scholarly journals Hierarchical Microstructure of Laser Powder Bed Fusion Produced Face-Centered-Cubic-Structured Equiatomic CrFeNiMn Multicomponent Alloy

Materials ◽  
2020 ◽  
Vol 13 (20) ◽  
pp. 4498
Author(s):  
Xuan Yang ◽  
Yanling Ge ◽  
Joonas Lehtonen ◽  
Simo-Pekka Hannula
Keyword(s):  
Cell Walls ◽  
Multicomponent Alloy ◽  
Face Centered Cubic ◽  
Powder Bed Fusion ◽  
Laser Powder Bed Fusion ◽  
Powder Bed ◽  
Hierarchical Microstructure ◽  
Cell Structures ◽  
Single Face ◽  
Face Centered

A cobalt-free equiatomic CrFeNiMn multicomponent alloy was fabricated from gas-atomized powder using laser powder bed fusion (L-PBF), also known as selective laser melting (SLM). The as-built specimens had a single face-centered cubic (FCC) structure, relative density of 98%, and hardness up to 248 HV0.5 for both the scanning speeds applied. In this work, we report the hierarchical microstructural features observed in the as-built specimens. These are comprised of melt pools, grains, cell structures including dendritic cells, elongated cells, equiaxed cells (~500 nm), and sub-cells (150–300 nm). The cell and sub-cell walls are composed of a notably high density of dislocations. In addition, segregation of Mn and Ni was detected at the cell walls, but only occasionally at the sub-cell walls. SLM exhibits the capability to produce FCC-structured equiatomic CrFeNiMn multicomponent alloy with the refined and hierarchical microstructure.

scholarly journals Hydrogen Effects in Equiatomic CrFeNiMn Alloy Fabricated by Laser Powder Bed Fusion

Metals ◽  
2021 ◽  
Vol 11 (6) ◽  
pp. 872
Author(s):  
Xuan Yang ◽  
Yuriy Yagodzinskyy ◽  
Yanling Ge ◽  
Eryang Lu ◽  
Joonas Lehtonen ◽  
...  
Keyword(s):  
Thermal Desorption Spectroscopy ◽  
Hydrogen Uptake ◽  
Hydrogen Desorption ◽  
Face Centered Cubic ◽  
Powder Bed Fusion ◽  
Laser Powder Bed Fusion ◽  
Powder Bed ◽  
The Face ◽  
316L Austenitic Stainless Steel ◽  
Face Centered

This study investigates the effects of laser powder bed fusion (LPBF) on the hydrogen uptake of the face-centered cubic (FCC) equiatomic CrFeNiMn multicomponent alloy after cathodic hydrogen charging (HC). Hydrogen desorption was evaluated using thermal desorption spectroscopy (TDS), and microstructural changes after the TDS test were examined. Results reveal that the amount of hydrogen absorbed by LPBF CrFeNiMn alloy was significantly higher than that in pulsed electric current sintered (PECS) CrFeNiMn alloy or in conventional 316L austenitic stainless steel. The observations are ascribed to the differences in the amount of hydrogen absorbed by the multicomponent lattice, dislocation densities, width of segregation range at cell walls created by the rapid cooling in LBPF, and vacancies remaining after cooling to room temperature. A hydrogen-charged LBPF transmission electron microscope (TEM) specimen was also characterized. Stacking faults and cracks along the (111)-planes of austenite were observed. Scanning electron microscopy (SEM) of the surface of the TDS-tested samples also indicated hydrogen-induced cracks and hydrogen-induced submicron pits at the grain boundary inclusions.

scholarly journals Microstructure Evolution of FeNiCoCrAl1.3Mo0.5 High Entropy Alloy during Powder Preparation, Laser Powder Bed Fusion, and Microplasma Spraying

Materials ◽  
2021 ◽  
Vol 14 (24) ◽  
pp. 7870
Author(s):  
Anton Semikolenov ◽  
Pavel Kuznetsov ◽  
Tatyana Bobkova ◽  
Svetlana Shalnova ◽  
Olga Klimova-Korsmik ◽  
...  
Keyword(s):  
Solid Solution ◽  
Phase Composition ◽  
Cast Alloy ◽  
High Entropy Alloy ◽  
Gas Atomization ◽  
Face Centered Cubic ◽  
Powder Bed Fusion ◽  
Laser Powder Bed Fusion ◽  
Powder Bed ◽  
X Ray

In the present study, powder of FeCoCrNiMo0.5Al1.3 HEA was manufactured by gas atomization process, and then used for laser powder bed fusion (L-PBF) and microplasma spraying (MPS) technologies. The processes of phase composition and microstructure transformation during above mentioned processes and subsequent heat treatment were analyzed by X-ray diffraction (XRD), scanning electron microscopy (SEM), energy dispersive X-ray spectroscopy (EDS), and differential thermal analysis (DTA) methods. It was found that gas atomization leads to a formation of dendrites of body centered cubic (BCC) supersaturated solid solution with insignificant Mo-rich segregations on the peripheries of the dendrites. Annealing leads to an increase of element segregations till to decomposition of the BCC solid solution and formation of σ-phase and B2 phase. Microstructure and phase composition of L-PBF sample are very similar to those of the powder. The MPS coating has a little fraction of face centered cubic (FCC) phase because of Al oxidation during spraying and formation of regions depleted in Al, in which FCC structure becomes more stable. Maximum hardness (950 HV) is achieved in the powder and L-PBF samples after annealing at 600 °C. Elastic modulus of the L-PBF sample, determined by nanoindentation, is 165 GPa, that is 12% lower than that of the cast alloy (186 GPa).

Microstructure of In738Lc Fabricated Using Laser Powder Bed Fusion Additive Manufacturing

2021 ◽  
pp. 1-19
Author(s):  
Nandana Menon ◽  
Tanjheel Hasan Mahdi ◽  
Amrita Basak
Keyword(s):  
Additive Manufacturing ◽  
Electron Backscatter Diffraction ◽  
Small Scale ◽  
Second Phase ◽  
Face Centered Cubic ◽  
Powder Bed Fusion ◽  
Laser Powder Bed Fusion ◽  
Powder Bed ◽  
Nickel Base Superalloys ◽  
Nickel Base

Abstract Nickel-base superalloys are extensively used in the production of gas turbine hot-section components as they offer exceptional creep strength and superior fatigue resistance at high temperatures. Such improved properties are due to the presence of precipitate-strengthening phases such as Ni3Ti or Ni3Al (gγ phases) in the normally face-centered cubic (FCC) structure of the solidified nickel. Although this second phase is the main reason for the improvements in properties, the presence of such phases also results in increased processing difficulties as these alloys are prone to crack formation. In this work, specimens of IN738LC are fabricated on a Coherent Creator laser powder bed fusion (L-PBF) additive manufacturing (AM) equipment. Optical microscopy (OM), scanning electron microscopy (SEM), electron backscatter diffraction (EBSD), and X-Ray diffraction (XRD) are carried out to characterize the deposit region. Metallurgical continuity is achieved in the entire deposit region and the specimens do not show any warpage. However, the specimens show voids (e.g., pores and cracks) in the deposit region. The results show that the percentage void area decreases along the build height direction. The deposited IN738LC shows polycrystalline grains in the entire deposit region as confirmed by XRD and EBSD. The grain size also shows variations along the build direction. In summary, the results open opportunities for academic researchers and small scale businesses in fabricating high-gγ nickel-base superalloys on a desktop laser powder bed fusion AM equipment

Microstructure of IN738LC Fabricated Using Laser Powder Bed Fusion Additive Manufacturing

2021 ◽  
Author(s):  
Nandana Menon ◽  
Tanjheel Hassan Mahdi ◽  
Amrita Basak
Keyword(s):  
Additive Manufacturing ◽  
Electron Backscatter Diffraction ◽  
Small Scale ◽  
Second Phase ◽  
Face Centered Cubic ◽  
Powder Bed Fusion ◽  
Laser Powder Bed Fusion ◽  
Powder Bed ◽  
Nickel Base Superalloys ◽  
Nickel Base

Abstract Nickel-base superalloys are extensively used in the production of gas turbine hot-section components as they offer exceptional creep strength and superior fatigue resistance at high temperatures. Such improved properties are due to the presence of precipitate-strengthening phases such as Ni3Ti or Ni3Al (γ′ phases) in the normally face-centered cubic (FCC) structure of the solidified nickel. Although this second phase is the main reason for the improvements in properties, the presence of such phases also results in increased processing difficulties as these alloys are prone to crack formation. In this work, specimens of IN738LC are fabricated on a Coherent Creator laser powder bed fusion (L-PBF) additive manufacturing (AM) equipment. Optical microscopy (OM), scanning electron microscopy (SEM), electron backscatter diffraction (EBSD), and X-Ray diffraction (XRD) are carried out to characterize the deposit region. Metallurgical continuity is achieved in the entire deposit region and the specimens do not show any warpage. However, the specimens show voids (e.g., pores and cracks) in the deposit region. The results show that the percentage void area decreases along the build height direction. The deposited IN738LC shows polycrystalline grains in the entire deposit region as confirmed by XRD and EBSD. The grain size also shows variations along the build direction. In summary, the results open opportunities for academic researchers and small-scale businesses in fabricating high-γ′ nickel-base superalloys on a desktop laser powder bed fusion AM equipment.

scholarly journals Influence of relative density on quasi-static and fatigue failure of lattice structures in Ti6Al4V produced by laser powder bed fusion

2021 ◽  
Vol 11 (1) ◽  
Author(s):  
Markel Alaña ◽  
Antonio Cutolo ◽  
Sergio Ruiz de Galarreta ◽  
Brecht Van Hooreweder
Keyword(s):  
Relative Density ◽  
Fatigue Failure ◽  
Lattice Structure ◽  
Yield Criterion ◽  
Fatigue Properties ◽  
Face Centered Cubic ◽  
Lattice Structures ◽  
Powder Bed Fusion ◽  
Laser Powder Bed Fusion ◽  
Powder Bed

AbstractLattice structures produced by additive manufacturing have been increasingly studied in recent years due to their potential to tailor prescribed mechanical properties. Their mechanical performances are influenced by several factors such as unit cell topology, parent material and relative density. In this study, static and dynamic behaviors of Ti6Al4V lattice structures were analyzed focusing on the criteria used to define the failure of lattices. A modified face-centered cubic (FCCm) lattice structure was designed to avoid the manufacturing problems that arise in the production of horizontal struts by laser powder bed fusion. The Gibson–Ashby curves of the FCCm lattice were obtained and it was found that relative density not only affects stiffness and strength of the structures, but also has important implications on the assumption of macroscopic yield criterion. Regarding fatigue properties, a stiffness based criterion was analyzed to improve the assessment of lattice structure failure in load bearing applications, and the influence of relative density on the stiffness evolution was studied. Apart from common normalization of S–N curves, a more accurate fatigue failure surface was developed, which is also compatible with stiffness based failure criteria. Finally, the effect of hot isostatic pressing in FCCm structures was also studied.

scholarly journals On the Relevance of Volumetric Energy Density in the Investigation of Inconel 718 Laser Powder Bed Fusion

Materials ◽  
2020 ◽  
Vol 13 (3) ◽  
pp. 538 ◽  
Author(s):  
Fabrizia Caiazzo ◽  
Vittorio Alfieri ◽  
Giuseppe Casalino
Keyword(s):  
Surface Roughness ◽  
Energy Density ◽  
Process Parameters ◽  
Vickers Hardness ◽  
Powder Bed Fusion ◽  
Processing Conditions ◽  
Laser Powder Bed Fusion ◽  
Powder Bed ◽  
Fractional Density ◽  
Experimental Variation

Laser powder bed fusion (LPBF) can fabricate products with tailored mechanical and surface properties. In fact, surface texture, roughness, pore size, the resulting fractional density, and microhardness highly depend on the processing conditions, which are very difficult to deal with. Therefore, this paper aims at investigating the relevance of the volumetric energy density (VED) that is a concise index of some governing factors with a potential operational use. This paper proves the fact that the observed experimental variation in the surface roughness, number and size of pores, the fractional density, and Vickers hardness can be explained in terms of VED that can help the investigator in dealing with several process parameters at once.

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