Microstructure Characteristics and Mechanical Properties of in-Situ Composite Steel Processed by Severe Cold-Rolling and Subsequent Annealing

2010 ◽  
Vol 168-170 ◽  
pp. 889-894
Author(s):  
Jun Zhao ◽  
Zhi Wang ◽  
Han Zhang ◽  
Hong Yan Zhai ◽  
Quan Xing Wen ◽  
...  

In this paper, Q235 steel was investigated in order to manufacturing ultra-high strength material. The process of severe cold-rolling and low temperature annealing of lath martensite effectively reduced the crystal size from about 300 nm to 20 nm, and introduced mass weak interfaces in steel, has been demonstrated a new promising technique for producing in-situ composite multi-nanolayer steel with ultra-high strength (b 2112 MPa). Cold rolling and subsequent annealing have great impact on microstructure evolution as well as material mechanical properties. In the as-rolled state, the strength is approximately four times increased than as-received material (hot-rolled state, b 515 MPa), which is attributed to work hardening and grain refining during cold rolling. As the cold-rolled sample subjected to further annealing below 500 , deformed microstructure underwent further recovery and recrystallization, finally became refined equiaxed grains, microstructure characteristics along rolling direction arrangement was decreased; In addition to ultrafine ferrite grains, nano-carbides precipitated uniformly in the specimen annealed at 500 , total elongation increased to 16%, the corresponding yield strength was 1208MPa, much higher than that of as-received samples. The phenomenon of fracture delamination was observed from the specimens, which were cold-rolled and annealed at 500 , and the delamination plane was parallel to the rolling plane. In-situ composite weak interfaces effect has great impact on the fracture surface.

2010 ◽  
Vol 667-669 ◽  
pp. 157-160
Author(s):  
Jun Zhao ◽  
Han Zhang ◽  
Yong Ming Yang ◽  
Jiu Chuan Chen ◽  
Quan Xing Wen ◽  
...  

In this paper, the process of severe cold-rolling and annealing for Q235 steel with lath martensite has demonstrated a new promising technique for producing in-situ composite multi-nanolayer steel. Cold rolling and subsequent annealing have great impact on microstructure evolution as well as mechanical properties. In the as-rolled state, the strength (b 2112 MPa) is approximately four times increased than as-received material, which is attributed to work hardening and grain refining during cold rolling. As cold-rolled sample subjected to further annealing below 500 °C, deformed microstructure underwent further recovery and recrystallization and finally became refined equiaxed grains; ultrafine ferrite grains, nano-carbides precipitated uniformly were seen in the specimen annealed at 500 °C, and the phenomenon of fracture delamination was observed from the specimens, the delamination plane was parallel to the rolling plane, in-situ composite weak interfaces effect has great impact on the fracture surface. Annealing at and above 600 °C resulted in coarse ferrite grains with spheroidized coarse carbides, causing grain growth.


2010 ◽  
Vol 152-153 ◽  
pp. 436-440
Author(s):  
Jun Zhao ◽  
Han Zhang ◽  
Zhi Wang ◽  
Hong Yan Zhai ◽  
Quan Xing Wen ◽  
...  

A new type of in-situ composite nano-multilayer plate with ultra-high strength (b 2112 MPa), Q235 steel plate with nano-layered structure of lath martensite produced by severe cold-rolling, was developed. After cold-rolling, subsequent annealing has great effect on the deformed lath morphology and grain refinement. Microstructure recrystallizing course have taken place after long time annealing at 350 °C. The recrystallization activation energy is 151 kJmol-1. Microstructure characteristics along rolling direction arrangement was decreased after annealing at 400 °C. In addition to the ultrafine ferrite grains, nano-carbides precipitated uniformly in the specimen annealed at 500 °C. Annealing at and above 600 °C resulted in coarse ferrite grains with spheroidized coarse carbides, causing grain growth. The average crystal size is about 4.7 m after annealing for 60 min at 600 °C.


2021 ◽  
Vol 904 ◽  
pp. 143-147
Author(s):  
You Yang ◽  
Hong Shuai Li ◽  
Yu Xin Huang

The effects of different cold rolling deformations on the microstructure and mechanical properties of high nitrogen and low nickel alloys were investigated. The microstructure of high nitrogen alloys with different rolling deformations were characterized by EBSD and TEM. The tensile mechanical properties of the high nitrogen alloys at room temperature were tested. The results showed that the microstructure of the cold rolled high nitrogen alloy with deformation of 0% to 70% shows a twinning process. The twin thickness of the high nitrogen alloy without deformation is micron degree. When the rolling deformation is over 50%, the average thickness of the deformation twin is 23nm. When the rolling deformation increases to 70%, the average thickness of the twin is 14nm. When the rolling deformation increases from 0% to 70%, the cold rolled high nitrogen alloy exhibits high strength (1001-2236 MPa) and excellent plasticity (5.9%-64.1%). It is beneficial to have a good combination of strength and plasticity after rolling deformation.


2009 ◽  
Vol 83-86 ◽  
pp. 16-23 ◽  
Author(s):  
H. Shirazi ◽  
Mahmoud Nili-Ahmadabadi ◽  
A. Fatehi ◽  
S. Hossein Nedjad

Fe-Ni-Mn martensitic steels show excellent age hardenability but suffer from embrittlement after aging. Discontinuous coarsening of grain boundary precipitates was found as the main source of embrittlement. Effect of cold rolling and equal channel angular pressing on the mechanical properties of an Fe-10Ni-7Mn steel was investigated. Cold rolling for 20%, 40%, 60%, 80% and 90% and equal channel angular pressing for four passes through the Bc route were carried out on a solution annealed material with subsequent aging at 753 K. Hardness measurement, tensile test and scanning electron microscopy were used to study mechanical properties and microstructural features of the as-deformed and aged alloys. Improvement in tensile properties of the as-deformed and aged alloys was found. A tensile strength of about 1840 MPa along with 3% elongation were determined for cold rolled by 90% thickness reduction and aged alloy, while conventional steel shows a premature fracture stress of 820 MPa with zero ductility. It was also indicated that after heavy cold rolling ductility increases in comparison to the equal channel angular pressed and aged alloy.


Materials ◽  
2019 ◽  
Vol 12 (9) ◽  
pp. 1478 ◽  
Author(s):  
Zhaoxin Du ◽  
Yan Ma ◽  
Fei Liu ◽  
Ning Xu ◽  
Yanfei Chen ◽  
...  

The influences of process annealing temperature during cold rolling on microstructure and mechanical properties of Ti-3.5Al-5Mo-6V-3Cr-2Sn-0.5Fe near β high strength titanium alloy sheets have been investigated. Results showed that the alloy mainly included the deformation induced dislocation structures after cold rolling but no obvious band structure, twin crystal or martensite were observed in this work. The texture components, which were affected by process annealing, are mainly γ-fiber, α-fiber and weak Goss texture. The γ-fiber of alloy when process annealed at 780 °C (α/β phase field) is stronger than at 830 °C (β phase field), where the Goss texture of alloy with process annealing temperature of 830 °C is more obvious. Results of annealing heat treatments showed that the recrystallization of the cold rolled was basically completed in a relatively short time of 2 min at 750 °C for 2 min. The refinement of grain size led to a significant increase of plasticity compared to rolled alloy. Results of tensile testing of aged alloy display the excellent combination of strength and plasticity, and the cold rolled alloy with process annealed at α/β phase field exhibits the better mechanical properties than at β phase field.


2016 ◽  
Vol 34 (1) ◽  
pp. 142-147 ◽  
Author(s):  
Junting Zhang ◽  
Xiaochao Cui ◽  
Jiankai Ma ◽  
Youhong Wang

AbstractCu–Sn–Fe alloys with different compositions were developed by casting, normalizing treatment, cold roll and subsequent annealing treatment. The results showed that the tensile strength and resistivity of the Cu–xSn–xFe alloys (where x represents wt.%) improved with increasing the content of Sn and Fe. Compared with the as-cast alloys, the resistivity and tensile strength of the Cu–xSn–xFe alloys after normalizing and cold rolling treatment increased. In addition, the resistivity and mechanical properties of the alloys after the annealing treatment were improved significantly. Finally, a conclusion could be drawn that the annealed Cu–2Sn–5Fe alloy had good mechanical properties and resistivity, and the values of the tensile strength, mechanical elongation and resistivity reached 552 MPa, 32 % and 1.92 μΩ cm, respectively.


2014 ◽  
Vol 915-916 ◽  
pp. 654-659
Author(s):  
Guo Liang Xie ◽  
Qiang Song Wang ◽  
Qing Miao Guo ◽  
Xu Jun Mi ◽  
Bai Qing Xiong

A Cu-24 wt % Ag composite alloy is prepared to reveal the evolutions of microstructures, mechanical properties and textures formed by cold rolling. A typical alternating distribution of Cu and Ag phase layers is observed, which becomes much finer with increasing cold rolling reduction. Copper texture ((112)<11-1> texture) and Goss texture ((110)<001> texture) with high intensities are found in the Cu phase of cold rolled samples. Ag phase containing strong Goss texture and weak Brass texture are observed, quite different from the case in cold rolled pure Ag. Significant change of textures, from the Goss texture to (111) textures with increasing rolling reduction, has been found of Ag phase. The strengthening mechanism of this Cu-Ag composite is described by a equation similar to the HallPetch relationship, the fitted results based on which shows good agreement with the experimental data when the layer thickness is lower than 100-200 nm.


2016 ◽  
Vol 849 ◽  
pp. 376-381
Author(s):  
Ming Long Li ◽  
Yu Jie Geng ◽  
Chen Chen ◽  
Shu Jie Pang ◽  
Tao Zhang

The effects of cold-rolling with different reduction ratios of 70%-90% on the microstructure and mechanical properties of Ti50Zr30Nb10Ta10 alloy were investigated. It was found that the β-Ti phase in this alloy was stable under cold-rolling. With the increase in reduction ratio from 70% to 90%, the microstructure of the alloys evolved from deformed dendrite structure to fiber-like structure. The alloy cold-rolled with the reduction ratio of 70% exhibited optimum mechanical properties of combined high fracture strength of 1012 MPa and plastic strain of 10.1%, which are closely correlated with the dendrite structure of the alloy. It is indicated that the proper cold-rolling is an effective way to improve the mechanical properties of the titanium alloy.


2008 ◽  
Vol 579 ◽  
pp. 15-28 ◽  
Author(s):  
Carl C. Koch ◽  
Khaled M. Youssef ◽  
Ron O. Scattergood

This paper reviews a method, “in situ consolidation ball milling” that provides artifactfree bulk nanocrystalline samples for several ductile metals such as Zn, Al and Al alloys, and Cu and Cu alloys. The preparation method is described in this paper and examples of the mechanical behavior of nanocrystalline materials made by this technique are given. It is found that in such artifact-free metals, combinations of both high strength and good ductility are possible.


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