scholarly journals Effect of Annealing on Strain Rate Sensitivity of Metallic Glass under Nanoindentation

Metals ◽  
2020 ◽  
Vol 10 (8) ◽  
pp. 1063
Author(s):  
Mingcan Li

The influence of isothermal annealing on the strain rate sensitivity (SRS) of a Zr-based bulk metallic glass (BMG) was investigated by nanoindentation. A more positive SRS is observed with a decrease in the content of the free volume (FV) of the sample. Furthermore, the SRS becomes nearly constant with increasing annealing time when the FV is annealed out. By taking into consideration the FV-assisted activation and combination of the shear transformation zones (STZs), the underlying mechanism is well understood. The current work may offer useful insights into the correlation between the microstructure and mechanical properties of BMGs.

Metals ◽  
2021 ◽  
Vol 11 (2) ◽  
pp. 339
Author(s):  
Xiang Wang ◽  
Zhi Qiang Ren ◽  
Wei Xiong ◽  
Si Nan Liu ◽  
Ying Liu ◽  
...  

The negative strain rate sensitivity (SRS) of metallic glasses is frequently observed. However, the physical essence involved is still not well understood. In the present work, small-angle X-ray scattering (SAXS) and high-resolution transmission electron microscopy (HRTEM) reveal the strong structure heterogeneity at nanometer and tens of nanometer scales, respectively, in bulk metallic glass (BMG) Zr64.13Cu15.75Ni10.12Al10 subjected to fully confined compression processing. A transition of SRS of stress, from 0.012 in the as-cast specimen to −0.005 in compression processed specimen, was observed through nanoindentation. A qualitative formulation clarifies the critical role of internal stress induced by structural heterogeneity in this transition. It reveals the physical origin of this negative SRS frequently reported in structurally heterogeneous BMG alloys and its composites.


2006 ◽  
Vol 503-504 ◽  
pp. 31-36 ◽  
Author(s):  
Johannes Mueller ◽  
Karsten Durst ◽  
Dorothea Amberger ◽  
Matthias Göken

The mechanical properties of ultrafine-grained metals processed by equal channel angular pressing is investigated by nanoindentations in comparison with measurements on nanocrystalline nickel with a grain size between 20 and 400 nm produced by pulsed electrodeposition. Besides hardness and Young’s modulus measurements, the nanoindentation method allows also controlled experiments on the strain rate sensitivity, which are discussed in detail in this paper. Nanoindentation measurements can be performed at indentation strain rates between 10-3 s-1 and 0.1 s-1. Nanocrystalline and ultrafine-grained fcc metals as Al and Ni show a significant strain rate sensitivity at room temperature in comparison with conventional grain sized materials. In ultrafine-grained bcc Fe the strain rate sensitivity does not change significantly after severe plastic deformation. Inelastic effects are found during repeated unloading-loading experiments in nanoindentations.


Metals ◽  
2019 ◽  
Vol 9 (3) ◽  
pp. 344 ◽  
Author(s):  
Simon Sevsek ◽  
Christian Haase ◽  
Wolfgang Bleck

The strain-rate-dependent deformation behavior of an intercritically annealed X6MnAl12-3 medium-manganese steel was analyzed with respect to the mechanical properties, activation of deformation-induced martensitic phase transformation, and strain localization behavior. Intercritical annealing at 675 °C for 2 h led to an ultrafine-grained multi-phase microstructure with 45% of mostly equiaxed, recrystallized austenite and 55% ferrite or recovered, lamellar martensite. In-situ digital image correlation methods during tensile tests revealed strain localization behavior during the discontinuous elastic-plastic transition, which was due to the localization of strain in the softer austenite in the early stages of plastic deformation. The dependence of the macroscopic mechanical properties on the strain rate is due to the strain-rate sensitivity of the microscopic deformation behavior. On the one hand, the deformation-induced phase transformation of austenite to martensite showed a clear strain-rate dependency and was partially suppressed at very low and very high strain rates. On the other hand, the strain-rate-dependent relative strength of ferrite and martensite compared to austenite influenced the strain partitioning during plastic deformation, and subsequently, the work-hardening rate. As a result, the tested X6MnAl12-3 medium-manganese steel showed a negative strain-rate sensitivity at very low to medium strain rates and a positive strain-rate sensitivity at medium to high strain rates.


2020 ◽  
Vol 4 (3) ◽  
pp. 110
Author(s):  
Sujan Debnath ◽  
Tan Ke Khieng ◽  
Mahmood Anwar ◽  
Animesh Kumar Basak ◽  
Alokesh Pramanik

Viscoelastic materials, such as natural fibre-reinforced polymer composites, are strain rate sensitive. In the present investigation, the low strain rate sensitivity (0.00028 s−1, 0.00085 s−1 and 0.0017 s−1) of different sized bagasse particle-reinforced (212 µm and 300 µm) epoxy composites was examined using the Weibull analysis method. The filler loading content was optimized at 2 wt.% to achieve better mechanical properties. Based on the experimental results, it was observed that composites with 212 µm filler particles had higher characteristic strengths, more consistent failure strengths and higher energy absorption properties with higher loading speeds, compared to that of 300 µm filler particles. Based on the mathematical models for particle–matrix interactions, improvements in mechanical properties are attributed to proper filler dispersion and a better fibre–matrix interfacial strength.


Metals ◽  
2019 ◽  
Vol 10 (1) ◽  
pp. 22 ◽  
Author(s):  
Lin Tian ◽  
Dominik Tönnies ◽  
Moritz Hirsbrunner ◽  
Tim Sievert ◽  
Zhiwei Shan ◽  
...  

In this work, structural and mechanical properties of hydrogen-charged metallic glass are studied to evaluate the effect of hydrogen on early plasticity. Hydrogen is introduced into samples of a Zr-based (Vit 105) metallic glass using electrochemical charging. Nanoindentation tests reveal a clear increase in modulus and hardness as well as in the load of the first pop-in with increasing hydrogen content. At the same time, the probability of a pop-in occurring decreases, indicating that hydrogen hinders the onset of plastic instabilities while allowing local homogeneous deformation. The hydrogen-induced stiffening and hardening is rationalized by hydrogen stabilization of shear transformation zones (STZs) in the amorphous structure, while the improved ductility is attributed to the change in the spatial correlation of the STZs.


Energies ◽  
2020 ◽  
Vol 13 (8) ◽  
pp. 2105 ◽  
Author(s):  
Alon Ratner ◽  
Richard Beaumont ◽  
Iain Masters

Strain rate sensitivity has been widely recognized as a significant feature of the dynamic mechanical properties of lithium-ion cells, which are important for their accurate representation in automotive crash simulations. This research sought to improve the precision with which dynamic mechanical properties can be determined from drop tower impact testing through the use of a diaphragm to minimize transient shock loads and to constrain off-axis motion of the indenter, specialized impact absorbers to reduce noise, and observation of displacement with a high speed camera. Inert pouch cells showed strain rate sensitivity in an increased stiffness during impact tests that was consistent with the poromechanical interaction of the porous structure of the jellyroll with the liquid electrolyte. The impact behaviour of the inert pouch cells was similar to that of an Expanded Polypropylene foam (EPP), with the exception that the inert pouch cells did not show hysteretic recovery under the weight of the indenter. This suggests that the dynamic mechanical behaviour of the inert pouch cells is analogous to a highly damped foam.


2020 ◽  
Vol 840 ◽  
pp. 155562
Author(s):  
Huaican Chen ◽  
Yang Hai ◽  
Gang Wang ◽  
Xiao Liu ◽  
Juping Xu ◽  
...  

2001 ◽  
Author(s):  
Paul S. Robinson ◽  
Tony W. Lin ◽  
Paul R. Reynolds ◽  
Kathleen A. Derwin ◽  
Renato V. Iozzo ◽  
...  

Abstract Little is known about the contributions of specific extracellular matrix components of tendon to the tissue’s mechanical properties. Type I collagen, given its abundance and association into long fibrils, is thought to dominate the elastic properties of tendon. Proteoglycans (PGs) are believed to provide elasticity through their potential role in transferring stress between discontinuous fibrils, as well as viscoelasticity via their interaction with water. Previous studies suggest relationships between collagen or PGs and tissue mechanics [1,2]. However, no study to date has isolated the contributions that distinct tendon components make to the elastic and viscoelastic properties of tendon. Recently, transgenic mice with prescribed mutations or deletions of various genes for specific tendon constituents have become available. In this study, we use transgenic mice as a tool to investigate the contributions of tendon components to tendon function based on a previously described approach [3]. In particular, we compare the strain rate sensitivity among fascicles from the tails of mice described in Table 1. We hypothesize that (a) fascicles with alterations in type I collagen (C1TJ8 and C1M8) will have different elastic properties but no difference in strain rate sensitivity than age-matched controls (CTL8), and (b) fascicles with alterations in proteoglycan (DKO8 and CTL3 [4]) will have different elastic properties and different strain rate sensitivity than CTL8 fascicles.


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