Supercritical Fluid Extraction of Genistein from Extruded Soybean

2012 ◽  
Vol 178-181 ◽  
pp. 838-842
Author(s):  
Gui Hua Sheng ◽  
Quan Cheng Zhou
Keyword(s):  
Mathematical Model ◽  
Optimal Condition ◽  
Supercritical Fluid Extraction ◽  
Supercritical Fluid ◽  
Orthogonal Rotation ◽  
Optimal Conditions ◽  
Fluid Extraction ◽  
Model Set ◽  
Experimental Values ◽  
The Mathematical Model

An optimal condition of supercritical fluid extraction (SFE) for genistein in extruded soybean was developed. Optimal conditions through quadratic orthogonal rotation design were verified. The results from SC – CO2 showed that all five experiment factors tested have significant effects on the yield of genistein. The mathematical model set had close agreements with experimental values. It was found that there were 32 optimal extract conditions under which genistein yield higher than 0.092% were gotten through simulate compute. The optimal extracting conditions were stable and recurrable. SC–CO2 had a potential in the extraction of genistein from extruded soybean products.

Modeling of supercritical fluid extraction of flavonoids from Calycopteris floribunda leaves

2014 ◽  
Vol 68 (3) ◽  
Author(s):  
Xiong Liu ◽  
Dong-Liang Yang ◽  
Jia-Jia Liu ◽  
Kuan Xu ◽  
Guo-Hui Wu
Keyword(s):  
Supercritical Fluid Extraction ◽  
Supercritical Fluid ◽  
Extraction Process ◽  
Optimal Conditions ◽  
Fluid Extraction ◽  
Pressure Method ◽  
Organic Solvent Extraction ◽  
Drug Lead ◽  
Temperature And Pressure ◽  
Central Composite

AbstractThe aim of this study was to obtain flavonoids extracts from Calycopteris floribunda leaves using supercritical fluid extraction (SFE) with CO2 and a co-solvent. Pachypodol, a potential anticancer drug lead compound separated from the extracts, was examined. Classical organic solvent extraction (CE) with ethanol was performed to evaluate the high pressure method. HPLC analysis was introduced to interpret the differences between SFE and CE extracts in terms of antioxidant activity and the concentration of pachypodol. SFE kinetics and mathematical modeling of the overall extraction curves (OEC) were investigated. Evaluation of the models against experimental data showed that the Sovová model performs the best. The supercritical fluid extraction process was optimized using a central composite design (CCD), where temperature and pressure were adjusted. The optimal conditions of SFE were: pressure of 30 MPa and temperature of 35°C.

Influence of the CO2 Quality in the Antioxidant Activity of Rosemary Extracts Dearomatized by Supercritical Fluid Extraction

2001 ◽  
Vol 7 (2) ◽  
pp. 177-182 ◽  
Author(s):  
E. Ibanez ◽  
S. Lopez-Sebastian ◽  
J. Fernandez ◽  
J. Tabera ◽  
J. M. Bueno ◽  
...  
Keyword(s):  
Antioxidant Activity ◽  
Experimental Design ◽  
Supercritical Fluid Extraction ◽  
Supercritical Fluid ◽  
Sunflower Oil ◽  
Extraction Process ◽  
Taguchi Experimental Design ◽  
Optimal Conditions ◽  
Fluid Extraction

The effect of the CO2 quality (mainly related to CO2 content) in the antioxidant activity of rosemary extracts deodorized by using a supercritical fluid extraction process is analyzed. A Taguchi experimental design was used to study the influence of the CO2 quality on the antioxidant activity of the rosemary dearomatized extracts. The antioxidant activity of the rosemary extracts obtained in optimal conditions was tested with sunflower oil.

scholarly journals Optimization of Extraction of Phenolic Compounds with Antimicrobial Properties from Origanum vulgare

Processes ◽  
2021 ◽  
Vol 9 (6) ◽  
pp. 1032
Author(s):  
Taja Žitek ◽  
Dragana Borjan ◽  
Andrej Golle ◽  
Željko Knez ◽  
Maša Knez
Keyword(s):  
Antimicrobial Activity ◽  
Antioxidant Activity ◽  
Supercritical Fluid Extraction ◽  
Supercritical Fluid ◽  
Inhibitory Concentration ◽  
Optimal Conditions ◽  
Fluid Extraction ◽  
Origanum Vulgare ◽  
E Coli ◽  
Design Expert

Oregano (Origanum vulgare) is considered to be a good and cheap source of phenolic compounds with favorable biological activities, especially antimicrobial and antioxidant properties. Hypothesis/Purpose: The current work explored the optimization of the process conditions of solid–liquid extraction from Origanum vulgare to obtain extracts with high antimicrobial activity. We investigated which parameters promoted different efficiencies, leading to the maximum extraction of phenols and the consequent highest level of biological activity. Design-Expert Pro 11 was selected to design and analyze the experiments. The extracts were obtained by maceration as a simple method to recover value-added compounds from plant material, and supercritical fluid extraction was carried out as a green method with a high selectivity to obtain the compounds of interest. Pressure, temperature, and time were varied to obtain extracts with high antioxidant and antimicrobial activity. According to the results obtained using Design-Expert, the optimal conditions for maceration were at a temperature of 83 °C. The 1,1′-diphenyl-2-picrylhydrase method was used for the determination of antioxidant potential, while microdilution methods were used to determine the antimicrobial potential with regard to Staphylococcus aureus, Escherichia coli, and Candida albicans. A level of antioxidant activity of 87.21% was achieved. Supercritical fluid extracts showed higher antioxidant activity at a higher temperature of 60 °C and higher pressure of 25 MPa, although the results at 40 °C and 25 MPa were similar. The lowest minimum inhibitory concentration (MIC) values were 0.147 mg/mL for S. aureus, 0.728 mg/mL for E. coli, and 0.311 mg/mL for C. albicans. Overall, the optimal conditions for supercritical fluid extraction were 25 MPa and 40 °C. On the other hand, amounts of 0.208 mg/mL for S. aureus, 1.031 mg/mL for E. coli and 0.872 mg/mL for C. albicans were obtained using maceration. The MIC values of extracts obtained by supercritical fluid extraction were comparable to the minimum inhibitory concentration values obtained by different conventional techniques, such as those of Clevenger and Soxhlet.

scholarly journals Determination of optimal parameters of basil supercritical fluid extraction by response surface methodology

2016 ◽  
pp. 193-203
Author(s):  
Snezana Filip ◽  
Senka Vidovic ◽  
Branimir Pavlic ◽  
Zoran Zekovic
Keyword(s):  
Response Surface Methodology ◽  
Response Surface ◽  
Supercritical Fluid Extraction ◽  
Supercritical Fluid ◽  
Interactive Effect ◽  
Extraction Process ◽  
Extraction Yield ◽  
Fluid Extraction ◽  
Experimental Values

The supercritical fluid extraction of aroma compounds from basil (Ocimum basilicum L.) was studied. Response surface methodology was used to optimize the parameters of the process. Full factorial design was applied to evaluate the effects of two independent variables (pressure and temperature) on the extraction yield and linalool yield. From the response surface plots, pressure and temperature exhibited independent and interactive effect on the extraction yield. The optimal conditions to obtain the highest extraction yield (1.91%) of O. basilicum were the pressure of 29.7 MPa and temperature of 59.2oC, whereas the highest yield of linalool (1.998 g?kg-1) was obtained at the pressure of 20 MPa and temperature of 40oC. The experimental values agreed with the predicted ones, indicating suitability of the response surface methodology for optimizing the extraction process.

Analytical Supercritical Fluid Extraction

1994 ◽  
Author(s):  
Maria Dolores Luque de Castro ◽  
Miguel Valcárcel ◽  
Maria Teresa Tena
Keyword(s):  
Supercritical Fluid Extraction ◽  
Supercritical Fluid ◽  
Fluid Extraction

VOLATILES IN TAMAIOASA ROMANEASCA VIA SUPERCRITICAL FLUID EXTRACTION (SFE) ANALYSIS

2015 ◽  
Vol 14 (2) ◽  
pp. 297-302 ◽  
Author(s):  
Valeriu V. Cotea ◽  
Lucia Cintia Colibaba ◽  
Liliana Rotaru ◽  
Bogdan Nechita ◽  
Marius Niculaua ◽  
...  
Keyword(s):  
Supercritical Fluid Extraction ◽  
Supercritical Fluid ◽  
Fluid Extraction

Modelling and Simulation of NO2 Dispersion Phenomenon in Atmosphere by Analytical-Experimental Methods

2008 ◽  
Vol 59 (10) ◽  
Author(s):  
Delia Perju ◽  
Harieta Pirlea ◽  
Gabriela-Alina Brusturean ◽  
Dana Silaghi-Perju ◽  
Sorin Marinescu
Keyword(s):  
Mathematical Model ◽  
Nitrogen Dioxide ◽  
Modeling And Simulation ◽  
Human Health ◽  
Experimental Methods ◽  
Negative Effects ◽  
Real Situation ◽  
Experimental Values ◽  
The Mathematical Model

The European laws and recently the Romanian ones impose more and more strict norms to the large nitrogen dioxide polluters. They are obligated to continuously improve the installations and products so that they limit and reduce the nitrogen dioxide pollution, because it has negative effects on the human health and environment. In this paper are presented these researches made within a case study for the Timi�oara municipality, regarding the modeling and simulation of the nitrogen dioxide dispersion phenomenon coming from various sources in atmosphere with the help of analytical-experimental methods. The mathematical model resulting from these researches is accurately enough to describe the real situation. This was confirmed by comparing the results obtained based on the model with real experimental values.

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