scholarly journals In-Situ XRD Study of Phase Transformation Kinetics in a Co-Cr-W-Alloy Manufactured by Laser Powder-Bed Fusion

Crystals ◽  
2021 ◽  
Vol 11 (2) ◽  
pp. 176
Author(s):  
Patrick Hegele ◽  
Jonas von Kobylinski ◽  
Leonhard Hitzler ◽  
Christian Krempaszky ◽  
Ewald Werner
Keyword(s):  
Residual Stresses ◽  
Sample Surface ◽  
Treatment Temperature ◽  
Ex Situ ◽  
Patient Specific ◽  
Powder Bed Fusion ◽  
Laser Powder Bed Fusion ◽  
Corrosion Properties ◽  
Powder Bed

The additive manufacturing process of laser powder-bed fusion (L-PBF) is an increasingly popular approach for patient-specific production of dental frameworks made from Co-Cr alloys. Macroscopically, frameworks produced in this way exhibit high anisotropy especially in Young’s modulus, and are missing standardized requirements. Microscopically, pronounced texture and high residual stresses are characteristic. To reduce resulting detrimental effects, the as-built (AB) parts are heat treated. Dependent on the treatment temperature, effects like the transformation of the γ-phase matrix in the AB condition to ϵ-phase, precipitation, stress relief, and grain growth were observed. While the existence of these processes was established in the past, little is known about their kinetics. To fill this gap, these effects were studied with in-situ X-ray diffraction (XRD) methods in isothermal heat treatments (HTs) at four different sample surface temperatures TS reaching from 650∘C to 900∘C. Furthermore, room temperature ex situ XRD and SEM/EDS measurements completed the analysis. An evaluation of the datasets, with single peak fitting and QXRD methods, yielded the following results. In the HTs below a certain threshold, a γ-to-ϵ transformation was observed in the sample bulk and close to the sample surface. In the latter case, evidence for a partially strain-induced transformation related to oxide formation was present. Above this threshold and possibly slightly below, σ- and Laves-phase precipitated. Additionally, peak profile evolutions hinted at a drop of inter- and intragranular stresses within the first 30 to 60 min. Therefore, an HT of about 30 to 60 min slightly above the threshold is proposed as optimal for reducing residual stresses while retaining a predominantly single-phased microstructure, possibly superior in corrosion properties and likewise in bio-compatibility.

scholarly journals In situ microstructure analysis of Inconel 625 during laser powder bed fusion

2021 ◽  
Author(s):  
Felix Schmeiser ◽  
Erwin Krohmer ◽  
Christian Wagner ◽  
Norbert Schell ◽  
Eckart Uhlmann ◽  
...  
Keyword(s):  
Laser Power ◽  
Scanning Speed ◽  
High Energy ◽  
Mechanical Anisotropy ◽  
Ex Situ ◽  
Inconel 625 ◽  
Powder Bed Fusion ◽  
Laser Powder Bed Fusion ◽  
Powder Bed

AbstractLaser powder bed fusion is an additive manufacturing process that employs highly focused laser radiation for selective melting of a metal powder bed. This process entails a complex heat flow and thermal management that results in characteristic, often highly textured microstructures, which lead to mechanical anisotropy. In this study, high-energy X-ray diffraction experiments were carried out to illuminate the formation and evolution of microstructural features during LPBF. The nickel-base alloy Inconel 625 was used for in situ experiments using a custom LPBF system designed for these investigations. The diffraction patterns yielded results regarding texture, lattice defects, recrystallization, and chemical segregation. A combination of high laser power and scanning speed results in a strong preferred crystallographic orientation, while low laser power and scanning speed showed no clear texture. The observation of a constant gauge volume revealed solid-state texture changes without remelting. They were related to in situ recrystallization processes caused by the repeated laser scanning. After recrystallization, the formation and growth of segregations were deduced from an increasing diffraction peak asymmetry and confirmed by ex situ scanning transmission electron microscopy. Graphical Abstract

scholarly journals Linking In Situ Melt Pool Monitoring to Melt Pool Size Distributions and Internal Flaws in Laser Powder Bed Fusion

Metals ◽  
2021 ◽  
Vol 11 (11) ◽  
pp. 1856
Author(s):  
Claudia Schwerz ◽  
Lars Nyborg
Keyword(s):  
Near Infrared ◽  
In Situ Monitoring ◽  
Ex Situ ◽  
Process Conditions ◽  
Powder Bed Fusion ◽  
Laser Powder Bed Fusion ◽  
Powder Bed ◽  
Melt Pool ◽  
Melt Pool Size

In situ monitoring of the melt pools in laser powder bed fusion (LPBF) has enabled the elucidation of process phenomena. There has been an increasing interest in also using melt pool monitoring to identify process anomalies and control the quality of the manufactured parts. However, a better understanding of the variability of melt pools and the relation to the incidence of internal flaws are necessary to achieve this goal. This study aims to link distributions of melt pool dimensions to internal flaws and signal characteristics obtained from melt pool monitoring. A process mapping approach is employed in the manufacturing of Hastelloy X, comprising a vast portion of the process space. Ex situ measurements of melt pool dimensions and analysis of internal flaws are correlated to the signal obtained through in situ melt pool monitoring in the visible and near-infrared spectra. It is found that the variability in melt pool dimensions is related to the presence of internal flaws, but scatter in melt pool dimensions is not detectable by the monitoring system employed in this study. The signal intensities are proportional to melt pool dimensions, and the signal is increasingly dynamic following process conditions that increase the generation of spatter.

scholarly journals Detecting keyhole pore defects and monitoring process signatures during laser powder bed fusion: A correlation between in situ pyrometry and ex situ X-ray radiography

2020 ◽  
Vol 35 ◽  
pp. 101336 ◽  
Author(s):  
Jean-Baptiste Forien ◽  
Nicholas P. Calta ◽  
Philip J. DePond ◽  
Gabe M. Guss ◽  
Tien T. Roehling ◽  
...  
Keyword(s):  
Ex Situ ◽  
Powder Bed Fusion ◽  
Laser Powder Bed Fusion ◽  
Powder Bed ◽  
X Ray ◽  
Monitoring Process

scholarly journals In situ radiographic and ex situ tomographic analysis of pore interactions during multilayer builds in laser powder bed fusion

2020 ◽  
Vol 36 ◽  
pp. 101512 ◽  
Author(s):  
Lorna Sinclair ◽  
Chu Lun Alex Leung ◽  
Sebastian Marussi ◽  
Samuel J. Clark ◽  
Yunhui Chen ◽  
...  
Keyword(s):  
Ex Situ ◽  
Powder Bed Fusion ◽  
Laser Powder Bed Fusion ◽  
Powder Bed ◽  
Tomographic Analysis

scholarly journals Comparison of Phase Characteristics and Residual Stresses in Ti-6Al-4V Alloy Manufactured by Laser Powder Bed Fusion (L-PBF) and Electron Beam Powder Bed Fusion (EB-PBF) Techniques

Crystals ◽  
2021 ◽  
Vol 11 (7) ◽  
pp. 796
Author(s):  
Aya Takase ◽  
Takuya Ishimoto ◽  
Naotaka Morita ◽  
Naoko Ikeo ◽  
Takayoshi Nakano
Keyword(s):  
Electron Beam ◽  
Residual Stresses ◽  
Cooling Rate ◽  
Process Parameters ◽  
Phase Evolution ◽  
Powder Bed Fusion ◽  
Laser Powder Bed Fusion ◽  
Solidification Temperature ◽  
Powder Bed ◽  
Β Phase

Ti-6Al-4V alloy fabricated by laser powder bed fusion (L-PBF) and electron beam powder bed fusion (EB-PBF) techniques have been studied for applications ranging from medicine to aviation. The fabrication technique is often selected based on the part size and fabrication speed, while less attention is paid to the differences in the physicochemical properties. Especially, the relationship between the evolution of α, α’, and β phases in as-grown parts and the fabrication techniques is unclear. This work systematically and quantitatively investigates how L-PBF and EB-PBF and their process parameters affect the phase evolution of Ti-6Al-4V and residual stresses in the final parts. This is the first report demonstrating the correlations among measured parameters, indicating the lattice strain reduces, and c/a increases, shifting from an α’ to α+β or α structure as the crystallite size of the α or α’ phase increases. The experimental results combined with heat-transfer simulation indicate the cooling rate near the β transus temperature dictates the resulting phase characteristics, whereas the residual stress depends on the cooling rate immediately below the solidification temperature. This study provides new insights into the previously unknown differences in the α, α’, and β phase evolution between L-PBF and EB-PBF and their process parameters.

scholarly journals Effect of Build Orientation on the Microstructure, Mechanical and Corrosion Properties of a Biodegradable High Manganese Steel Processed by Laser Powder Bed Fusion

Metals ◽  
2021 ◽  
Vol 11 (6) ◽  
pp. 944
Author(s):  
Martin Otto ◽  
Stefan Pilz ◽  
Annett Gebert ◽  
Uta Kühn ◽  
Julia Hufenbach
Keyword(s):  
Electron Backscatter Diffraction ◽  
Longitudinal Axis ◽  
Manganese Steel ◽  
Compressive Yield Strength ◽  
Powder Bed Fusion ◽  
Compression Tests ◽  
Laser Powder Bed Fusion ◽  
Corrosion Properties ◽  
Powder Bed ◽  
Manufacturing Technologies

In the last decade, additive manufacturing technologies like laser powder bed fusion (LPBF) have emerged strongly. However, the process characteristics involving layer-wise build-up of the part and the occurring high, directional thermal gradient result in significant changes of the microstructure and the related properties compared to traditionally fabricated materials. This study presents the influence of the build direction (BD) on the microstructure and resulting properties of a novel austenitic Fe‑30Mn‑1C‑0.02S alloy processed via LPBF. The fabricated samples display a {011} texture in BD which was detected by electron backscatter diffraction. Furthermore, isolated binding defects could be observed between the layers. Quasi-static tensile and compression tests displayed that the yield, ultimate tensile as well as the compressive yield strength are significantly higher for samples which were built with their longitudinal axis perpendicular to BD compared to their parallel counterparts. This was predominantly ascribed to the less severe effects of the sharp-edged binding defects loaded perpendicular to BD. Additionally, a change of the Young’s modulus in dependence of BD could be demonstrated, which is explained by the respective texture. Potentiodynamic polarization tests conducted in a simulated body fluid revealed only slight differences of the corrosion properties in dependence of the build design.

scholarly journals Corrosion Fatigue Characteristics of 316L Stainless Steel Fabricated by Laser Powder Bed Fusion

Metals ◽  
2021 ◽  
Vol 11 (7) ◽  
pp. 1046
Author(s):  
Balachander Gnanasekaran ◽  
Jie Song ◽  
Vijay Vasudevan ◽  
Yao Fu
Keyword(s):  
Fatigue Crack ◽  
Crack Propagation ◽  
Fatigue Crack Propagation ◽  
Corrosion Fatigue ◽  
Fatigue Properties ◽  
Powder Bed Fusion ◽  
Laser Powder Bed Fusion ◽  
Corrosion Properties ◽  
Powder Bed ◽  
Fatigue Characteristics

Laser powder bed fusion (LPBF) has been increasingly used in the fabrication of dense metallic structures. However, the corrosion related properties of LPBF alloys, in particular environment-assisted cracking, such as corrosion fatigue properties, are not well understood. In this study, the corrosion and corrosion fatigue characteristics of LPBF 316L stainless steels (SS) in 3.5 wt.% NaCl solution have been investigated using an electrochemical method, high cycle fatigue, and fatigue crack propagation testing. The LPBF 316L SSs demonstrated significantly improved corrosion properties compared to conventionally manufactured 316L, as reflected by the increased pitting and repassivation potentials, as well as retarded crack initiation. However, the printing parameters did not strongly affect the pitting potentials. LPBF samples also demonstrated enhanced capabilities of repassivation during the fatigue crack propagation. The unique microstructural features introduced during the printing process are discussed. The improved corrosion and corrosion fatigue properties are attributed to the presence of columnar/cellular subgrains formed by dislocation networks that serve as high diffusion paths to transport anti-corrosion elements.

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