The Analysis of Morphology Characteristics of Iron Plaque on the Roots of Carex cinerascens

2014 ◽  
Vol 675-677 ◽  
pp. 140-144
Author(s):  
Chun Ying Liu ◽  
Xiao Feng Gong ◽  
Ju Yun Yang
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Chemical Properties ◽  
Amorphous Coating ◽  
X Ray ◽  
Eds Analysis ◽  
Physico Chemical ◽  
Root Surfaces ◽  
Morphology Characteristics ◽  
Scanning Electron

The physico-chemical properties of iron plaques formed on the root surfaces ofCmarex cinerascensunder laboratory conditions were determined using Scanning Electron Microscopy (SEM) and Energy Dispersive X-Ray Spectrometry (EDS) analysis. Iron plaques were present as an amorphous coating on root surfaces with an uneven distribution. EDS analysis showed that iron plaques were composed of Fe , Si, Al and lesser amounts of Ca in plaqued root surfaces.

scholarly journals Scanning Electron Microscopy–Energy-Dispersive X-ray Spectrometry (SEM–EDS) Analysis of PM1–2 Microspheres Located in Coal Char Particles with Different Morphologies

2020 ◽  
Vol 34 (7) ◽  
pp. 8848-8856
Author(s):  
Elena V. Fomenko ◽  
Vladimir V. Yumashev ◽  
Sergey V. Kukhtetskiy ◽  
Anatoliy M. Zhizhaev ◽  
Alexander G. Anshits
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Coal Char ◽  
Energy Dispersive ◽  
X Ray ◽  
Eds Analysis ◽  
Scanning Electron

scholarly journals Physico-Chemical Characteristics of Shungite Rock of Kazakhstan

2013 ◽  
Vol 15 (3) ◽  
pp. 241 ◽  
Author(s):  
S.A. Efremov ◽  
S.V. Nechipurenko ◽  
M.K. Kazankapova ◽  
B. Washington ◽  
Kh.S. Tassibekov ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Physicochemical Characteristics ◽  
Chemical Characteristics ◽  
X Ray ◽  
Elementary Analysis ◽  
Physico Chemical ◽  
Developed Surface ◽  
Scanning Electron ◽  
Shungite Carbon

Physico-chemical characteristics of shugite rocks of Kazakhstan (Bakyrchik deposit) were studied using the methods of elementary analysis, IR-spectroscopy, scanning electron microscopy, Raman spectroscopy and X-ray phase analysis. The content of carbon in shungite rock was determined to be from 3% to 19%. The flotation technology for shungite rocks of Kazakhstan was developed, the content of carbon in the concentrate reaching 40.0%. When studying the elemental composition, the mineral part of shungite rocks was stated to be presented, mainly, by silicon, aluminium, calcium, magnesium, potassium, sodium, iron and titanium oxides. IR-spectroscopic investigations showed that in the concentrate, apart from polycyclic hydrocarbons containing methylene groups, there appeared carboxyl groups. The results of scanning electron microscopy (SEM) showed that flotation and thermal activation of shungite rocks on carbon allow obtaining a more developed surface structure and porosity. The structure of shungite carbon was shown by the method of Raman scattering to be close to that of glassy carbon. The results of X-ray diffraction analysis (XRD) of natural shungite rocks showed that the samples under study contained a carbonaceous substance and a number of mineral components: quartz, illite, bassanite, burgerite, muscovite. It is shown that shungite carbon of “Bakyrchik” deposit is identical to shungite of Zazhogino deposit in Russia. The stated physicochemical characteristics allow to determine the directions of the use of carbon concentrate for solution of ecological and technological problems.

scholarly journals CHARACTERISTICS OF FRAGMENTS OF SHELLS AFTER HITTING THE TRIPLEX GLASS OF THE CAR WITH SHOTS FROM A HUNTING "SAIGA" CARBINE UNDER THE CARTRIDGE 5, 45X39

2021 ◽  
Author(s):  
Sergey Leonov
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Foreign Bodies ◽  
Experimental Studies ◽  
Dispersion Analysis ◽  
Energy Dispersion ◽  
X Ray ◽  
Wooden Frame ◽  
Eds Analysis ◽  
Scanning Electron

Abstract. The article is devoted to the possibilities of innovative research methods in forensic medicine-scanning electron microscopy with energy-dispersion analysis. The described methods were used in conducting experimental studies in the case of a gunshot retrograde injury. Aim. The purpose of the work was to study the particles formed during the destruction of a semi-shell shell and an obstacle (triplex car glass) when fired from a hunting Saiga carbine with 5. 45x39 cartridges. Material and methods. Car triplex windshields from BMW and Mercedes-Benz cars were used as a barrier. The shots were fired from a hunting Saiga carbine with a 5.45x39 cartridge. The shots were fired from a distance of 10 m. As targets, white calico with dimensions of 100x150 cm was used, stretched on a wooden frame, or fixed on a chipboard. The distance between the target and the barrier was 100 cm, which roughly corresponded to the distance from the windshield of the car to the driver and the passenger in the front seat. The studies were carried out using the SEM "Hitachi FlexSem1000 II" and the energy-dispersive X-ray spectrometer "Bruker Quantax 80". Results. As a result of the conducted research with the help of microscopy, the presence of 7 types of foreign bodies on the surface of the target was established, which are the products of the destruction of the fire projectile and the barrier: glass fragments; glass fragments; crumbly deposition of glass particles; glass fragments caked with the metal of the projectile; fragments of the projectile; spherical metal particles; overlays of molten metal in the form of puddles. With the help of energy dispersion analysis, it was possible to determine the elemental composition of the particles of the barrier, the fire shell, and to identify the overlap of the target particles. Conclusion. As a result of the experimental study, it was found that the use of SEM and EDS analysis significantly increases the effectiveness and evidence-based expert research in solving the problems of causing damage through the barrier-the windscreen of modern cars. Key words: scanning electron microscopy, gunshot trauma, energy dispersion analysis, fragments of the barrier.

scholarly journals Influence of Bi2O3 on sintering and crystallization of cordierite ceramics

2005 ◽  
Vol 37 (3) ◽  
pp. 189-197 ◽  
Author(s):  
N. Djordjevic
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Liquid Phase ◽  
Binary Systems ◽  
X Ray Diffraction ◽  
X Ray ◽  
Eds Analysis ◽  
Cordierite Ceramics ◽  
Scanning Electron

The influence of Bi2O3 on the process of cordierite ceramics preparation, 2MgO-2Al2O3-5SiO2 (MAS) was investigated. The following binary systems were used for the presented research: MgO/Bi2O3 (sintered at 820?C and 1100?C), Al2O3/Bi2O3 and SiO2/Bi2O3 (sintered at 1100?C). The composition of these systems consisted of 80% of oxide and 20% Bi2O3. The effects of sintering, composition and morphology were investigated by X-ray diffraction, scanning electron microscopy and EDS analysis. It has been found that Bi2O3, besides a liquid phase, forms intermediary unstable compounds with MgO and Al2O3. MAS ceramics were sintered with 10% Bi2O3 at 1000?C, 1100?C and 1200?C. .

Characterization and Adsorption Efficiency of the Natural and the Modified Diatomite via the Low Temperature Hydrothermal Route

2012 ◽  
Vol 506 ◽  
pp. 425-428 ◽  
Author(s):  
Pusit Pookmanee ◽  
P. Thippraphan ◽  
P. Jansanthea ◽  
Sukon Phanichphant
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Low Temperature ◽  
Chemical Properties ◽  
Chemical Compositions ◽  
Adsorption Efficiency ◽  
Hydrothermal Route ◽  
X Ray ◽  
Modified Diatomite ◽  
Scanning Electron

Natural diatomite was modified by manganese chloride via the low temperature hydrothermal route. The chemical properties and adsorption efficiency of the natural and the modified diatomite were characterized. The chemical compositions of the natural and the modified diatomite were determined by X-ray fluorescence spectroscopy (XRF) and energy dispersive X-ray spectrometry (EDXS). Morphology of the natural and the modified diatomite was investigated by scanning electron microscopy (SEM). The adsorptions of Cd (II) and Pb (II) ions onto the natural and the modified diatomite were determined by atomic absorption spectroscopy (AAS).

Identification of calcium oxalate crystals in dried or fixed tobacco leaf

1984 ◽  
Vol 42 ◽  
pp. 288-289
Author(s):  
Vicki L. Baliga ◽  
Mary Ellen Counts
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Calcium Oxalate ◽  
Growth And Development ◽  
Polarized Light ◽  
Calcium Oxalate Crystals ◽  
X Ray Diffraction ◽  
X Ray ◽  
Transmission Electron ◽  
Scanning Electron

Calcium is an important element in the growth and development of plants and one form of calcium is calcium oxalate. Calcium oxalate has been found in leaf seed, stem material plant tissue culture, fungi and lichen using one or more of the following methods—polarized light microscopy (PLM), scanning electron microscopy (SEM), transmission electron microscopy (TEM) and x-ray diffraction.Two methods are presented here for qualitatively estimating calcium oxalate in dried or fixed tobacco (Nicotiana) leaf from different stalk positions using PLM. SEM, coupled with energy dispersive x-ray spectrometry (EDS), and powder x-ray diffraction were used to verify that the crystals observed in the dried leaf with PLM were calcium oxalate.

Scanning Electron Microscopy and X-Ray Analyses of Dental Tissues from a Hibernator

1976 ◽  
Vol 34 ◽  
pp. 178-179
Author(s):  
M. L. Zimny ◽  
A. C. Haller
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Body Temperature ◽  
Ground Squirrel ◽  
Alveolar Bone ◽  
X Ray ◽  
Dental Tissues ◽  
Bone Minerals ◽  
Apical Tooth ◽  
Scanning Electron

During hibernation the ground squirrel is immobile, body temperature reduced and metabolism depressed. Hibernation has been shown to affect dental tissues varying degrees, although not much work has been done in this area. In limited studies, it has been shown that hibernation results in (1) mobilization of bone minerals; (2) deficient dentinogenesis and degeneration of alveolar bone; (3) presence of calculus and tears in the cementum; and (4) aggrevation of caries and pulpal and apical tooth abscesses. The purpose of this investigation was to study the effects of hibernation on dental tissues employing scanning electron microscopy (SEM) and related x-ray analyses.

Scanning Electron Microscopy and x-ray analysis of microparticles and early hydration effects

1995 ◽  
Vol 53 ◽  
pp. 692-693
Author(s):  
Yun Lu ◽  
David C. Joy
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
High Resolution ◽  
Morphological Development ◽  
Early Hydration ◽  
X Ray ◽  
Blended Cements ◽  
Powder Particles ◽  
Chemical Wastes ◽  
Scanning Electron

High resolution scanning electron microscopy (SEM) and energy dispersive x-ray analysis (EDXA) were performed to investigate microparticles in blended cements and their hydration products containing sodium-rich chemical wastes. The physical appearance of powder particles and the morphological development at different hydration stages were characterized by using high resolution SEM Hitachi S-900 and by SEM S-800 with a EDX spectrometer. Microparticles were dispersed on the sample holder and glued by 1% palomino solution. Hydrated bulk samples were dehydrated by acetone and mounted on the holder by silver paste. Both fracture surfaces and flat cutting sections of hydrating samples were prepared and examined. Some specimens were coated with an 3 nm thick Au-Pd or Cr layer to provide good conducting surfaces. For high resolution SEM S-900 observations the accelerating voltage of electrons was 1-2 KeV to protect the electron charging. Microchemical analyses were carried out by S800/EDS equipped with a LINK detector of take-off angle =40°.

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