Enabling Standardization in Shear Bond Strength Tests for Orthodontic Adhesives on Natural Teeth by Using an Innovative Grip Accessory for the Testing Machine

2014 ◽  
Vol 568-570 ◽  
pp. 121-125
Author(s):  
Anca Stefania Mesaros ◽  
Gabriel Furtos ◽  
Michaela F. Mesaros ◽  
Mindra E. Badea
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Testing Machine ◽  
Testing Procedure ◽  
Testing Procedures ◽  
Orthodontic Adhesives ◽  
Number Of Factors ◽  
Natural Teeth ◽  
Material Testing Machine

Shear Bond Strength testing is one of the most common used tests for Orthodontics Adhesives. However, the standardizations of such procedures is quite difficult due to a large number of factors. While scientists are designing their studies in order to reduce errors, sometime they may find themselves in front of technical difficulties. A custom device was developed in order to allow a testing procedure that is closer to in vitro conditions. The device, mounted on a material testing machine permits sample inclination to a degree that reduces tensile component to the shear stress, therefore more accurate readings of the values are available and standardization of shear bond testing procedures is more probable.

scholarly journals Comparative Evaluation of varying Photo-polymerization Time on Shear Bond Strength and Microleakage of Four Orthodontic Adhesives: An in vitro Study

2017 ◽  
Vol 7 (3) ◽  
pp. 156-160
Author(s):  
Prerana N Zanke ◽  
Vivek Patni ◽  
Marshal Maskarenj
Keyword(s):  
Bond Strength ◽  
Comparative Evaluation ◽  
Shear Bond Strength ◽  
Testing Machine ◽  
Curing Time ◽  
Polymerization Time ◽  
Photo Polymerization ◽  
Orthodontic Adhesives ◽  
Group I

ABSTRACT Introduction High early bond strength, extended working time for optimal bracket placement, and easy cleanup of excess adhesive are few advantages of visible light-cure orthodontic adhesives. However, the shorter duration of polymerization may lead to polymer shrinkage and eventually microleakage. Objective To observe and evaluate shear bond strength (SBS) and microleakage of orthodontic brackets bonded to enamel with four commercially available orthodontic adhesives, cured only from incisal direction at various polymerization times. Materials and methods A total of 160 bovine incisors were randomly assigned to four groups according to adhesive used. Group I: bonded with Transbond XT (3M Unitek™, USA); group II: Enlight (Ormco, USA); group III: Light Bond (Reliance Ortho, USA); and group IV: Discover (Prime Dental, USA). Each group was further divided into four subgroups of A, B, C, and D according to the polymerization duration of 5, 10, 15, and 20 seconds respectively. The bonded teeth were immersed in dye solution. Brackets were then subjected to SBS test on a Universal testing machine. Surface microleakage was observed with the help of optical stereomicroscope. Results The SBS was obtained within the range of clinically accepted values, with curing time for Enlight at 5 seconds, Transbond XT and Discover at 15 seconds, and Light Bond at 20 seconds. However, Enlight was demonstrated to provide optimum SBS at least curing time: Minimum duration of 5 seconds achieved adequate SBS ~11 MPa SBS for each of Transbond XT and Enlight. The surface microleakage observed is statistically insignificant among the groups. Conclusion From a clinical perspective, a composite resin that needs minimum curing time without compromising on the bond strength is most advantageous. The results for SBS tests showed a better performance for Enlight as compared with the other adhesives: it reached its bond strength of optimum value at curing time of 5 seconds. How to cite this article Zanke PN, Patni V, Maskarenj M. Comparative Evaluation of varying Photo-polymerization Time on Shear Bond Strength and Microleakage of Four Orthodontic Adhesives: An in vitro Study. J Contemp Dent 2017;7(3):156-160.

scholarly journals Shear Bond Strength of Different Adhesive Materials used for Bonding Orthodontic Brackets : A Comparative in vitro Study

2015 ◽  
Vol 5 (1) ◽  
pp. 22-26
Author(s):  
Muzin Shahi Shaik ◽  
Snigdha Pattanaik ◽  
Sudhakar Pathuri ◽  
Arunachalam Sivakumar
Keyword(s):  
Bond Strength ◽  
Treatment Duration ◽  
Shear Bond Strength ◽  
Testing Machine ◽  
Test Group ◽  
In Vitro Study ◽  
Universal Testing ◽  
Materials Used ◽  
Adhesive Materials

Introduction: Bond strength is an important property and determines the amount of force delivered and treatment duration in orthodontics. Many light-cured bonding materials are being used; but it is required to determine the most efficient one withdesired bond strength. Objective: To determine and compare the shear bond strength of three visible light-cured composites (Transbond XT, Heliositand Enlight) and two self-cured composites (Rely-a-bond and Concise). Materials & Method: 100 extracted premolars were collected and randomly divided into 5 test groups of different adhesives. Brackets were bonded to the teeth in each test group with the respective adhesive according to the manufacturer’s instructions. Each specimen was debonded using Universal Testing Machine and the shear bond strength for each specimen was calculated. All the groups were compared by ANOVA one-way test. Results: There were statistically significant differences among the five groups (P<0.05). The shear bond strength of Enlight (13.92 ± 3.92) is similar to Transbond XT (14.30 ± 4.35). Conclusion: Light cure composites showed higher bond strength than self cure composites.

scholarly journals Effects of Universal Adhesive on Shear Bond Strength of Resin Cement to Zirconia Ceramic with Different Surface Treatments

2021 ◽  
Vol 2021 ◽  
pp. 1-6
Author(s):  
Zohreh Moradi ◽  
Farnoosh Akbari ◽  
Sara Valizadeh
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Testing Machine ◽  
In Vitro Study ◽  
Surface Treatments ◽  
Resin Cement ◽  
Zirconia Ceramic ◽  
Single Bond ◽  
Universal Adhesive

Aim. This study aimed to assess shear bond strength (SBS) of resin cement to zirconia ceramic with different surface treatments by using Single Bond Universal. Methods. In this in vitro study, 50 zirconia discs (2 × 6 mm) were divided into 5 groups of (I) sandblasting with silica-coated alumina (CoJet)  + silane + Single Bond 2, (II) sandblasting with CoJet + Single Bond Universal, (III) sandblasting with alumina + Single Bond Universal, (IV) sandblasting with alumina + Z-Prime Plus, and (V) Single Bond Universal with no surface treatment. Resin cement was applied in plastic tubes (3 × 5 mm2), and after 10,000 thermal cycles, the SBS was measured by a universal testing machine. The mode of failure was determined under a stereomicroscope at × 40 magnification. Data were analyzed using one-way ANOVA. Results. The maximum (6.56 ± 4.29 MPa) and minimum (1.94 ± 1.96 MPa) SBS values were noted in groups III and I, respectively. Group III had the highest frequency of mixed failure (60%). Group V had the maximum frequency of adhesive failure (100%). Conclusion. Single Bond Universal + sandblasting with alumina or silica-coated alumina particles is an acceptable method to provide a strong SBS between resin cement and zirconia.

scholarly journals COMPARATIVE EVALUATION OF THE SHEAR BOND STRENGTH OF THREE SELF-ETCH DENTIN BONDING AGENTS TO DENTIN: AN IN-VITRO STUDY

2020 ◽  
Vol 8 (10) ◽  
pp. 454-459
Author(s):  
Bhalla V. ◽  
◽  
K. Goud M. ◽  
Chockattu S. ◽  
Khera A ◽  
...  
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Resin Composite ◽  
Testing Machine ◽  
Group Analysis ◽  
In Vitro Study ◽  
Bonding Agents ◽  
Mandibular Molar ◽  
Self Etch

Background:Dentin bonding is an ever-evolving field in adhesive dentistry. With the introduction of newer systems into the market, there is a crucial need to test their efficiency in terms of bond strength. Dual-cured adhesives in theory may provide for a better degree of conversion as compared to conventional light-cured adhesives .Thus, the aim of this study was to compare the shear bond strength of three different self-etch adhesives namely ClearfilSE bond (Kuraray), Tetric N Bond Universal (IvoclarVivadent) and Futura Bond DC (Voco) to dentin. Materials & Methods: Ninety extracted non-carious, intact human mandibular molar teeth were selected for this study. Each tooth was decoronated using a double-sided diamond disc with water coolant to a depth of 2mm from the cusp tip .The cut dentin surface was then abraded against 600-grit wet silicon carbide papers for 60 seconds to produce a uniform smear layer. The root portion of each tooth was mounted on a plastic ring using cold cure acrylic resin. Specimens were then divided into three adhesive groups of 30 teeth each, Group A: ClearfilSE Bond (Kuraray), Group B: Tetric N Bond Universal (IvoclarVivadent), Group C :Futura Bond DC (Voco). All bonding agents were used according to the manufacturers’ instructions, in combination with the resin composite Tetric N Ceram (IvoclarVivadent). The samples were thermocycled, followed by shear bond strength testing using a Universal testing machine (Hounsfield). Data were subjected to statistical analysis using one-way analysis of variance (ANOVA) (P<0.05) and Post hoc Tukey’s test for inter- and intra- group analysis respectively. Results: Clearfil SE Bond yielded the highest shear bond strength values (30.9 ±4.66 MPa) which were statistically significant, followed byTetric N Bond Universal group (29.8 ±4.34) and the lowest shear bond strength values were recorded for Futura Bond DC (18.2 ±3.13). Conclusion: Clearfil SE bond and Tetric N bond Universal can be considered as better options than Futura Bond DC.

scholarly journals Shear Bond Strength Comparison between Two Orthodontic Adhesives and Self-Ligating and Conventional Brackets

2007 ◽  
Vol 77 (4) ◽  
pp. 701-706 ◽  
Author(s):  
Rodney G. Northrup ◽  
David W. Berzins ◽  
Thomas Gerard Bradley ◽  
William Schuckit
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Orthodontic Adhesives ◽  
Significant Difference ◽  
Conventional Brackets ◽  
Group 3 ◽  
Group 2 ◽  
Post Hoc ◽  
Group 1

Abstract Objective: To evaluate and compare the shear bond strengths of two adhesives using two types of brackets: a conventional and a self-ligating bracket system. Materials and Methods: Sixty extracted human premolars were collected. The premolars were randomly divided into three groups of 20 teeth. All three groups were direct bonded. Groups 1 and 2 used light-cured adhesive and primer (Transbond XT) with a conventional (Orthos) and a self-ligating bracket (Damon 2), respectively. Group 3 used a light-cured primer (Orthosolo) and a light-cured adhesive (Blūgloo) with a self-ligating bracket (Damon 2). The specimens were stored in distilled water at 37°C for 40 ± 2 hours, after which they were debonded and inspected for Adhesive Remnant Index (ARI) scoring. Results: The mean shear bond strength was 15.2 MPa for group 1, 23.2 MPa for group 2, and 24.8 MPa for group 3. A one-way analysis of variance and post hoc Tukey test showed significant differences in bond strength (P &lt; .001) between group 1 and groups 2 and 3 but no significant difference (P &gt; .05) between groups 2 and 3. A Weibull analysis demonstrated that all three groups provided sufficient bond strength with over 90% survival rate at normal masticatory and orthodontic force levels. A Kruskal-Wallis test showed no significant difference (P &gt; .05) in ARI scores among all three groups. Conclusions: All three groups demonstrated clinically acceptable bond strength. The Damon 2 self-ligating bracket exhibited satisfactory in vitro bond strength with both adhesive systems used.

scholarly journals Evaluation of Shear-Bond-Strength of Dental Self-Adhering Flowable Resin-Composite versus Total-Etch One to Enamel and Dentin Surfaces: An In-Vitro Study

2019 ◽  
Vol 7 (13) ◽  
pp. 2162-2166 ◽  
Author(s):  
Rasha M. Abdelraouf ◽  
Manar Mohammed ◽  
Fatma Abdelgawad
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Resin Composite ◽  
Testing Machine ◽  
Tooth Surface ◽  
Mean Values ◽  
Modes Of Failure ◽  
Group I ◽  
Permanent Molars

AIM: This study aimed to assess the shear bond strength of a self-adhering flowable resin composite versus a total-etch one to different surfaces of permanent-molars. MATERIAL AND METHODS: Thirty-six sound human permanent molars were used. The teeth were embedded in acrylic blocks, such that their buccal surfaces were shown. The teeth were divided into three groups: Group I: Uncut-Enamel, Group II: Cut-enamel-surfaces with minimal-grinding and Group III: dentin-surfaces. Half of the teeth in each group were used for bonding to a self-adhering flowable resin-composite (Dyad-flow, Kerr, USA). While the other half of each group was bonded to a total-etch flowable resin-composite (Filtek™Z350-XT,3M-ESPE, USA) which necessitate etching and bonding. Teflon-mold was used for constructing resin composite cylinders (3 × 3 mm) over the buccal surfaces. The Dyad-flow was applied in the central hole of the mould placed upon tooth-surface, and then light-cured for 20 seconds. The Filtek-Z350-XT was applied similarly after etching and bonding steps. The teeth were stored in 37°C distilled water for 24 hours. The strength was measured using a universal testing machine and statistically analysed. Modes of failure were studied using digital-microscope. RESULTS: Mean values of shear bond strength for the Dyad and Filtek-Z350-XT in the uncut-enamel were 3.5 and 24.6MPa respectively, while that for cut-enamel were 4.5 and 12.7MPa respectively (Both highly statistically significant P ≤ 0.01) and in dentin were 4.3 and 6.7MPa respectively (Statistically significant P ≤ 0.05). The failure mode for Dyad was mainly adhesive (un-cut or cut-enamel 83.3% adhesive and 16.7% mixed, while in dentin 100% adhesive). While the modes of failure for Filtek-Z350-XT in enamel, either cut or un-cut, were 50% cohesive and 50% mixed, whereas in dentin 100% adhesive. CONCLUSION: Bonding of self-etch ″Dyad-flow″ flowable resin-composite was lower than the total-etch one in enamel and dentin. Thus further material improvement may be required.

Shear Bond Strength of a Resin Composite to Six Pulp Capping Materials Used in Primary Teeth

2020 ◽  
Vol 44 (4) ◽  
pp. 234-239
Author(s):  
Latifa Alhowaish ◽  
Fouad Salama ◽  
Mohammed Al-Harbi ◽  
Mohamad Abumoatti
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Primary Teeth ◽  
Resin Composite ◽  
Testing Machine ◽  
Bond Failure ◽  
Pulp Capping ◽  
Machine Failure ◽  
Materials Used

Aim: The purpose of this in vitro study was to assess the shear bond strength (SBS) and bond failure types of a resin-composite to six pulp-capping materials used in primary teeth. Study design: Eight-disc specimens from each pulp-capping material (6 groups) to bond to Filtek™ Z350 XT Flowable using a standard PVC tube (2×2mm). All groups were prepared according to the instruction of the manufacturer. The SBS was measured with a crosshead speed of 0.5 mm/min using a universal testing machine. Failure mode evaluation was completed using Digital Microscope by two independent examiners. Results: Urbical LC® showed the highest SBS (Mean±SD) followed by ProRoot® MTA and TheraCal LC® (35.422±2.910, 22.114±2.515, and 21.175±1.983) respectively. ANOVA showed significant differences between all groups (P=0.0001). Urbical LC® and Photac™ Fil QuickAplicap™ were statistically significant different from all other pulp-capping materials groups. ProRoot® MTA was statistically significant different than Biodentine® (P=0.0001) and Photac™ Fil (P=0.0001). The total number of bond failure was recorded for cohesive B failure/cohesive in the pulp-capping material (14) and adhesive failure (14). Conclusion: Most of the tested pulp-capping materials bonded to Filtek™ Z350 XT demonstrated clinically acceptable and high SBS. Urbical LC showed the highest SBS while Biodentine® showed the lowest SBS.

In vitro peel/shear bond strength of orthodontic adhesives

1997 ◽  
Vol 25 (3-4) ◽  
pp. 263-270 ◽  
Author(s):  
G. Willems ◽  
C.E.L. Carels ◽  
G. Verbeke
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Orthodontic Adhesives

scholarly journals Shear Bond Strength of Three Orthodontic Bonding Systems on Enamel and Restorative Materials

2016 ◽  
Vol 2016 ◽  
pp. 1-10 ◽  
Author(s):  
Andreas Hellak ◽  
Jennifer Ebeling ◽  
Michael Schauseil ◽  
Steffen Stein ◽  
Matthias Roggendorf ◽  
...  
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Testing Machine ◽  
In Vitro Study ◽  
Control Group ◽  
Metal Composite ◽  
Universal Adhesive ◽  
Restorative Materials ◽  
Bonding Systems

Objective.The aim of this in vitro study was to determine the shear bond strength (SBS) and adhesive remnant index (ARI) score of two self-etching no-mix adhesives (iBond™and Scotchbond™) on different prosthetic surfaces and enamel, in comparison with the commonly used total etch system Transbond XT™.Materials and Methods. A total of 270 surfaces (1 enamel and 8 restorative surfaces,n=30) were randomly divided into three adhesive groups. In group 1 (control) brackets were bonded with Transbond XT primer. In the experimental groups iBond adhesive (group 2) and Scotchbond Universal adhesive (group 3) were used. The SBS was measured using a Zwicki 1120™testing machine. The ARI and SBS were compared statistically using the Kruskal–Wallis test (P≤0.05).Results. Significant differences in SBS and ARI were found between the control group and experimental groups.Conclusions. Transbond XT showed the highest SBS on human enamel. Scotchbond Universal on average provides the best bonding on all other types of surface (metal, composite, and porcelain), with no need for additional primers. It might therefore be helpful for simplifying bonding in orthodontic procedures on restorative materials in patients. If metal brackets have to be bonded to a metal surface, the use of a dual-curing resin is recommended.

scholarly journals INFLUÊNCIA DA MODIFICAÇÃO DA BASE DE COLAGEM E DA CONTAMINAÇÃO SALIVAR NA RESISTÊNCIA DE UNIÃO DE TUBOS ORTODÔNTICOS COLADOS AO ESMALTE HUMANO

2021 ◽  
Vol 58 (1) ◽  
pp. eUJ3657
Author(s):  
Germano Brandão ◽  
◽  
Liliana Ávila Maltagliati ◽  
Ana Carla Raphaelli Nahás-Scocate ◽  
Murilo Matias ◽  
...  
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Statistical Significance ◽  
Testing Machine ◽  
In Vitro Study ◽  
Metal Mesh ◽  
Human Teeth ◽  
Significance Level ◽  
Significant Difference

The objective of this in vitro study was to assess and compare the shear bond strength of conventional and modified orthodontic tubes bonded to the surface of dry and saliva-contaminated enamel. The sample consisted of 40 human teeth, which were randomly divided into four groups according to attachment base and presence or absence of saliva contamination as follows: Group CB, conventional orthodontic tubes without salivary contamination; Group CB-S, conventional orthodontic tubes with salivary contamination; Groups BM, orthodontic tubes modified by welding a metal mesh to their base without salivary contamination; and Group BM-S, modified orthodontic tubes with salivary contamination. Shear bond strength test was performed in a universal testing machine and analysis of the adhesive remnant index (ARI) by optical microscopy. Two-way ANOVA was used, followed by Tukey’s test at a statistical significance level of 5%. The ARI results were analysed descriptively. There was statistically significant difference between the groups regarding the shear bond strength values, with conventional tubes presenting significantly higher values (P < 0.05). In addition, the presence of salivary contamination interfered negatively with the behaviour of conventional tubes only (P < 0.05). Shear bond strength was not improved by increasing the area of the orthodontic tubes. Moreover, salivary contamination influenced negatively the SBS values, but only when conventional tubes were used.

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