scholarly journals Selective Laser Melting of High Relative Density and High Strength Parts Made of Minor Surface Oxidation Treated Pure Copper Powder

Metals ◽  
2021 ◽  
Vol 11 (12) ◽  
pp. 1883
Author(s):  
Peng Yang ◽  
Xingye Guo ◽  
Dingyong He ◽  
Zhen Tan ◽  
Wei Shao ◽  
...  

Pure Copper (Cu) is very difficult to prepare using selective laser melting (SLM) technology. This work successfully prepared the pure Cu with high relative density and high strength by the SLM technology using a surface oxidation treatment. The gas-atomized pure Cu powder was used as the feedstock in this work. Before the SLM process, the pure Cu powder was initially handled using the surface oxidation treatment to coat the powder with an extremely thin layer of Cu2O. The SLMed highly dense specimens contain α-Cu and nano-Cu2O phases. A relationship between the processing parameters (laser power (LP), scanning speed (SS), and hatch space (HS)) and density of Cu alloy in SLM was also investigated. The microstructure of SLMed Cu consists of fine grains with grain sizes ranging from 0.5 to ~30 μm. Tensile testing and detailed microstructural characterization were performed on specimens in the as-SLMed and pure copper state specimens. The mechanical property experiments showed that the specimens prepared by SLM technology containing nano-oxide phases had higher yield strength and tensile strength than that of other SLM-built pure copper. However, the elongation was remarkably decreased compared to other SLM-built pure copper, due to the fine grains and the nano-oxides.

Materials ◽  
2020 ◽  
Vol 13 (19) ◽  
pp. 4268 ◽  
Author(s):  
Mariusz Król ◽  
Przemysław Snopiński ◽  
Jiří Hajnyš ◽  
Marek Pagáč ◽  
Dariusz Łukowiec

In the present study, 18% Ni 300 maraging steel powder was processed using a selective laser melting (SLM) technique to study porosity variations, microstructure, and hardness using various process conditions, while maintaining a constant level of energy density. Nowadays, there is wide range of utilization of metal technologies and its products can obtain high relative density. A dilatometry study revealed that, through heating cycles, two solid-state effects took place, i.e., precipitation of intermetallic compounds and the reversion of martensite to austenite. During the cooling process, one reaction took place (i.e., martensitic transformation), which was confirmed by microstructure observation. The improvements in the Rockwell hardness of the analyzed material from 42 ± 2 to 52 ± 0.5 HRC was improved as a result of aging treatment at 480 °C for 5 h. The results revealed that the relative density increased using laser speed (340 mm/s), layer thickness (30 µm), and hatch distance (120 µm). Relative density was found approximately 99.3%. Knowledge about the influence of individual parameters in the SLM process on porosity will enable potential manufacturers to produce high quality components with desired properties.


2019 ◽  
Vol 9 (3) ◽  
pp. 583 ◽  
Author(s):  
Shigang Bai ◽  
Nataliya Perevoshchikova ◽  
Yu Sha ◽  
Xinhua Wu

In view of the importance of accurately measuring the relative density of a selective laser melted (SLMed) part for optimizing the selective laser melting (SLM) processing parameters, suitable procedures of the Archimedes method considering the surface-connected cavities were proposed by comparing the results using the Archimedes method with image analysis. The effects of the SLM processing parameters on the relative density of AlSi10Mg were investigated using the proposed procedures of the Archimedes methods and image analysis. Fourteen SLMed samples were produced by different SLM processing parameters according to Doehlert Matrix. The regression models correlating relative density and three SLM processing parameters (laser power, scan speed, and hatching distance) were built and the optimum parameter combination to get a high relative density was obtained. By plotting the response surfaces and contours of the regression models, it was found that the relative densities are both higher at the combination of the higher scan speed, higher power, and lower hatching distance and at the combination of a lower scan speed, a moderate laser power, and a optional hatching distance. It was also found that the parameter of hatching distance is the crucial parameter to get a high relative density and to get high mechanical property.


Author(s):  
Christian Felber ◽  
Florian Rödl ◽  
Ferdinand Haider

Abstract The most promising metal processing additive manufacturing technique in industry is selective laser melting, but only a few alloys are commercially available, limiting the potential of this technique. In particular high strength aluminum alloys, which are of great importance in the automotive industry, are missing. An aluminum 2024 alloy, reinforced by Ti-6Al-4V and B4C particles, could be used as a high strength alternative for aluminum alloys. Heat treating can be used to improve the mechanical properties of the metal matrix composite. Dynamic scanning calorimetry shows the formation of Al2Cu precipitates in the matrix instead of the expected Al2CuMg phases due to the loss of magnesium during printing, and precipitation processes are accelerated due to particle reinforcement and additive manufacturing. Strong reactions between aluminum and Ti-6Al-4V are observed in the microstructure, while B4C shows no reaction with the matrix or the titanium. The material shows high hardness, high stiffness, and low ductility through precipitation and particle reinforcement.


Materials ◽  
2019 ◽  
Vol 12 (6) ◽  
pp. 930 ◽  
Author(s):  
Martin Malý ◽  
Christian Höller ◽  
Mateusz Skalon ◽  
Benjamin Meier ◽  
Daniel Koutný ◽  
...  

The aim of this study is to observe the effect of process parameters on residual stresses and relative density of Ti6Al4V samples produced by Selective Laser Melting. The investigated parameters were hatch laser power, hatch laser velocity, border laser velocity, high-temperature preheating and time delay. Residual stresses were evaluated by the bridge curvature method and relative density by the optical method. The effect of the observed process parameters was estimated by the design of experiment and surface response methods. It was found that for an effective residual stress reduction, the high preheating temperature was the most significant parameter. High preheating temperature also increased the relative density but caused changes in the chemical composition of Ti6Al4V unmelted powder. Chemical analysis proved that after one build job with high preheating temperature, oxygen and hydrogen content exceeded the ASTM B348 limits for Grade 5 titanium.


2016 ◽  
Vol 2016 (1) ◽  
pp. 000517-000522
Author(s):  
Aarief Syed-Khaja ◽  
Christopher Kaestle ◽  
Joerg Franke

Abstract Additive manufacturing (AM) has the potential to lead significant changes in the present state-of-the-art production processes. This provides tool-free and direct manufacturing of complex geometries simultaneously integrating various functions into components. Though AM techniques are widely used in various sectors, the application into electronics production has been not yet explored. In electronics production, substrate development has high relevance due to their multi-functionality in giving the mechanical support and electrically connecting electronic components. This contribution introduces an innovative approach in the development of high-temperature substrates through additive layered manufacturing. The technique used in the investigations was selective laser melting (SLM) of copper based powder materials mainly bronze alloy and pure copper, for the generation of conductive patterns on ceramic surfaces. The process parameters for the SLM technique and the influential factors in the generation of conductive structures are discussed in detail.


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