scholarly journals Facile Synthesis and Characterization of Palm CNF-ZnO Nanocomposites with Antibacterial and Reinforcing Properties

2021 ◽  
Vol 22 (11) ◽  
pp. 5781
Author(s):  
Janarthanan Supramaniam ◽  
Darren Yi Sern Low ◽  
See Kiat Wong ◽  
Loh Teng Hern Tan ◽  
Bey Fen Leo ◽  
...  
Keyword(s):  
Plant Biomass ◽  
Cellulose Nanofibers ◽  
High Strength ◽  
Salmonella Typhi ◽  
Particle Sizes ◽  
Mechanical Reinforcement ◽  
Uniform Size ◽  
Preparation Methods ◽  
Potential Applications

Cellulose nanofibers (CNF) isolated from plant biomass have attracted considerable interests in polymer engineering. The limitations associated with CNF-based nanocomposites are often linked to the time-consuming preparation methods and lack of desired surface functionalities. Herein, we demonstrate the feasibility of preparing a multifunctional CNF-zinc oxide (CNF-ZnO) nanocomposite with dual antibacterial and reinforcing properties via a facile and efficient ultrasound route. We characterized and examined the antibacterial and mechanical reinforcement performances of our ultrasonically induced nanocomposite. Based on our electron microscopy analyses, the ZnO deposited onto the nanofibrous network had a flake-like morphology with particle sizes ranging between 21 to 34 nm. pH levels between 8–10 led to the formation of ultrafine ZnO particles with a uniform size distribution. The resultant CNF-ZnO composite showed improved thermal stability compared to pure CNF. The composite showed potent inhibitory activities against Gram-positive (methicillin-resistant Staphylococcus aureus (MRSA)) and Gram-negative Salmonella typhi (S. typhi) bacteria. A CNF-ZnO-reinforced natural rubber (NR/CNF-ZnO) composite film, which was produced via latex mixing and casting methods, exhibited up to 42% improvement in tensile strength compared with the neat NR. The findings of this study suggest that ultrasonically-synthesized palm CNF-ZnO nanocomposites could find potential applications in the biomedical field and in the development of high strength rubber composites.

scholarly journals Microstructural and Mechanical Characterization of a Nanostructured Bainitic Cast Steel

Metals ◽  
2020 ◽  
Vol 10 (5) ◽  
pp. 612 ◽  
Author(s):  
Andrés Felipe Santacruz-Londoño ◽  
Oscar Rios-Diez ◽  
José A. Jiménez ◽  
Carlos Garcia-Mateo ◽  
Ricardo Aristizábal-Sierra
Keyword(s):  
Cast Steel ◽  
Isothermal Holding ◽  
High Strength ◽  
Cast Steels ◽  
Final Microstructure ◽  
Potential Applications ◽  
Steel Castings ◽  
Kinetics Of ◽  
Holding Temperature

Nanoscale bainite is a remarkable microstructure that exhibits a very promising combination of high strength with good ductility and toughness. The development of these types of microstructures has been focused on wrought materials, and very little information is available for steel castings. In this work, a specially designed cast steel with 0.76 wt % C was fabricated, and the heat treatment cycles to develop bainitic nanostructures were determined by studying the kinetics of the bainitic transformation using high-resolution dilatometry. The effects of isothermal holding temperature and time on the final microstructure and mechanical properties were thoroughly characterized in order to evaluate a future industrial implementation of the process in an effort to contribute to enhance and widen the potential applications for cast steels.

scholarly journals Phylogenetic and Kinetic Characterization of a Suite of Dehydrogenases from a Newly Isolated Bacterium, Strain SG61-1L, That Catalyze the Turnover of Guaiacylglycerol-β-Guaiacyl Ether Stereoisomers

2015 ◽  
Vol 81 (23) ◽  
pp. 8164-8176 ◽  
Author(s):  
Shannu Palamuru ◽  
Nikki Dellas ◽  
Stephen L. Pearce ◽  
Andrew C. Warden ◽  
John G. Oakeshott ◽  
...  
Keyword(s):  
Cell Walls ◽  
Plant Biomass ◽  
Catalytic Performance ◽  
Manufacturing Industries ◽  
Plant Cell Walls ◽  
Chemical Manufacturing ◽  
Potential Applications ◽  
Bacterium Strain ◽  
Alternative Feedstocks

ABSTRACTLignin is a complex aromatic polymer found in plant cell walls that makes up 15 to 40% of plant biomass. The degradation of lignin substructures by bacteria is of emerging interest because it could provide renewable alternative feedstocks and intermediates for chemical manufacturing industries. We have isolated a bacterium, strain SG61-1L, that rapidly degrades all of the stereoisomers of one lignin substructure, guaiacylglycerol-β-guaiacyl ether (GGE), which contains a key β-O-4 linkage found in most intermonomer linkages in lignin. In an effort to understand the rapid degradation of GGE by this bacterium, we heterologously expressed and kinetically characterized a suite of dehydrogenase candidates for the first known step of GGE degradation. We identified a clade of active GGE dehydrogenases and also several other dehydrogenases outside this clade that were all able to oxidize GGE. Several candidates exhibited stereoselectivity toward the GGE stereoisomers, while others had higher levels of catalytic performance than previously described GGE dehydrogenases for all four stereoisomers, indicating a variety of potential applications for these enzymes in the manufacture of lignin-derived commodities.

Characterization of “Green” Composites Reinforced by Cellulose Nanofibers

2007 ◽  
Vol 334-335 ◽  
pp. 389-392 ◽  
Author(s):  
Hitoshi Takagi ◽  
Akira Asano
Keyword(s):  
Mechanical Properties ◽  
Flexural Modulus ◽  
Cellulose Nanofibers ◽  
Molding Pressure ◽  
Green Composites ◽  
Mixing Process ◽  
Environment Friendly ◽  
Preparation Methods ◽  
Uniform Dispersion

Environment-friendly “green” composites were fabricated from a starch-based, dispersion-type biodegradable resin and cellulose nanofibers. The mixture of the dispersion-type biodegradable resin and cellulose nanofibers were blended well by using a home-use mixer and a stirrer, and then dried in air or in a vacuum. Composites were prepared by conventional hot pressing at a constant temperature of 140°C and at pressures from 10 to 50 MPa. Their flexural strength as well as flexural modulus increased with increasing the molding pressure, and were also affected by preparation methods and conditions. Their mechanical properties such as strength and modulus had a good correlation with their density. Especially it can be seen that there is significant effectiveness in a stirrer mixing process, which results in the improved uniform dispersion of nanofibers.

Characterization of carbides in M50NiL

1991 ◽  
Vol 49 ◽  
pp. 606-607
Author(s):  
L. S. Lin ◽  
K. P. Gumz ◽  
A. V. Karg ◽  
C. C. Law
Keyword(s):  
Temperature Effects ◽  
Base Composition ◽  
Lattice Parameter ◽  
Control Surface ◽  
Carbide Formation ◽  
Particle Sizes ◽  
Low Carbon ◽  
Fee Structure ◽  
Heat Treated

Carbon and temperature effects on carbide formation in the carburized zone of M50NiL are of great importance because they can be used to control surface properties of bearings. A series of homogeneous alloys (with M50NiL as base composition) containing various levels of carbon in the range of 0.15% to 1.5% (in wt.%) and heat treated at temperatures between 650°C to 1100°C were selected for characterizations. Eleven samples were chosen for carbide characterization and chemical analysis and their identifications are listed in Table 1.Five different carbides consisting of M6C, M2C, M7C3 and M23C6 were found in all eleven samples examined as shown in Table 1. M6C carbides (with least carbon) were found to be the major carbide in low carbon alloys (<0.3% C) and their amounts decreased as the carbon content increased. In sample C (0.3% C), most particles (95%) encountered were M6C carbide with a particle sizes range between 0.05 to 0.25 um. The M6C carbide are enriched in both Mo and Fe and have a fee structure with lattice parameter a=1.105 nm (Figure 1).

Characterization of high strength cement paste with pristine graphite and heptane-graphite emulsion

2016 ◽  
Author(s):  
Aileen Vandenberg ◽  
Daniel Massucci ◽  
Steven Woltornist ◽  
Douglas Adamson ◽  
Kay Wille
Keyword(s):  
Cement Paste ◽  
High Strength

Characterization of Clad Joints of High Strength Low Alloy Steel with Stainless Steel and Titanium

2018 ◽  
Vol 51 (4) ◽  
pp. 46
Author(s):  
N. Venkateswara Rao ◽  
G. Madhusudhan Reddy ◽  
S. Nagarjuna
Keyword(s):  
Stainless Steel ◽  
Alloy Steel ◽  
High Strength ◽  
Low Alloy Steel

scholarly journals Synthesis and Characterization of Novel Castor Oil-Based Polyol for Potential Applications in Coatings

2019 ◽  
Vol 7 (1) ◽  
pp. 31-40 ◽  
Author(s):  
Azam Sardari ◽  
Ali Asghar Sabbagh Alvani ◽  
Seyed Reza Ghaffarian
Keyword(s):  
Castor Oil ◽  
Synthesis And Characterization ◽  
Potential Applications

scholarly journals Characterization of Phosphate Coatings: Influence of the Acid Pickling Conditions

Materials ◽  
2021 ◽  
Vol 14 (4) ◽  
pp. 1048
Author(s):  
Belén Díaz ◽  
X. Ramón Nóvoa ◽  
Carmen Pérez ◽  
Sheila Silva-Fernández
Keyword(s):  
Citric Acid ◽  
High Strength ◽  
Acid Pickling ◽  
Acid Cleaning ◽  
Inorganic Acids ◽  
Phosphate Coatings ◽  
Acid Bath ◽  
Coating Morphology ◽  
Coating Weight

This research emphasizes the importance of the acid cleaning prior to the phosphate development on high-strength steel rods. It compares the phosphate properties achieved after different acid-pickling conditions. The most common inorganic acids were considered in this study. Additionally, taking into account the environmental and safety concerns of these acids, the assessment of a less harmful organic acid is presented. This study revealed significant differences in the coating morphology and chemical composition whereas no great changes were found in terms of the coating weight or porosity. Thus, hydrochloric and sulfuric acid promote the growth of a Fe-enriched phosphate layer with a less conductive character that is not developed after the pickling with phosphoric acid. The phosphate developed after the citric acid pickling is comparable to that developed after the inorganic acids although with a porosity slightly higher. The temperature of the citric acid bath is an important parameter that affects to the phosphate appearance, composition, and porosity.

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