scholarly journals Ultrasound Assisted Extraction Approach to Test the Effect of Elastic Rubber Nettings on the N-Nitrosamines Content of Ham Meat Samples

Foods ◽  
2021 ◽  
Vol 10 (11) ◽  
pp. 2564
Author(s):  
Claudia Giménez-Campillo ◽  
Marta Pastor-Belda ◽  
Natalia Campillo ◽  
Juan de Dios Hernández ◽  
Isidro Guillén ◽  
...  
Keyword(s):  
Meat Products ◽  
Gas Chromatography Mass Spectrometry ◽  
Sample Treatment ◽  
Ultrasound Assisted Extraction ◽  
Assisted Extraction ◽  
Cooked Ham ◽  
Ultrasonic Assisted ◽  
Elastic Rubber ◽  
Dispersive Liquid Liquid Microextraction ◽  
Meat Samples

Nitrosamines (NAs), which are catalogued as carcinogenic compounds, may be present in meat products due to the conversion of nitrites and as result of migration from elastic rubber nettings used. A method based on ultrasonic assisted extraction coupled with dispersive liquid–liquid microextraction as sample treatment and gas chromatography-mass spectrometry as separation and detection technique was proposed for the determination of twelve NAs in cooked ham samples. The method was validated by evaluating linearity (0.5–1000 ng g−1), matrix effect, sensitivity (detection limits were between 0.15 and 1.4 ng g−1) and precision, which was below 12%. Five NAs were found in the samples with levels ranging from not quantifiable to 40 ng g−1. The effect of the elastic rubber nettings on the nitrosamine content of meat was evaluated by comparing the levels found in products made with several plastics or thread in the presence of additives.

Ultrasound-assisted extraction and dispersive liquid–liquid microextraction coupled with gas chromatography-mass spectrometry for the sensitive determination of essential oil components in lavender

2019 ◽  
Vol 11 (11) ◽  
pp. 1541-1550 ◽  
Author(s):  
Ping Chen ◽  
Bing Liu ◽  
Xin Liu ◽  
Jihong Fu
Keyword(s):  
Essential Oil ◽  
Gas Chromatography Mass Spectrometry ◽  
Ultrasound Assisted Extraction ◽  
Assisted Extraction ◽  
Sensitive Determination ◽  
Ultrasound Assisted ◽  
Oil Components ◽  
Dispersive Liquid Liquid Microextraction ◽  
Liquid Microextraction

Ultrasound-assisted extraction and dispersive liquid–liquid microextraction coupled with GC-MS for the sensitive determination of essential oil components in lavender.

Differentiation of two types of pu-erh teas by using an electronic nose and ultrasound-assisted extraction-dispersive liquid–liquid microextraction-gas chromatography-mass spectrometry

2016 ◽  
Vol 8 (3) ◽  
pp. 593-604 ◽  
Author(s):  
Jing Ye ◽  
Wenguang Wang ◽  
Chitang Ho ◽  
Jun Li ◽  
Xiaoyu Guo ◽  
...  
Keyword(s):  
Mass Spectrometry ◽  
Gas Chromatography ◽  
Sensory Evaluation ◽  
Electronic Nose ◽  
Gas Chromatography Mass Spectrometry ◽  
Ultrasound Assisted Extraction ◽  
Assisted Extraction ◽  
Ultrasound Assisted ◽  
Dispersive Liquid Liquid Microextraction ◽  
Liquid Microextraction

It is a challenging task to discriminate raw pu-erh tea, notably aged raw tea, from ripened pu-erh tea, both of which are the two primary types of pu-erh teas, only based on the taster's sensory evaluation.

scholarly journals Ultrasonic-Assisted Extraction and Natural Deep Eutectic Solvents Combination: A Green Strategy to Improve the Recovery of Phenolic Compounds from Lavandula pedunculata subsp. lusitanica (Chaytor) Franco

Antioxidants ◽  
2021 ◽  
Vol 10 (4) ◽  
pp. 582
Author(s):  
Inês Mansinhos ◽  
Sandra Gonçalves ◽  
Raquel Rodríguez-Solana ◽  
José Luis Ordóñez-Díaz ◽  
José Manuel Moreno-Rojas ◽  
...  
Keyword(s):  
Antioxidant Activity ◽  
Phenolic Compounds ◽  
Deep Eutectic Solvents ◽  
Industrial Applications ◽  
Total Phenolic ◽  
Ultrasound Assisted Extraction ◽  
Phenolic Contents ◽  
Assisted Extraction ◽  
Natural Deep Eutectic Solvents ◽  
Ultrasonic Assisted

The present study aimed at evaluating the effectiveness of different natural deep eutectic solvents (NADES) on the extraction of phenolic compounds from Lavandula pedunculata subsp. lusitanica (Chaytor) Franco, on the antioxidant activity, and acetylcholinesterase (AChE), butyrylcholinesterase (BChE) and tyrosinase (Tyr) inhibitory capacities. Ten different NADES were used in this research and compared with conventional solvents. Ultrasound-assisted extraction (UAE) for 60 min proved to be the best extraction condition, and proline:lactic acid (1:1) and choline chloride:urea (1:2) extracts showed the highest total phenolic contents (56.00 ± 0.77 mgGAE/gdw) and antioxidant activity [64.35 ± 1.74 mgTE/gdw and 72.13 ± 0.97 mgTE/gdw in 2.2-diphenyl-1-picrylhydrazyl (DPPH) and 2.2′-azino-bis(3-ethylbenzothiazoline-6-sulfonic acid) (ABTS) methods, respectively]. These extracts also exhibited enzymes inhibitory capacity particularly against Tyr and AChE. Even so, organic acid-based NADES showed to be the best extractants producing extracts with considerable ability to inhibit enzymes. Twenty-four phenolic compounds were identified by HPLC-HRMS, being rosmarinic acid, ferulic acid and salvianolic acid B the major compounds. The results confirmed that the combination of UAE and NADES provide an excellent alternative to organic solvents for sustainable and green extraction, and have huge potential for use in industrial applications involving the extraction of bioactive compounds from plants.

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