scholarly journals Effect of Deep Cryogenic Treatment on Microstructure and Properties of Sintered Fe–Co–Cu-Based Diamond Composites

2019 ◽  
Vol 9 (16) ◽  
pp. 3353
Author(s):  
Siqi Li ◽  
Wenhao Dai ◽  
Zhe Han ◽  
Xinzhe Zhao ◽  
Baochang Liu

Metal-matrix-impregnated diamond composites are used for fabricating many kinds of diamond tools. In the efforts to satisfy the increasing engineering requirements, researchers have brought more attention to find novel methods of enhancing the performance of impregnated diamond composites. In this study, deep cryogenic treatment was applied to Fe–Co–Cu-based diamond composites to improve their performance. Relative density, hardness, bending strength, and grinding ratio of matrix and diamond composite samples were measured by a series of tests. Meanwhile, the fracture morphologies of all samples after the bending strength test were observed and analyzed by scanning electron microscope. The results showed that the hardness and bending strength of matrix increased slightly after deep cryogenic treatment. The grinding ratio of impregnated diamond composites exhibited a great increase by 32.9% as a result of deep cryogenic treatment. The strengthening mechanism was analyzed in detail. The Fe–Co–Cu-based impregnated composites subjected to deep cryogenic treatment for 1 h exhibited the best overall performance.

2018 ◽  
Vol 8 (9) ◽  
pp. 1501 ◽  
Author(s):  
Siqi Li ◽  
Zhe Han ◽  
Qingnan Meng ◽  
Xinzhe Zhao ◽  
Xin Cao ◽  
...  

Metal matrix-impregnated diamond composites are widely used for fabricating diamond tools. In order to meet the actual engineering challenges, researchers have made many efforts to seek effective methods to enhance the performance of conventional metal matrices. In this work, tungsten carbide (WC) nanoparticles were introduced into WC-Bronze-Ni-Mn matrix with and without diamond grits for improving the performance of conventional impregnated diamond composites. The influence of WC nanoparticles on the microstructure, densification, hardness, bending strength and wear resistance of matrix and diamond composites were investigated. The results showed that the bending strength of matrix increased up to approximately 20% upon nano-WC addition, while densification and hardness fluctuate slightly. The grinding ratio of diamond composites increased significantly by about 100% due to nano-WC addition. The strengthening mechanism was proposed according to experimental results. The diamond composites with 2.8 wt% nano-WC addition exhibited the best overall properties, thus having potential to apply to further diamond tools.


2021 ◽  
Vol 548 ◽  
pp. 149257
Author(s):  
Patricia Jovičević-Klug ◽  
Monika Jenko ◽  
Matic Jovičević-Klug ◽  
Barbara Šetina Batič ◽  
Janez Kovač ◽  
...  

Author(s):  
Menderes Kam

This study investigated the effects of Deep Cryogenic Treatment (DCT) on machinability, hardness, and microstructure in dry turning process of AISI 4140 (48-51 HRc) tempered steels with ceramic cutting tools on the surface roughness (Ra). DCT process of steels has shown significant improvement in their mechanical properties. In this context, experiments were made with Taguchi L16 method and optimum values were determined. Three different values for each control factors as: different heat treated samples, cutting speeds (160, 200, 240, 280 m/min), feed rates (0.08, 0.12, 0.16, 0.20 mm/rev) were selected. As a result, the lowest Ra value was found to be 0.159 µm for the DCTT36 sample at a cutting speed of 240 m/min, a feed rate of 0.08 mm/rev. The optimum Ra value was the lowest for the DCTT36 sample compared to the other samples as 0.206 µm. The hardness values of the micro and macro were highest for the DCTT36 sample. Microstructural point of view Scanning Electron Microscopy (SEM) point of view, the DCCT36 sample showed that best results owing to its homogeneity. It was concluded that lower Ra values can be obtained with ceramic cutting tool in dry turning experiments according to the studies in the literature review. It is thought to be preferred as an alternative to cylindrical grinding process due to lower cost.


Metals ◽  
2020 ◽  
Vol 11 (1) ◽  
pp. 14
Author(s):  
Jure Voglar ◽  
Živa Novak ◽  
Patricia Jovičević-Klug ◽  
Bojan Podgornik ◽  
Tadeja Kosec

The aim of the study was to evaluate the corrosion properties of three different grades of high-speed steel following a heat treatment procedure involving deep cryogenic treatment after quenching and to investigate how these properties are connected to the microstructure and hardness of the material. The hardness of steels was measured, and microstructural properties were determined through observation of the metallographically prepared steels using scanning electron microscopy. These studies were complemented corrosion evaluation by the use of corrosion potential measurement and linear polarization measurement of steels in a sodium tetraborate buffer at pH 10. The results showed that the deep cryogenic procedure of high-speed steel changed the microstructure and consequently affected the hardness of the investigated steels to different extents, depending on their chemical composition. Corrosion studies have confirmed that some high-speed steels have improved corrosion properties after deep cryogenic treatment. The most important improvement in corrosion resistance was observed for deep cryogenically treated high-speed steel EN 1.3395 (M3:2) by 31% when hardened to high hardness values and by 116% under lower hardness conditions. The test procedure for differentiating corrosion properties of differently heat-treated tool steels was established alongside the investigation.


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