A New Method for Nondestructive Evaluation of Mechanical Properties Using Instrumented Indentation Technique

2007 ◽  
Vol 26-28 ◽  
pp. 1239-1242
Author(s):  
Kyung Woo Lee ◽  
Kug Hwan Kim ◽  
Kwang Ho Kim ◽  
Dong Il Kwon

The development of the instrumented indentation test (IIT), which gives accurate measurements of the continuous variation in indentation load as a function of depth, has paved the way to assessing tensile properties and residual stress in addition to hardness by analyzing the indentation load-depth curve. In this study, analytic models and procedures are presented for evaluating tensile flow properties and residual stress states using IIT. Tensile properties were obtained by defining representative stress and strain beneath the spherical indenter. The evaluation of residual stress is based on the concepts that the deviatoric stress part of the residual stress affects the indentation load-depth curve, and that analyzing the difference between the residual stressinduced indentation curve and the residual stress-free curve permits evaluation of the quantitative residual stress in a target region.

Author(s):  
Dongil Kwon ◽  
Jung-Suk Lee ◽  
Kwang-Ho Kim ◽  
Afshin Motarjemi ◽  
Julian Speck

The weld joints in structural components have long been considered important sites for safety and reliability assessment. In particular, the residual stress in piping weldments induced by the welding process must be evaluated accurately before and during service. This study reports an indentation technique for evaluating welding residual stress nondestructively. Indentation load-depth curves were found to shift with the magnitude and direction of the residual stress. Nevertheless, contact depths in the stress-free and stressed states were constant at a specific indentation load. This means that residual stress induces additional load to keep contact depth constant at the same load. By taking these phenomena into account, welding residual stress was obtained directly from the indentation load-depth curve. In addition, the results were compared with values from the conventional hole-drilling and saw-cutting method.


2005 ◽  
Vol 297-300 ◽  
pp. 2122-2127 ◽  
Author(s):  
Yeol Choi ◽  
Yun Hee Lee ◽  
Jae Il Jang ◽  
Sang Ki Park ◽  
Kwang Ho Kim ◽  
...  

The weld joints in power-plant pipelines have long been considered important sites for safety and reliability assessment. In particular, the residual stress in pipeline weldments induced by the welding process must be evaluated accurately before and during service. This study reports an indentation technique for evaluating welding residual stress nondestructively. Indentation load-depth curves were found to shift with the magnitude and direction of the residual stress. Nevertheless, contact depths in the stress-free and stressed states were constant at a specific indentation load. This means that residual stress induces additional load to keep contact depth constant at the same load. By taking these phenomena into account, welding residual stress was obtained directly from the indentation load-depth curve. In addition, the results were compared with values from the conventional hole-drilling and saw-cutting methods.


Author(s):  
Dongil Kwon ◽  
Min-Jae Choi ◽  
Kug-Hwan Kim ◽  
Kyung-Woo Lee ◽  
Kwang-Ho Kim

The instrumented indentation technique has taken the limelight as a promising alternative to conventional residual stress measurement methods for welds with rapid microstructural gradients because of its easy and nondestructive testing procedure. The technique is based on the key concept that the deviatoric-stress part of residual stress affects the indentation load-depth curve. By analyzing the difference between the residual stress-induced curve and residual stress-free curve, the quantitative residual stress of the target region can be evaluated. To determine the stress-free curve of the target region, we take into consideration microstructural changes that accommodate strength differences. In addition, we determine the ratio of the non-equibiaxial residual stress by using an asymmetric Knoop indenter, which has an elongated four-sided pyramidal geometry. We find that the load-depth curve is changed on penetration direction of the long diagonal for Knoop indenter, and derive a quantitative relation between the stress ratio and the load difference through both theoretical analysis and experiments. Finally, indentation tests and conventional tests were performed on the welded zone to verify the applicability of the technique. The estimated residual stress values obtained from instrumented indentation technique agreed well with those from conventional tests.


Author(s):  
Sungki Choi ◽  
Jong Hyoung Kim ◽  
Jun Sang Lee ◽  
Kyungyul Lee ◽  
Min-Jae Choi ◽  
...  

Residual stress is a major factor in failure and fracture in structures or electronic components. Various testing methods are used to measure residual stress: there are saw-cutting, holedrilling, X-ray diffraction and layer-removing methods. In particular, instrumented indentation testing (IIT) has many advantages: it is a simple and non-destructive procedure that can be used for in-field testing. In previous research, we proposed an algorithm for evaluating the magnitude and directionality of residual stress using an asymmetric Knoop indenter with long and short axes in the ratio 7.11:1. Indenting in different directions with a Knoop indenter creates different indentation load-depth curves depending on the residual stress state. In addition, the directionality of the residual stress can be expressed as a function of the load difference ratio calculated from these load-depth curves. However, When the Knoop indentation test is performed at small indentation depths, experimental issues such as surface preparation or indentation normality can become significant as the load difference decreases. In order to solve these issues, we introduce a wedge indenter, that makes it possible to select the edge length independent of indentation depth. We can thus decrease indent size when working in a small testing area. The load difference between the stress-free and stressed state is related to the sensitivity of residual stresses, and a wedge indenter can maximize the sensitivity to residual stress. In this study, we suggest a way to use the wedge indenter and verify the model using cruciform bending specimens and finite element analysis.


2007 ◽  
Vol 345-346 ◽  
pp. 1125-1128 ◽  
Author(s):  
Jae Hwan Han ◽  
Jung Suk Lee ◽  
Yun Hee Lee ◽  
Min Jae Choi ◽  
Gyu Jei Lee ◽  
...  

The instrumented indentation technique (IIT) has recently attracted significant research interest because it is nondestructive and easy to perform, and can characterize materials on local scales. Residual stress can be determined by analyzing the indentation load-depth curve from IIT. However, this technique using a symmetric indenter is limited to an equibiaxial residual stress state. In this study, we determine the directionality of the non-equibiaxial residual stress by using the Knoop indentation technique. Different indentation load-depth curves are obtained at nonequibiaxial residual stresses depending on the Knoop indentation direction. A model for Knoop indentation was developed through experiments and theoretical analysis.


2000 ◽  
Vol 657 ◽  
Author(s):  
Youngman Kim ◽  
Sung-Ho Choo

ABSTRACTThe mechanical properties of thin film materials are known to be different from those of bulk materials, which are generally overlooked in practice. The difference in mechanical properties can be misleading in the estimation of residual stress states in micro-gas sensors with multi-layer structures during manufacturing and in service.In this study the residual stress of each film layer in a micro-gas sensor was measured according to the five difference sets of film stacking structure used for the sensor. The Pt thin film layer was found to have the highest tensile residual stress, which may affect the reliability of the micro-gas sensor. For the Pt layer the changes in residual stress were measured as a function of processing variables and thermal cycling.


Author(s):  
Seung-Kyun Kang ◽  
Young-Cheon Kim ◽  
Chan-Pyoung Park ◽  
Dongil Kwon

Understanding the property distribution in the weld zone is very important for structural safety, since deformation and fracture begin at the weakest point. However, conventional tensile tests can measure only average material properties because they require large specimens. Small-scale tests are being extensively researched to remove this limitation, among such tests, instrumented indentation test (IIT) are of great interest because of their simple procedures. Here we describe the evaluation of tensile properties using IIT and a representative stress-strain approach. The representative stressstrain method, introduced in 2008 in ISO/TR29381, directly correlates the stress and strain under the indenter to the true stress and strain of tensile testing by defining representative functions. Using this technique, we successfully estimate the yield strength and tensile strength of structural metallic materials and also obtain profiles of the weld-zone tensile properties.


Author(s):  
Dongil Kwon ◽  
Jong Hyoung Kim ◽  
Ohmin Kwon ◽  
Woojoo Kim ◽  
Sungki Choi ◽  
...  

The instrumented indentation technique (IIT) is a novel method for evaluating mechanical properties such as tensile properties, toughness and residual stress by analyzing the indentation load-depth curve measured during indentation. It can be applied directly on small-scale and localized sections in industrial structures and structural components since specimen preparation is very easy and the experimental procedure is nondestructive. We introduce the principles for measuring mechanical properties with IIT: tensile properties by using a representative stress and strain approach, residual stress by analyzing the stress-free and stressed-state indentation curves, and fracture toughness of metals based on a ductile or brittle model according to the fracture behavior of the material. The experimental results from IIT were verified by comparing results from conventional methods such as uniaxial tensile testing for tensile properties, mechanical saw-cutting and hole-drilling methods for residual stress, and CTOD test for fracture toughness.


Author(s):  
Eun-chae Jeon ◽  
Joo-Seung Park ◽  
Doo-Sun Choi ◽  
Kug-Hwan Kim ◽  
Dongil Kwon

The instrumented indentation test, which measures indentation tensile properties, has attracted interest recently because this test can replace uniaxial tensile test. An international standard for instrumented indentation test has been recently legislated. However, the uncertainty of the indentation tensile properties has never been estimated. The indentation tensile properties cannot be obtained directly from experimental raw data as can the Brinell hardness, which makes estimation of the uncertainty difficult. The simplifying uncertainty estimation model for the indentation tensile properties proposed here overcomes this problem. Though the influence quantities are generally defined by experimental variances when estimating uncertainty, here they are obtained by calculation from indentation load-depth curves. This model was verified by round-robin test with several institutions. The average uncertainties were estimated as 18.9% and 9.8% for the indentation yield strength and indentation tensile strength, respectively. The values were independent of the materials’ mechanical properties but varied with environmental conditions such as experimental instruments and operators. The uncertainties for the indentation yield and tensile strengths were greater than those for the uniaxial tensile test. These larger uncertainties were caused by measuring local properties in the instrumented indentation test. The two tests had the same tendency to have smaller uncertainties for tensile strength than yield strength. These results suggest that the simplified model can be used to estimate the uncertainty in indentation tensile properties.


2013 ◽  
Vol 586 ◽  
pp. 31-34 ◽  
Author(s):  
Petr Haušild ◽  
Aleš Materna ◽  
Jiri Nohava

The most commonly used method for the analysis of instrumented indentation test (Oliver-Pharr) is based on isotropic elastic solution of contact problem which is not necessarily valid when indenting at the scale of one (anisotropic) grain. In this paper, we performed the grid indentation method at the sub-micron scale (at low indentation load and depth of penetration) on an area containing several grains with different crystallographic orientation which was simultaneously characterized by electron back-scattered diffraction. Measured dependencies of hardness and indentation modulus on crystallographic orientation were compared with analytical solution and finite element simulations.


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