scholarly journals Simultaneous Distillation–Extraction of Essential Oils from Rosmarinus officinalis L.

Cosmetics ◽  
2021 ◽  
Vol 8 (4) ◽  
pp. 117
Author(s):  
Bárbara Silva Ribeiro ◽  
Maria de Fátima Ferreira ◽  
José Luís Moreira ◽  
Lúcia Santos

The present study describes a procedure to isolate essential oils from Rosmarinus officinalis L. using simultaneous distillation–extraction (SDE). Rosmarinus officinalis L. can be used for medicinal purposes, as well in the cooking and cosmetics industries. SDE technique extraction combines a steam distillation combined with a continuous extraction using a solvent or a co-solvent mixture, providing faster extractions with low extraction solvent volumes. The effect of the solvent nature and the extraction time on the simultaneous distillation–extraction efficiency was evaluated. The best performance was achieved using pentane as a solvent for 1 h of extraction. The essential oils obtained by simultaneous distillation–extraction extracts were analyzed by gas chromatography with flame ionization detection (GC-FID). Extraction efficiencies ranged from 40 to 70% for the majority of the compounds tested, and the precision (measured by the relative standard deviation) varied between 6 and 35%. Among the compounds analyzed the most abundant in the Rosmarinus officinalis L. sample were 1,8-cineole, (-) –borneol, α-pinene, (S)-(-)- α–terpineol, (-)-bornyl acetate, linalool, and 2,2,6-trimethylcyclohexanone. The SDE method proved to be a suitable option for obtaining extracts free from cuticular waxes or chlorophylls.

Author(s):  
SARAH ALI HAMID

Objective: The purpose of this study was to identify and characterize chemical constituents of Rosmarinus officinalis L. essential oils from Diyala Province, an eastern side of Iraq. Methods: Following hydrodistillation extraction of the leaves, gas chromatography–mass spectrometry (MS) was performed. Eighteen peaks were identified and compared to known compounds and MS patterns. Results: The two major components identified were eucalyptol (1,8-cineole) and L-camphor, and they represent 59% and 29%, respectively. In addition, α-terpineol, bornyl acetate, borneol, linalool, and β-terpineol were detected in 3.75, 2.83, 1.96, 1.22, and 0.65%, respectively. Conclusion: The present study showed that rosemary essential oils from Diyala Province of Iraq consisted mostly of oxygenated monoterpenes (>96%) and hydrocarbon monoterpenes are less than 1%. The latter suggest that hydrocarbon monoterpenes may undergo transformation due to atmospheric as well as microbiological metabolism which more studies are needed to confirm such suggestion.


2019 ◽  
Vol 14 (7) ◽  
pp. 1934578X1986400 ◽  
Author(s):  
Sara Melito ◽  
Giacomo Luigi Petretto ◽  
Sarah Chahine ◽  
Giorgio Pintore ◽  
Mario Chessa

Rosmarinus officinalis L. is an aromatic plant belonging to the Lamiaceae family widely distributed in the Mediterranean area. The interest on this species is related to the multiple uses of the plant as a food ingredient, in the pharmaceutical and cosmetic industries. The chemical composition of essential oil (EO) from 5 accessions of R. officinalis L., collected monthly through a full year in Sardinia, has been studied by gas chromatography (GC) and GC-mass spectrometry technique. The EO ranged from 0.29% to 0.89%. The qualitative determinations revealed the presence of 27 compounds belonging to 6 chemical groups (hydrocarbon monoterpene, alcohols, aldehydes, ketones, esters, hydrocarbon sesquiterpene). Overall the GC-flame ionization detector analysis showed the presence of 7 major compounds: α-pinene (26%-28%), camphene (5%-8%), 1,8-cineole (15%-25%), borneol (5%-11%), camphor (3%-12%), verbenone (6%-15%), and bornyl acetate (4%-7%). Chromatographic data were also subjected to a chemometric approach that evidenced discrimination of the samples according to the site of collection.


2011 ◽  
Vol 44 (5) ◽  
pp. 1541-1548 ◽  
Author(s):  
Geíza Alves de Azeredo ◽  
Tânia Lúcia Montenegro Stamford ◽  
Pollyana Campos Nunes ◽  
Nelson Justino Gomes Neto ◽  
Maria Elieidy Gomes de Oliveira ◽  
...  

2009 ◽  
Vol 4 (12) ◽  
pp. 1934578X0900401 ◽  
Author(s):  
Giorgio Pintore ◽  
Mauro Marchetti ◽  
Mario Chessa ◽  
Barbara Sechi ◽  
Nadia Scanu ◽  
...  

Rosmarinus officinalis essential oil was separated into its hydrocarbon and oxygenated fractions. The major compounds in the hydrocarbon fraction were α-pinene (44.2%), camphene (24.5%), and limonene (11.7%), while in the oxygenated fraction they were 1,8-cineole (37.6%), camphor (16.5%), and bornyl acetate (21.4%). The hydrocarbon fraction was submitted to a hydroformylation process and the antioxidant activity of the product was screened by the DPPH and β-carotene/linoleic acid tests. The hydroformylated fraction maintained the antioxidant activity of the whole oil. The MIC (minimal inhibitory concentration) and the MBC (minimal bactericidal concentration) of the essential oil, hydrocarbon, oxygenated and hydroformylated fractions were also tested on several microorganisms. Aeromonas sobria and Candida strains were the most susceptible micro-organisms. The hydroformylated fraction exhibited a MBC against Candida strains resistant to the other fractions.


2014 ◽  
Vol 47 (2) ◽  
pp. 451-457 ◽  
Author(s):  
Samir Smeti ◽  
Hadhami Hajji ◽  
Kahena Bouzid ◽  
Jaouida Abdelmoula ◽  
Fernando Muñoz ◽  
...  

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