Development of Abnormal Grain Growth in Cold Rolled and Recrystallized AA 5182 Sheet

Author(s):  
Han Gil Suk ◽  
E.J. Shin ◽  
Moo Young Huh
2021 ◽  
Author(s):  
Sukjin Lee ◽  
Eun Jung Seo ◽  
Robert L. Cryderman ◽  
David K. Matlock ◽  
John G. Speer

Abstract Precision cold-forging processes are used to produce near-netshape parts that may then be carburized. During carburization thermal cycles, abnormal grain growth (AGG) after cold forging is known to develop microstructures which limit fatigue strength. In the present study, a small 0.04 wt.% Nb addition was made to a low-alloyed AISI 4121 steel containing 0.3 wt.% Mo. Subcritically annealed specimens were cold rolled (to simulate cold forging) at selected reduction ratios up to 50%, heated according to a simulated gas carburizing cycle at 930 °C, and water quenched to produce a final martensitic microstructure. The number density of abnormally grown grains increased rapidly as the cold rolling reduction ratio increased from 0 to 10%. With a further increase in reduction ratio, the extent of AGG decreased and was absent in samples subjected to the maximum reduction ratio of 50%. The evolution of fine (Nb, Mo)(C,N) precipitates at various stages of processing was characterized by thermodynamic calculations and electron microscopy and compared to the occurrence of abnormal austenite grain growth. The significance of these results for controlling AGG and thus optimizing fatigue performance in commercially-produced cold-forged and carburized components is discussed.


2017 ◽  
Vol 898 ◽  
pp. 1123-1133
Author(s):  
Y.Z. Zhu ◽  
Xiao Hui Li ◽  
J.C. Li ◽  
Wei Long Fan ◽  
Cheng Wei Xia ◽  
...  

AA1235 aluminum alloys were twin roll cast into a 7.0 mm-thick billet and further rolled into a plate with 70% reduction, followed by annealing at 500 C for 8 h. Abnormal grains were found to be formed on the plate bottom surface. SEM, EBSD, and micro X-ray diffraction were used to analyze the mechanism underlying the abnormal growth of these grains. Results showed that the {100} <001> texture was formed in the surrounding normal grains adjacent to the abnormal grain. The orientation angle between the abnormal grain and its adjacent normal grains was 45°. The {100} <001> texture formed during rolling and annealing accelerated abnormal grain growth. The partially dissolved Fe precipitates were heterogeneously distributed in the plate bottom heterogeneously, which also mainly explained abnormal grain growth.


2013 ◽  
Vol 753 ◽  
pp. 329-332
Author(s):  
Yoshihiro Arita ◽  
Yoshiyuki Ushigami ◽  
Kenichi Murakami ◽  
Kohsaku Ushioda

Texture change during grain growth in Fe-3%Si non-oriented electrical steel was investigated. Cold rolled steel, 0.35mm in thickness, was annealed and recrystallized as an initial structure. Normal grain growth and abnormal grain growth occurred by additional annealing. {111} was dominant in the initial texture. However {100} component, which was not in majority in the initial structure, became stronger after normal grain growth. It was revealed that an average grain size of {100} in the initial structure was bigger than those of other components by analysis of the EBSD data,. Therefore, it is concluded that {100} strengthened after normal grain growth due to its size advantage. On the other hand, {111} components became more stronger after abnormal grain growth. It is inferred that another mechanism of the texture change worked in abnormal grain growth.


2012 ◽  
Vol 715-716 ◽  
pp. 946-951 ◽  
Author(s):  
Dmitri A. Molodov ◽  
Nathalie Bozzolo

The effect of a magnetic field on texture and microstructure development in cold rolled (80%) commercially pure zirconium (Zr701) was investigated. X-ray diffraction and EBSD measurements were utilized for the texture and microstructure characterization. The results revealed that a magnetic field promotes grain growth in the investigated material. During annealings at 550°C this is particularly apparent from the faster development of specific (0/180, 35, 30) texture components and the bigger mean grain size after magnetic annealing. The magnetic annealing at 700°C resulted in an asymmetry of the two major texture components. This is due to a magnetic driving force for grain growth arising from the anisotropic magnetic susceptibility of zirconium. During annealing at 700°C the abnormal grain growth occurred. This behavior is attributed to the higher mobility of grain boundaries between grains misoriented by 30° around [000. The magnetic field essentially enhanced the observed abnormal grain growth.


2006 ◽  
Vol 116-117 ◽  
pp. 316-319 ◽  
Author(s):  
Han Gil Suk ◽  
E.J. Shin ◽  
Moo Young Huh

Grain growth in the cold rolled and subsequently recrystallized AA 5182 sheets was investigated by means of microstructure observations and texture measurements. Grain growth behavior strongly depends on the annealing temperatures. Grain growth hardly took place at temperatures lower than 470°C, which is attributed to a low mobility of grain boundaries. Abnormal grain growth occurred at temperatures ranging from 480 to 530°C. Annealing above 560°C gave rise to the dissolution of inhibitor precipitates, which led to normal grain growth.


2018 ◽  
Author(s):  
Risheng Pei ◽  
Sandra Korte-Kerzel ◽  
Talal Al-Samman

Metals ◽  
2021 ◽  
Vol 11 (3) ◽  
pp. 504
Author(s):  
Huasong Liu ◽  
Yannan Dong ◽  
Hongguang Zheng ◽  
Xiangchun Liu ◽  
Peng Lan ◽  
...  

AlN precipitates are frequently adopted to pin the austenite grain boundaries for the high-temperature carburization of special gear steels. For these steels, the grain coarsening criterion in the carburizing process is required when encountering the composition optimization for the crack-sensitive steels. In this work, the quantitative influence of the Al and N content on the grain size after carburization is studied through pseudocarburizing experiments based on 20Cr steel. According to the grain structure feature and the kinetic theory, the abnormal grain growth is demonstrated as the mode of austenite grain coarsening in carburization. The AlN precipitate, which provides the dominant pinning force, is ripened in this process and the particle size can be estimated by the Lifshitz−Slyosov−Wagner theory. Both the mass fraction and the pinning strength of AlN precipitate show significant influence on the grain growth behavior with the critical values indicating the grain coarsening. These criteria correspond to the conditions of abnormal grain growth when bearing the Zener pinning, which has been analyzed by the multiple phase-field simulation. Accordingly, the models to predict the austenite grain coarsening in carburization were constructed. The prediction is validated by the additional experiments, resulting in accuracies of 92% and 75% for the two models, respectively. Finally, one of the models is applied to optimize the Al and N contents of commercial steel.


2020 ◽  
Vol 128 (18) ◽  
pp. 185109
Author(s):  
Christian Braun ◽  
Raphael A. Zeller ◽  
Hanadi Menzel ◽  
Jörg Schmauch ◽  
Carl E. Krill ◽  
...  

1994 ◽  
Vol 343 ◽  
Author(s):  
J. A. Floro ◽  
C. V. Thompson

ABSTRACTAbnormal grain growth is characterized by the lack of a steady state grain size distribution. In extreme cases the size distribution becomes transiently bimodal, with a few grains growing much larger than the average size. This is known as secondary grain growth. In polycrystalline thin films, the surface energy γs and film/substrate interfacial energy γi vary with grain orientation, providing an orientation-selective driving force that can lead to abnormal grain growth. We employ a mean field analysis that incorporates the effect of interface energy anisotropy to predict the evolution of the grain size/orientation distribution. While abnormal grain growth and texture evolution always result when interface energy anisotropy is present, whether secondary grain growth occurs will depend sensitively on the details of the orientation dependence of γi.


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