scholarly journals Parameters Influencing the Outcome of Additive Manufacturing of Tiny Medical Devices Based on PEEK

Materials ◽  
2020 ◽  
Vol 13 (2) ◽  
pp. 466 ◽  
Author(s):  
Yiqiao Wang ◽  
Wolf-Dieter Müller ◽  
Adam Rumjahn ◽  
Andreas Schwitalla
Keyword(s):  
Medical Devices ◽  
Fused Deposition Modeling ◽  
High Accuracy ◽  
Design Parameters ◽  
Fused Deposition ◽  
Polyether Ether Ketone ◽  
Deposition Modeling ◽  
3D Printed ◽  
Ether Ketone

In this review, we discuss the parameters of fused deposition modeling (FDM) technology used in finished parts made from polyether ether ketone (PEEK) and also the possibility of printing small PEEK parts. The published articles reporting on 3D printed PEEK implants were obtained using PubMed and search engines such as Google Scholar including references cited therein. The results indicate that although many have been experiments conducted on PEEK 3D printing, the consensus on a suitable printing parameter combination has not been reached and optimized parameters for printing worth pursuing. The printing of reproducible tiny-sized PEEK parts with high accuracy has proved to be possible in our experiments. Understanding the relationships among material properties, design parameters, and the ultimate performance of finished objects will be the basis for further improvement of the quality of 3D printed medical devices based on PEEK and to expand the polymers applications.

scholarly journals Applications of 3D-Printed PEEK via Fused Filament Fabrication: A Systematic Review

Polymers ◽  
2021 ◽  
Vol 13 (22) ◽  
pp. 4046
Author(s):  
Rupak Dua ◽  
Zuri Rashad ◽  
Joy Spears ◽  
Grace Dunn ◽  
Micaela Maxwell
Keyword(s):  
Systematic Review ◽  
Fused Deposition Modeling ◽  
Chemical Properties ◽  
Organic Polymer ◽  
Current Status ◽  
Fused Filament Fabrication ◽  
Fused Deposition ◽  
Polyether Ether Ketone ◽  
Deposition Modeling ◽  
3D Printed

Polyether ether ketone (PEEK) is an organic polymer that has excellent mechanical, chemical properties and can be additively manufactured (3D-printed) with ease. The use of 3D-printed PEEK has been growing in many fields. This article systematically reviews the current status of 3D-printed PEEK that has been used in various areas, including medical, chemical, aerospace, and electronics. A search of the use of 3D-printed PEEK articles published until September 2021 in various fields was performed using various databases. After reviewing the articles, and those which matched the inclusion criteria set for this systematic review, we found that the printing of PEEK is mainly performed by fused filament fabrication (FFF) or fused deposition modeling (FDM) printers. Based on the results of this systematic review, it was concluded that PEEK is a versatile material, and 3D-printed PEEK is finding applications in numerous industries. However, most of the applications are still in the research phase. Still, given how the research on PEEK is progressing and its additive manufacturing, it will soon be commercialized for many applications in numerous industries.

scholarly journals Research on the Fused Deposition Modeling of Polyether Ether Ketone

Polymers ◽  
2021 ◽  
Vol 13 (14) ◽  
pp. 2344
Author(s):  
Ruoxiang Gao ◽  
Jun Xie ◽  
Jinghui Yang ◽  
Chaojie Zhuo ◽  
Jianzhong Fu ◽  
...  
Keyword(s):  
Tensile Strength ◽  
Fused Deposition Modeling ◽  
Fused Deposition ◽  
Polyether Ether Ketone ◽  
Raster Angle ◽  
Deposition Modeling ◽  
Ether Ketone ◽  
Nozzle Temperature ◽  
Warpage Deformation ◽  
Printing Speed

As a special engineering polymer, polyether ether ketone (PEEK) has been used widely due to its excellent mechanical properties, high thermal stability, and chemical resistance. Fused deposition modeling (FDM) is a promising process for fabricating PEEK parts. However, due to the semi-crystalline property and high melting point of PEEK, determining appropriate process parameters is important to reduce warpage deformation and improve the mechanical properties of PEEK. In this article, the influence of raster angle and infill density was determined by single factor experiment, which are the two most important parameters. The results showed that samples with 0°/90° raster angle and 50% infill density had the best comprehensive properties in terms of warpage deformation, tensile strength, and specific strength. Subsequently, based on the results above, the effects of printing speed, nozzle temperature, platform temperature, raster width, and layer thickness were analyzed by orthogonal experiment. The results indicated that platform temperature had the greatest impact on warpage deformation while printing speed and nozzle temperature were significant parameters on tensile strength. Through optimization, warpage deformation of the samples could be reduced to almost 0 and tensile strength could increase by 19.6% (from 40.56 to 48.50 MPa). This will support the development of FDM for PEEK.

Optimization of fused deposition modeling process parameters using the Taguchi method to improve the tensile properties of 3D-printed polyether ether ketone

2021 ◽  
pp. 146442072110175
Author(s):  
Timoumi Mohamed ◽  
Najoua Barhoumi ◽  
Khalid Lamnawar ◽  
Abderrahim Maazouz ◽  
Amna Znaidi
Keyword(s):  
Tensile Properties ◽  
Young’S Modulus ◽  
Layer Thickness ◽  
Process Parameters ◽  
Fused Deposition Modeling ◽  
Young's Modulus ◽  
Fused Deposition ◽  
Polyether Ether Ketone ◽  
Deposition Modeling ◽  
Ether Ketone

The interesting mechanical properties of polyether ether ketone give the material a place among the foremost competitors when it comes to replacing metal. Fused deposition modeling has been recognized as an alternative method to process polyether ether ketone parts. In this study, the effect of different process parameters such as nozzle, bed, and radiant temperatures as well as printing speed and layer thickness on the tensile properties of three-dimensional printed polyether ether ketone was investigated. The optimization of the tensile properties of PEEK were studied by performing a reduced number of experiments, using the experimental design method based on the Taguchi approach which limits the number of experiments to 8 instead of 32. Results showed that a decent Young’s modulus was found by setting the nozzle temperature, print speed, and bed temperatures to their high levels and by setting the layer thickness and radiant temperature to their low level. Using these parameters, a Young’s modulus of 3.5 GPa was obtained, which represents 87.5% of the value indicated in the technical sheet. With these settings, we also found a tensile strength of 45.5 MPa, which corresponds to 46.4% of the value given by the studied polyether ether ketone material. A scanning electron microscopic investigation of the porosity and interlayer adhesion, confirmed that a higher bed temperature also tended to promote adhesion between layers.

scholarly journals Method of smoothing the surface of additively manufactured polylactide by thermal treatment in sodium chloride

2021 ◽  
Vol 338 ◽  
pp. 01022
Author(s):  
Jan Pawlik ◽  
Damian Dzienniak
Keyword(s):  
Surface Roughness ◽  
Sodium Chloride ◽  
Thermal Treatment ◽  
Polylactic Acid ◽  
Fused Deposition Modeling ◽  
Optimal Parameters ◽  
Fused Deposition ◽  
Deposition Modeling ◽  
3D Printed

The paper contains a study of the influence of thermal treatment of the 3D-printed polylactide parts in sodium chloride dust on the surface roughness of the manufactured part. The conducted experiment features annealing with the use of two different sizes of NaCl crystals and two levels of temperature. All the samples were made with natural polylactic acid filament using the fused deposition modeling (FDM) method. The samples were put into a salt scaffold and placed in the electric furnace to remelt the surface of the part while keeping pressure on the walls to prevent unwanted deformation. The results show that it is possible to improve the quality of additively manufactured component’s surfaces as long as optimal parameters are applied.

Biodegradable 3D Printed Polymer Microneedles for Transdermal Drug Delivery

2018 ◽  
Author(s):  
Michael A. Luzuriaga ◽  
Danielle R. Berry ◽  
John C. Reagan ◽  
Ronald A. Smaldone ◽  
Jeremiah J. Gassensmith
Keyword(s):  
Drug Delivery ◽  
3D Printing ◽  
Transdermal Drug Delivery ◽  
Fused Deposition Modeling ◽  
Fused Deposition ◽  
Modeling Software ◽  
Deposition Modeling ◽  
3D Printed ◽  
Microfabrication Technique ◽  
Mechanical Strengths

Biodegradable polymer microneedle (MN) arrays are an emerging class of transdermal drug delivery devices that promise a painless and sanitary alternative to syringes; however, prototyping bespoke needle architectures is expensive and requires production of new master templates. Here, we present a new microfabrication technique for MNs using fused deposition modeling (FDM) 3D printing using polylactic acid, an FDA approved, renewable, biodegradable, thermoplastic material. We show how this natural degradability can be exploited to overcome a key challenge of FDM 3D printing, in particular the low resolution of these printers. We improved the feature size of the printed parts significantly by developing a post fabrication chemical etching protocol, which allowed us to access tip sizes as small as 1 μm. With 3D modeling software, various MN shapes were designed and printed rapidly with custom needle density, length, and shape. Scanning electron microscopy confirmed that our method resulted in needle tip sizes in the range of 1 – 55 µm, which could successfully penetrate and break off into porcine skin. We have also shown that these MNs have comparable mechanical strengths to currently fabricated MNs and we further demonstrated how the swellability of PLA can be exploited to load small molecule drugs and how its degradability in skin can release those small molecules over time.

scholarly journals Controlling magnetic properties of 3D-printed magnetic elastomer structures via fused deposition modeling

AIP Advances ◽  
2021 ◽  
Vol 11 (2) ◽  
pp. 025223
Author(s):  
Thomas M. Calascione ◽  
Nathan A. Fischer ◽  
Thomas J. Lee ◽  
Hannah G. Thatcher ◽  
Brittany B. Nelson-Cheeseman
Keyword(s):  
Magnetic Properties ◽  
Fused Deposition Modeling ◽  
Fused Deposition ◽  
Deposition Modeling ◽  
3D Printed

scholarly journals Pressure Orientation-Dependent Recovery of 3D-Printed PLA Objects with Varying Infill Degree

Polymers ◽  
2021 ◽  
Vol 13 (8) ◽  
pp. 1275 ◽  
Author(s):  
Guido Ehrmann ◽  
Andrea Ehrmann
Keyword(s):  
Shape Memory ◽  
Fused Deposition Modeling ◽  
Static Load ◽  
Shape Memory Polymer ◽  
Applied Pressure ◽  
Poly Lactic Acid ◽  
Fused Deposition ◽  
Deposition Modeling ◽  
Load Tests ◽  
3D Printed

Poly(lactic acid) is not only one of the most often used materials for 3D printing via fused deposition modeling (FDM), but also a shape-memory polymer. This means that objects printed from PLA can, to a certain extent, be deformed and regenerate their original shape automatically when they are heated to a moderate temperature of about 60–100 °C. It is important to note that pure PLA cannot restore broken bonds, so that it is necessary to find structures which can take up large forces by deformation without full breaks. Here we report on the continuation of previous tests on 3D-printed cubes with different infill patterns and degrees, now investigating the influence of the orientation of the applied pressure on the recovery properties. We find that for the applied gyroid pattern, indentation on the front parallel to the layers gives the worst recovery due to nearly full layer separation, while indentation on the front perpendicular to the layers or diagonal gives significantly better results. Pressing from the top, either diagonal or parallel to an edge, interestingly leads to a different residual strain than pressing from front, with indentation on top always firstly leading to an expansion towards the indenter after the first few quasi-static load tests. To quantitatively evaluate these results, new measures are suggested which could be adopted by other groups working on shape-memory polymers.

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