scholarly journals Oil Recovery from Dry Grind Ethanol Plant Coproducts Using Ethanol

Processes ◽  
2021 ◽  
Vol 9 (12) ◽  
pp. 2282
Author(s):  
Md. Sanaul Huda ◽  
Nurun Nahar

Corn ethanol bio-refineries are seeking economic processing strategies for recovering oil from their coproducts. The addition of ethanol can be an efficient method to recover the oil from the coproducts as the industry has available ethanol. This study considered the effects of ethanol on oil recovery from distillers’ dried grains with solubles (DDGS) and oil partitioning from whole stillage (WS) on a laboratory scale. Ethanol was added with original and heavier fraction DDGS in different temperatures (room temperature ~20 °C, 30 °C, 40 °C, and 50 °C) and solids loadings (20%, 30%, and 40%), and their effects on oil recovery were evaluated. The whole stillage was incubated with ethanol at room temperature (~20 °C) and 50 °C separately to analyze WS’s oil distribution in the liquid and solid phases. The amount of recovered oil from the original and heavier fractions of DDGS varies from 25–45% and 45–70%, respectively, with an increment of temperature. Increasing solids loadings up to 30% had no effect on oil recovery from either DDGS sample. Ethanol treatment in WS resulted in 8–10% higher wet yield of liquid fraction and 17–20% of oil increase in liquid fraction than the control treatment. It is also notable that temperature positively impacted oil partitioning from WS. The results showed that ethanol could improve oil recovery from DDGS and oil partition in WS by varying different process conditions. This outcome is beneficial to ethanol plants to increase corn oil yield using their existing setup and in-situ product.

2021 ◽  
Vol 11 (1) ◽  
Author(s):  
Liliana G. Fidalgo ◽  
Mário M. Q. Simões ◽  
Susana Casal ◽  
José A. Lopes-da-Silva ◽  
Ivonne Delgadillo ◽  
...  

AbstractHyperbaric storage at room temperature (HS/RT: 75 MPa/25 °C) of vacuum-packaged fresh Atlantic salmon (Salmo salar) loins was studied for 30 days and compared to atmospheric pressure at refrigerated temperatures (AP/5 °C, 30 days) and RT (AP/25 °C, 5 days). Most of the fatty acids were not affected by storage conditions, with only a slight decrease of docosahexaenoic acid (DHA) content (n-3 polyunsaturated fatty acid) for AP samples, reflected in the lower polyene index values obtained and higher oxidation extent. For HS, a lower lipid oxidation extension and a slower increase of myofibrillar fragmentation index values were observed, when compared to AP samples. The volatile profile was similar for the HS and fresh samples, with the HS samples retaining fresh-like alcohols and aldehydes components, which disappeared in AP samples, mainly in AP/25 °C samples. The volatile profile for AP samples (5 and 25 °C) revealed mostly spoilage-like compounds due to microbial activity. Drip loss increased progressively during the 30 days of storage under HS, while a slight decrease of water holding capacity after 5 days was observed, increasing further after 30 days. Regarding textural properties, only resilience was affected by HS, decreasing after 30 days. So, HS/RT could represent an interesting extended preservation methodology of fresh salmon loins, since allows retaining important physicochemical properties for at least 15 days, while refrigeration after 5 days showed already volatile spoilage-like compounds due to microbial activity. Furthermore, this methodology allows additional considerable energy savings when compared to refrigeration.


Bioethanol ◽  
2016 ◽  
Vol 2 (1) ◽  
Author(s):  
María García-Torreiro ◽  
Miguel Álvarez Pallín ◽  
María López-Abelairas ◽  
Thelmo A. Lu-Chau ◽  
Juan M. Lema

AbstractBioconversion of lignocellulosic materials into ethanol requires an intermediate pretreatment step for conditioning biomass. Sugar yields from wheat straw were previously improved by the addition of a mild alkali pretreatment step before bioconversion by the white-rot fungus Irpex lacteus. In this work, an alternative alkaline treatment, which significantly reduces water consumption, was implemented and optimized. Sugar recovery increased 117% with respect to the previously developed alkaline wash process at optimal process conditions (30°C, 30 minutes and 35.7% (w/w) of NaOH). In order to further reduce operational costs, a system for alkali recycling was implemented. This resulted in the treatment of 150% more wheat straw using the same amount of NaOH. Finally, enzymatic hydrolysis was optimized and resulted in a reduction of enzyme dose of 33%.


1986 ◽  
Vol 73 ◽  
Author(s):  
William L. Olson

ABSTRACTAlumina sols derived from aluminum sec-butoxide (Yoldas) were characterized. The distribution of the polymer sizes within the sol, determined by gel filtration chromatography (GFC), was found to be dramatically affected by small changes in the chemical processing or preparative procedure. Aging the sol at room temperature for two weeks produced no significant change in the GFC elution curves of the alumina sol. Sols with a “milky” appearance were found to exhibit a wider distribution of polymers by GFC than transparent sols. Rotary evaporation of the sol followed by redissolution of the residue was found to change the polymer size distribution described by the gel filtration elution curves. These observations coupled with 27Al NMR spectroscopy and viscometry measurements were used to elucidate the effects of process conditions and aging on the molecular structure of the sol.


2021 ◽  
Vol 11 (1) ◽  
Author(s):  
Tomasz K. Pietrzak ◽  
Agata Jarocka ◽  
Cezariusz Jastrzębski ◽  
Tomasz Płociński ◽  
Marek Wasiucionek ◽  
...  

AbstractBismuth sesquioxide ($$\hbox {Bi}_2\hbox {O}_3$$ Bi 2 O 3 ) draws much attention due to wide variety of phases in which it exists depending on the temperature. Among them, $$\delta$$ δ phase is specially interesting because of its high oxide ion conductivity and prospects of applications as an electrolyte in fuel cells. Unfortunately, it is stable only in a narrow temperature range ca. 730–830 $$^{\circ }$$ ∘ C. Our group has developed a facile and reproducible two-stage method of stabilizing $$\hbox {Bi}_2\hbox {O}_3$$ Bi 2 O 3 crystalline phases confined in nanocrystallites embedded in amorphous matrix. In the first stage, glassy materials were obtained by a routine melt-quenching method: pure $$\hbox {Bi}_2\hbox {O}_3$$ Bi 2 O 3 powders were melted in porcelain crucibles and fast-cooled down to room temperature. In the second step, the materials were appropriately heat-treated to induce formation of crystallites of $$\beta$$ β , $$\delta$$ δ or $$\gamma$$ γ $$\hbox {Bi}_2\hbox {O}_3$$ Bi 2 O 3 phases confined in a glassy matrix, depending on the process conditions. It was found out that the vitrification of the initial $$\hbox {Bi}_2\hbox {O}_3$$ Bi 2 O 3 and the subsequent nanocrystallization were unexpectedly possible due to the presence of some Al, and Si impurities from the crucibles. Systematic DTA, XRD, optical, Raman and SEM/EDS studies were carried out to investigate the influence of the syntheses processes and allowed us to determine conditions under which the particular phases appear and remain stable down to room temperature.


2021 ◽  
Vol 9 ◽  
Author(s):  
Malte Jörn Krafft ◽  
Jens Berger ◽  
Bodo Saake

The utilization of agricultural products and residues for the production of value-added and biobased products is a highly relevant topic in present research. Due to the natural recalcitrance of lignocellulosic biomass against enzymatic degradation, pretreatments are important requirement for further processes. For the raw material in this study, corn stover (CS) as highly available agricultural residue and maize silage (MS) as model substrate for an ensiled agricultural product were pretreated by steam refining. However, after processing a liquid fraction and fibers are present. Subsequent to steaming the fiber fraction is well characterized. Nonetheless, in depth characterizations of the filtrates are also important for their subsequent utilization. Decreasing molar masses from 7,900 g/mol to 1,100 g/mol for CS filtrates and 100.000–12.900 g/mol for MS filtrates were determined with increasing severity. Due to their proven inhibitory effect on microorganisms weak acids, furans and phenolic compounds within the liquid phased were analyzed. Especially formic acid increases with increasing severity from 0.27 to 1.20% based on raw material for CS and from 0.07 to 0.23% based on raw material for MS. Further GC/MS measurements indicate, that up to 8.25% (CS filtrate) and 5.23% (MS filtrates) of the total peak area is related to inhibitory phenols. Considering the data, detoxification strategies are of non-negligible importance for filtrates after steam refining and should be considered for further research and process or parameter optimizations. An alternative may be the application of milder process conditions in order to prevent the formation of inhibitory degradation products or the dilution of the gained filtrates.


2012 ◽  
Vol 594-597 ◽  
pp. 2541-2544
Author(s):  
Xiao Hui Wu ◽  
Kao Ping Song ◽  
Chi Dong ◽  
Ji Cheng Zhang ◽  
Jing Fu Deng

As line well pattern is the main development technique in the thin and poor oil layers of Daqing Oilfield South West Ⅱ PⅠ group, the layers have been idle and the degree of reserve recovery is far less than the region level. In response to these problems, we analyzed the balanced flood performance of various layers and the remaining oil distribution through numerical simulation technique. It shows that, the main remaining oil type of intended layers is caused by voidage-injection imperfection. Considering the needs of the follow-up infill well pattern and tertiary oil recovery, we decided to keep the well network independent and integrated without disturbing the pattern configuration and main mining object of various sets of well pattern. Finally we confirmed to perforate-adding the first infill wells of intended layers to consummate the water flooding regime. Through analyzing the production target of different well pattern optimization programs relatively, it shows that the best program has regular well pattern and large drilled thickness.


2016 ◽  
Vol 4 (3) ◽  
pp. 121
Author(s):  
Amir Zaman Khan

Exploring ways to improve stand establishment and crop productivity under abiotic stresses like drought is important. Two years experiments were conducted at University of Agriculture, Peshawar-Pakistan to examine the efficacy of six pre-sowing seed hardening agents. Seeds of wheat cultivar Uqab-2000 were hardened in six different chemicals of various concentration viz; PEG-8000 (10%), CaCl2 (4%), KNO3, (3%), Mannital (4%), NaCl (5%), Na2SO4 (2%) along with water soaking and dry seeds as control for 24 hours and drying back to original moisture content at room temperature. The soaking and drying of seeds was repeated twice for 12 hours. The results showed that pre-sowing hardening of seed with PEG-8000, CaCl2 and KNO3 gave higher germination, decreased days to 50% germination, increased shoot length, root length, seedling fresh and dry weight in laboratory experiment as compared with other hardening and control treatment. Under field conditions, maximum plant height (93.53cm), spikelet’s spike-1 (17.16), grains spike-1 (50.82), 1000 grain weight (39.97 g), grain yield (3482 kg ha-1) and maximum harvest index (32.5%) were observed in PEG-8000 hardened seed than control treatment (2872 kg ha-1). Seed hardened in PEG-8000, CaCl2 and KNO3 gave 30% increase in grain yield as compared to Mannital, NaCl and Na2SO4 which gave 15% increase in grain yield over control treatment.


2008 ◽  
Vol 86 (1) ◽  
pp. 83-91 ◽  
Author(s):  
Hossein Noureddini ◽  
Santosh R. P. Bandlamudi ◽  
Emily A. Guthrie
Keyword(s):  
Corn Oil ◽  

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