Epoxy Composites ◽  
The Matrix ◽  
Sunflower Seed Shells

The use of natural fiber composite has been widely promoted in many industries such as construction, automotive and even aerospace. Natural fibers can be extracted from plants that are abundantly available in the form of waste such as sunflower seed shells (SSS) and groundnut shells (GNS). These fibers were chosen as the reinforcement in epoxy to form composites. The performance of composites was evaluated following the ASTM D3039 and ASTM D790 for tensile and flexural tests respectively. Eight types of composites were prepared using SSS and GNS fibers as reinforcement and epoxy as the matrix with the fiber content of 20wt %. The fibers were untreated and treated with Sodium Hydroxide (NaOH) at various concentrations (6%, 10%, 15%, and 20%) and soaking time (24, 48 and 72 hours). The treatment has successfully enhanced the mechanical properties of both composites, namely SSS/epoxy and GNS/epoxy composites. The SSS/epoxy composite has the best mechanical properties when the fibers were treated for 48 hours using 6% of NaOH that produced 22 MPa and 13 MPa of tensile and flexural strength respectively. Meanwhile, the treatment on groundnut shells with 10% sodium Hydroxide for 24 hours has increased the Flexural strength tremendously (53%), however no significant effect on the tensile strength. The same trend was also observed on the tensile and flexural modulus. The increase of 41% in flexural modulus after treatment with 10% NaOH for 24 hours was also the evidence of mechanical properties enhancement. The evidence of improved fiber and matrix bonding after fiber treatment was also observed using a scanning electron microscope (SEM). The SSS/epoxy composites performed better in tensile application, meanwhile the GNS/epoxy composites are good in flexural application.

scholarly journals Mechanical Properties of Benzoylation Treated Sugar Palm Fiber and Its Composite

2020 ◽  
Vol 8 (6) ◽  
pp. 4248-4252
Keyword(s):  
Tensile Strength ◽  
Sodium Hydroxide ◽  
Benzoyl Chloride ◽  
Fiber Strength ◽  
Fiber Composite ◽  
Alkaline Treatment ◽  
Single Fiber ◽  
Soaking Time ◽  
Palm Fiber ◽  
Sugar Palm Fiber

Studies on the effect of treated sugar palm fiber with alkaline treatment and benzoylation treatment on single fiber tensile strength and interfacial shear strength (IFSS) are shown in this paper. Also shown is the tensile strength of treated sugar palm fiber composite with variable fiber loading (10%, 20% and 30%). For alkaline treatment sodium hydroxide (NaOH) was used, while benzoyl chloride (C7H5ClO) was used in benzoylation treatment. Polymer matrix that was used in the process of making sugar palm fiber composite is epoxy resin with hardener. For the single fiber test and IFSS, the alkaline treatment was carried out using 1% concentration of sodium hydroxide for one hour soaking time while 5ml of benzoyl chloride was used to agitate with sodium hydroxide for benzoylation treatment with variable soaking time (10, 20 and 30 minutes). Treated sugar palm fiber showed higher single fiber strength and IFSS compared to untreated fiber due to the efficiency of both treatments which help rearrangement of fibrils along the tensile force direction. Tensile properties of sugar palm fiber composite show improvement in tensile stress and tensile modulus for treated sugar palm fiber composite while tensile strain show the opposite result. This is because the bonding strength between fiber and matrix increased by removing the outer layer together with impurities from the fiber during chemical treatment. Thus, with this treatment method, sugar palm fiber can be use as reinforcement material for composite and use them for commercial use such as for furniture and component inside vehicle.

scholarly journals Oxidation of Cellulose from Oil Palm Empty Fruit Bunch Using Hydrogen Peroxide in Alkaline Condition

2018 ◽  
Vol 8 (02) ◽  
pp. 51 ◽  
Author(s):  
Isroi Isroi ◽  
Adi Cifriadi
Keyword(s):  
Hydrogen Peroxide ◽  
Sodium Hydroxide ◽  
Sodium Hypochlorite ◽  
Oil Palm ◽  
Visual Analysis ◽  
Alkaline Condition ◽  
Cellulose Content ◽  
Empty Fruit Bunch ◽  
Cellulose Oxidation ◽  
Oxidation Effect

There are growing interest to use cellulose as renewable material in order to replace non-renewable polymeric materials. Alteration and chemical modifications of the cellulose by oxidation is needed to improve its properties and functionality. The aim of this study was to evaluate oxidation effect of the cellulose from oil palm empty fruit bunch (OPEFB) using hydrogen peroxide in alkaline condition. Cellulose has been isolated and purified by sodium hydroxide method followed by sodium hypochlorite bleaching. The oxidation effect of the cellulose by hydrogen peroxide was investigated by component analysis of the lignocelluloses, visual analysis, physical and chemical properties. Fourier transform infrared spectroscopy was employed to evaluate the changes of functional groups. Digesting of the OPEFB by sodium hydroxide at temperature 160oC for 4 hours reduced lignin content from 22.58% to 16.60%, increase cellulose and hemicelluloses content from 60.76% to 73.87% and 25.86% to 30.95%, respectively. Treatment of the OPEFB pulp using sodium hypochlorite removed all residual lignin. Cellulose content was increased up to 90.86%. Degree of polymerization of the oxidized cellulose was reduced from 1997 to 658. Carboxyl groups of celluloses was significantly increased and confirmed by titration analysis. OPEFB cellulose fiber was damage and broken, meanwhile crystallinity of the cellulose was reduced.Keywords: cellulose, oxidation, oil palm empty fruit bunch, carboxyl group, crystallinity, physical properties Oksidasi Selulosa dari Tandan Kosong Kelapa Sawit menggunakan Hidrogen Peroksida dalam Kondisi BasaAbstrakPerhatian untuk memanfaatkan selulosa sebagai polimer terbarukan untuk menggantikan polimer tidak terbarukan mengalami peningkatan. Perubahan dan modifikasi kimia selulosa melalui proses oksidasi diperlukan untuk meningkatkan sifat dan fungsi selulosa. Penelitian ini bertujuan untuk mempelajari pengaruh oksidasi selulosa dari tandan kosong kelapa sawit (TKKS) menggunakan hidrogen peroksida dalam suasana basa. Selulosa diisolasi dan dimurnikan dengan metode natrium hidroksida dan dilanjutkan dengan pemutihan natrium hipoklorit. Efek oksidasi selulosa oleh hidrogen peroksida dievaluasi menggunakan analisis komponen lignoselulosa, analisis visual, sifat fisik dan kimia. Analisis spektroskopi inframerah (FTIR) digunakan untuk mengevaluasi perubahan gugus fungsional selulosa. Pemasakan TKKS dengan natrium hidroksida pada suhu160oC selama 4 jam mengurangi kandungan lignin dari 22,58% menjadi 16,60%, meningkatkan kandungan selulosa dari 60,76% menjadi 73,87% dan hemiselulosa dari 25,86% menjadi 30,95%. Perlakuan pulp TKKS menggunakan natrium hipoklorit menghilangkan semua sisa lignin. Kandungan selulosa meningkat hingga 90,86%. Oksidasi selulosa dengan hidrogen peroksida menurunkan derajat polimerisasi selulosa dari 1997 menjadi 658. Gugus karboksil selulosa meningkat secara signifikan dan dikonfirmasi dengan analisis titrasi. Analisis visual menunjukkan kerusakan serabut selulosa, sesuai dengan pengurangan kristalinitas selulosa.Kata kunci: selulosa, oksidasi, tandan kosong kelapa sawit, gugus karboksil, kristalinitas, sifat fisik 

scholarly journals The effect of alkaline treatments soaking time on oil palm empty fruit bunch (OPEFB) fibre structure

2017 ◽  
Vol 908 ◽  
pp. 012033 ◽  
Author(s):  
M K Faizi ◽  
A B Shahriman ◽  
M S Abdul Majid ◽  
Z A Ahmad ◽  
B M T Shamsul ◽  
...  
Keyword(s):  
Oil Palm ◽  
Empty Fruit Bunch ◽  
Fibre Structure ◽  
Soaking Time

Effect of Fibre Size on the Tensile Properties of Oil Palm Empty Fruit Bunch Fibre Composites

2012 ◽  
Vol 576 ◽  
pp. 280-283 ◽  
Author(s):  
Noorrul Wahida Abdul Razak ◽  
Anizah Kalam
Keyword(s):  
Tensile Strength ◽  
Tensile Properties ◽  
Oil Palm ◽  
Matrix Material ◽  
Tensile Modulus ◽  
Empty Fruit Bunch ◽  
Fibre Size ◽  
Fibre Composites ◽  
The Matrix ◽  
Pp Composites

The principal aim of this project was to achieve a better understanding of the various parameters that contribute to the tensile properties. These parameters were manipulated in order to improve and produced PPnanoclay/ Polypropylene (PP) reinforced oil palm empty fruit bunch composite material (OPEFB). OPEFB fibre was treated with sodium hydroxide (NaOH) in order to improve the tensile properties of the composites. Thus, in this study the oil palm empty fruit bunch fibres were used as a filler and PPnanoclay/ PP composite as the matrix material. Tensile test was used to assess the effect on the tensile strength and tensile modulus of OPEFB/PPnanoclay/PP composites. Morphologies of the composites were examined using a scanning electron microscope (SEM). The average tensile properties obtained were tensile strength 22 MPa at 180 µm and Young’s modulus 2120 MPa at 355 µm treated.

scholarly journals BIODEGRADABILITY OF BIOPLASTIC IN NATURAL ENVIRONMENT

2019 ◽  
Vol 9 (2) ◽  
pp. 258-263
Author(s):  
Anggun Rahman Rahman ◽  
Khaswar Syamsu Syamsu ◽  
Isroi Isroi Isroi
Keyword(s):  
Sodium Hydroxide ◽  
Natural Environment ◽  
Oil Palm ◽  
Co2 Production ◽  
Empty Fruit Bunch ◽  
Biodegradation Rate ◽  
Empty Fruit Bunches ◽  
Top Soil ◽  
Biodegradation Process ◽  
Biodegradation Test

Biodegradation of the bioplastic composite based on cellulose from oil palm empty fruit bunches was investigated in this study. Microbes consortium from landfill soil collected from top soil were used as the inoculums for the biodegradation process. Biodegradation test of the bioplastic from oil palm empty fruit bunch samples compared with oxodegradation and conventional plastic samples were conducted in the glass jar. The biodegradation rate was evaluated from CO2 generated from the biodegradation process and absorbed by 0.1 N sodium hydroxide solutions. The generated CO2 was titrated with 0.1 N HCl and using phenolphthalein (PP) followed by methyl oranges indicator. The results showed that the highest CO2 production on landfill soil indicating the highest rate of biodegradation was found on bioplastic from oil palm empty fruit bunch followed by oxodegradable plastic and conventional plastic. The rate of biodegradation for bioplastic from oil palm empty fruit bunch, oxodegradable plastic and conventional plastic were 0.067mg CO2/day, 0.052 mg CO2/day and 0 mg CO2/day, respectively.

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