scholarly journals Microstructure and Rutherford Backscattering Spectrometry of Hard/Lubricant Mo-Ti-Al-N Multilayered Coatings Prepared by Multi-Arc Ion Plating at Low Substrate Rotation

Coatings ◽  
2020 ◽  
Vol 10 (2) ◽  
pp. 101
Author(s):  
Zesong Wang ◽  
Canxin Tian ◽  
Alexander Tolstogouzov ◽  
Feng Liang ◽  
Changwei Zou ◽  
...  

To develop the hard and self-lubricating coatings applied for the industrial dry-cutting and die-casting machining tool fields, a series of MoTiAlN/MoN/Mo multilayered coatings were deposited on Si substrates under low substrate rotation by cathodic multi-arc ion plating. XRD, SEM, TEM, RBS, nanoindentation, and tribology tester were used to monitor the phase structure, morphology, component, nanohardness, and friction coefficient of the coatings. It was found that the coatings deposited at various substrate rotations comprised paramount cubic B1 structure TiAlN and Mo2N phases. The micrographs confirmed that the mean modulation period and total physical thickness of multilayered TiAlN/Mo2N coatings with a sharp interface fabricated at 2 revolutions per minute (rpm) were 26 nm and 1.15 μm. The mean nanohardness and friction coefficient were ca. 30 GPa and 0.4, respectively. RBS results along with the SIMNRA code allowed to estimate the total atomic concentrations and the physical thickness of individual sublayer as well as the modulation period of multilayered coatings, which demonstrated an efficiency of this approach for characterization of nano-multilayered structures.

2006 ◽  
Vol 118 ◽  
pp. 311-316 ◽  
Author(s):  
Eun Young Choi ◽  
Chul Sik Jang ◽  
Myung Chang Kang ◽  
Kwang Ho Kim

Ternary Ti-Cx-N1-x coatings were deposited on stainless steel substrates by arc ion plating (AIP) technique using Ti target at the temperature of 300 with a negative substrate bias voltage of -25 V. The carbon content in Ti-Cx-N1-x coatings linearly increased with increasing CH4/(CH4+N2) gas flow ratio at a constant arc current of 60 A. The microstructure and mechanical properties such as micro-hardness and average friction coefficient of Ti-Cx-N1-x coatings were investigated as a function of carbon content. As the carbon content in Ti-Cx-N1-x coatings increased, the microhardness values of Ti-Cx-N1-x coatings increased from 20 GPa for TiN coatings and reached the maximum value of approximately 32 GPa at x=0.52 in Ti-Cx-N1-x coatings. The variation of microhardness of Ti-Cx-N1-x coatings had a relationship with the change of residual stress. The average friction coefficient of Ti-Cx-N1-x coatings largely decreased with increasing carbon content.


2014 ◽  
Vol 887-888 ◽  
pp. 1096-1100 ◽  
Author(s):  
Guo Dong Sun ◽  
Deng Liang Yi ◽  
Chang Hua Liu

TiN and TiAlN films have been coated on the surface of tool materials by various methods for the life-time extension of tool. In this work, for the improvement of hardness and adhesion of coating to SKD61 substrate, radical nitriding (RN) of substrate was carried out at 450°C for 5 hours in ammonia gas pressure of 2.7×103 Pa. The results showed that TiN and TiAlN coatings were distributed uniformly on the SKD 61 substrate. And the film thickness was up to 4 μm, which showed so high deposition efficiency (~ 66.7 nm/min) of arc ion plating at this typical process condition. For both coatings, the TiN phases could be detected and the (111) was dominant crystallite grown orientation. The AlN crystallite structure could be detected as expected in TiAlN film. The critical load of TiN film (22.36 N) was slightly smaller than that of TiAlN film (23.88 N). With increasing the load during scratch test, the friction coefficient of TiN film rose quickly, but friction coefficient of TiAlN had a little change, even decreased slightly.


2002 ◽  
Vol 17 (12) ◽  
pp. 3133-3138 ◽  
Author(s):  
Fei Zhou ◽  
Chang-Min Suh ◽  
Seock-Sam Kim ◽  
Ri-Ichi Murakami

Dry sliding wear and friction tests of CrN coating on two types of aluminum alloy substrates, 6061 Al and 7075 Al, deposited by arc ion plating were performed with a ball-on-disk tribometer. The effects of normal load and the mechanical properties of the substrate on the friction coefficient and wear resistance of CrN coating were investigated. The worn surfaces were observed by scanning electron microscopy. The results show that surface microhardness of CrN-coated 7075 Al is higher than that of CrN-coated 6061 Al. With an increase in normal load, wear volume increases, while the friction coefficient decreases. The friction coefficient of CrN-coated 6061 Al is higher than that of CrN-coated 7075 Al, while the wear resistance of CrN-coated 6061 Al is lower than that of the CrN-coated 7075 Al. This indicates that the substrate mechanical properties have strong influence on the friction coefficient and wear of CrN coating. The main wear mechanism was fragments of CrN coating, caused by apparent plastic deformation of substrate during wear tests.


2008 ◽  
Vol 368-372 ◽  
pp. 1307-1309 ◽  
Author(s):  
Li Yun Zheng ◽  
Li Xin Zhao ◽  
Jing Jun Zhang

Ti(C,N)-based cermets were coated with a TiN/TiAlN coating using ion plating technology. The sliding wear test was performed for the coated cermets and the microstructure, composition and surface roughness of the coated cermets under different velocities and loads were characterized. The results showed that the friction coefficients of the coated cermets were lower than that of the neat cermets. Under the same load, the adhesion phenomenon of the counterpart materials on the specimens was improved and the mean friction coefficient increased with increasing sliding speed. Under the same sliding velocity, the average friction coefficient of the coated cermets was lower under higher load. The wear mechanisms were mainly adhesive wear and abrasive wear.


Vacuum ◽  
2016 ◽  
Vol 126 ◽  
pp. 34-40 ◽  
Author(s):  
S.Y. Zhou ◽  
V.O. Pelenovich ◽  
B. Han ◽  
M.I. Yousaf ◽  
S.J. Yan ◽  
...  

Vacuum ◽  
2021 ◽  
pp. 110152
Author(s):  
Lijun Xian ◽  
Haibo Zhao ◽  
Guang Xian ◽  
Chencheng Wang ◽  
Hong He

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