Experimental Study on Distillation Column Parameters for Liquefaction Device of Low Concentration Coalbed Methane

The input-output ratio and comprehensive energy consumption of low concentration coalbed methane cryogenic liquefaction devices are determined by the process parameters in control of the distillation column. In order to accurately control the actual operation process of the distillation column, the effect of the operating temperature of the distillation column on the liquefaction performance of a cold box was studied experimentally, and the optimal control parameters of the distillation column were obtained. The results show that the recovery rate of methane decreases with the increase in temperature at the top of the distillation column, and when this temperature is higher than −178 °C, the methane recovery rate drops sharply to below 90%. When the temperature at the bottom of the distillation column rises from −154 °C to −142.7 °C, the purity of LNG products is improved, and when this temperature is increased to −143.5 °C, the purity of products at the bottom of the distillation column reaches the standard, and can be stored safely. In actual operation, the evaporation temperature at the bottom of the column should not be higher than −140 °C. In the process of industrial plant design, measures should be taken to reduce the interaction of the temperature regulation at the top and bottom of the distillation column. When selecting the refrigerant circulation compressor, the leakage of the refrigerant should be considered to maintain the operating pressure of the refrigeration cycle.