Study on Preparation and Near-Infrared Reflective Properties of NaZnPO4

2011 ◽  
Vol 399-401 ◽  
pp. 1289-1293
Author(s):  
Ming Feng Zhong ◽  
Wen Xiang Fu ◽  
Wang Da ◽  
Da Gen Su
Keyword(s):  
Heat Treatment ◽  
Near Infrared ◽  
Raw Materials ◽  
Heat Treating ◽  
Treatment Temperature ◽  
Precipitation Method ◽  
Anhydrous Sodium Carbonate ◽  
Reflection Property ◽  
Infrared Reflection ◽  
Co Precipitation

NaZnPO4was prepared by heat-treating precursor with Zn(NO3)2٠6H2O、H3PO4and anhydrous sodium carbonate as raw materials by co-precipitation method, and it was characterized with UV/VIS spectrophotometer、X-ray diffraction (XRD). The experiment results shown that the near-infrared reflection property of NaZnPO4was very good. when the heat treatment temperature of preparation of NaZnPO4was range from 400°C to 800°C, near-infrared reflection properties of products were similar. Among them, the products with the heat treatment of 600°C has the best near-infrared reflection property,which is reached up to 95.2% in average,while the near-infrared reflection of TiO2is 74.1% in average.

Synthesis of pigments in Fe2O3-Al2O3-CoO by co-precipitation method

2017 ◽  
Vol 46 (5) ◽  
pp. 356-361 ◽  
Author(s):  
Liliya Frolova ◽  
Alexander Pivovarov ◽  
Tatyana Butyrina
Keyword(s):  
Heat Treatment ◽  
Phase Composition ◽  
Treatment Temperature ◽  
Precipitation Method ◽  
Colour Properties ◽  
X Ray Diffraction ◽  
Content Type ◽  
Composition Property ◽  
Yellow Pigments ◽  
Co Precipitation

Purpose The purpose of this work is to study the patterns of pigment colour formation and to develop metal compositions for obtaining spinels using the precipitation and heat treatment methods. Design/methodology/approach Precursor materials were prepared using co-precipitation method. Phase composition of pigments were determined by X-ray diffraction. Colour of pigments was determined spectrophotometry. Modelling of colour formation was performed using simplex method. Planning in the future to carry out full synthesis of pigments of blue, red and yellow colours. Findings The paper deals with the results of theoretical and experimental research on the synthesis pigments of blue, red and yellow colours based on Fe-Co-Al-O spinel. The influence of the chromophore cation content and the heat treatment temperature on optical and colour characteristics of pigments were studied. Originality/value The resulting composition-property diagrams make it possible to evaluate the effect of chromophore cations and heat treatment on the colour formation for Fe2O3-Al2O3-CoO system. Crystal-phase composition of the pigments is installed and its relationship with the optical colour characteristics. That makes it possible carry out targeted synthesis of pigments blue, red and yellow colours in further. The phase composition of pigments and its relationship with optical and colour properties has been established thus enabling the directed synthesis of blue, red and yellow pigments.

BÖHLER W403 VMR

Alloy Digest ◽  
2013 ◽  
Vol 62 (9) ◽  
Keyword(s):  
Heat Treatment ◽  
Chemical Composition ◽  
Physical Properties ◽  
Tool Steel ◽  
Raw Materials ◽  
Heat Treating ◽  
Diffusion Annealing ◽  
Selection Of

Abstract Böhler (or Boehler) W403 VMR is a tool steel with outstanding properties, based not only on a modified chemical composition, but on the selection of highly clean raw materials for melting, remelting under vacuum (VMF), optimized diffusion annealing, and a special heat treatment. This datasheet provides information on composition, physical properties, and elasticity. It also includes information on forming and heat treating. Filing Code: TS-721. Producer or source: Böhler Edelstahl GmbH.

Novel Fe3O4/HNT@rGO composite via a facile co-precipitation method for the removal of contaminants from aqueous system

RSC Advances ◽  
2016 ◽  
Vol 6 (54) ◽  
pp. 49228-49235 ◽  
Author(s):  
Chengwei Gao ◽  
Baojun Li ◽  
Ning Chen ◽  
Jie Ding ◽  
Qiang Cai ◽  
...  
Keyword(s):  
Heat Treatment ◽  
Water Treatment ◽  
Potential Application ◽  
High Performance ◽  
Aqueous System ◽  
Precipitation Method ◽  
Precipitation Process ◽  
System P ◽  
Removal Of Contaminants ◽  
Co Precipitation

Fe3O4/HNT@rGO composite (FHGC) was fabricated via a facile co-precipitation process, followed by heat treatment. For RhB and As5+removal, the high performance and easy separation of FHGC highlight its potential application in water treatment.

Preparation and Electrochemical Performance of Mn3O4/GR Composites Electrode Material in Supercapacitors

2019 ◽  
Vol 807 ◽  
pp. 50-56
Author(s):  
Yun Long Zhou ◽  
Zhi Biao Hu ◽  
Li Mei Wu ◽  
Jiao Hao Wu
Keyword(s):  
Room Temperature ◽  
Raw Materials ◽  
Precipitation Method ◽  
Electrochemical Performances ◽  
Manganese Sulfate ◽  
X Ray Diffraction ◽  
X Ray ◽  
Co Precipitation ◽  
A Current ◽  
Discharge Test

Using hydrated manganese sulfate and general type graphene (GR) as raw materials, Mn3O4/GR composite has been successfully prepared by the liquid phase chemical co-precipitation method at room temperature. X-ray diffraction (XRD) was used to investigate the phase structure of Mn3O4powder and Mn3O4/GR composite; The electrochemical performances of the samples were elucidated by cyclic voltammetry and galvanostatic charge-discharge test in 0.5 mol/L Na2SO4electrolyte. The results show that the Mn3O4/GR composite possesses graphene phase and good reversibility; the composite also displays a specific capacitance of 318.8 F/g at a current density of 1 A/g.

Synthesis and Properties of Cerium Oxide Nanoparticles

2011 ◽  
Vol 299-300 ◽  
pp. 118-121 ◽  
Author(s):  
Yong Li ◽  
Jin Gui He ◽  
Xiao Wei Huang
Keyword(s):  
Cerium Oxide ◽  
Raw Materials ◽  
Morphological Characteristics ◽  
Treatment Temperature ◽  
Precipitation Method ◽  
Thermal Treatment Temperature ◽  
X Ray ◽  
Structure And Morphology ◽  
Dispersing Agent ◽  
Scanning Electron

Cerium oxide(CeO2)nanoparticles were synthesized via a precipitation method using cerous sulfate, ammonia water and cetyl three methyl brominated ammoniu(CTAB) as raw materials. The effect of thermal treatment temperature and dispersing agent on the crystal structure and morphology were discussed. The structural evolutions and morphological characteristics of the nanoparticles were investigated using X-ray diffractometery, scanning electron microscopy, Fourier transform infrared spectroscopy. The results showed that the broadening of CeO2peaks decreases by the increasing in heat-treatment temperature and the dispersing agent playes key roles in microstructure of the CeO2.

Preparation and Impaction on the Yield and Abrasion Resistance of Polycrystalline Diamond Powder of Copper/Graphite Raw Materials

2012 ◽  
Vol 550-553 ◽  
pp. 93-98
Author(s):  
Chun Lin Li ◽  
Jian Chen
Keyword(s):  
Heat Treatment ◽  
Particle Size ◽  
Abrasion Resistance ◽  
Heat Treatment Temperature ◽  
Copper Content ◽  
Raw Materials ◽  
Polycrystalline Diamond ◽  
Graphite Powder ◽  
Diamond Powder ◽  
Treatment Temperature

Taking earthy graphite and electrolytic powder as raw materials, copper/graphite raw material is prepared by power metallurgy and then polycrystalline diamond powder is prepared by shock wave synthesis. Impaction on yield and abrasion resistance from copper content, particle size of graphite powder, heat treatment and re-pressing process has been researched. As result, yield of polycrystalline diamond powder is decreasing as decreasing copper content. It is decreased dramatically when the copper content is less than 90%. It is increased and then decreased as increasing the particle size of graphite powder, and the better particle size of graphite powder is 70μm. It is increased slightly and then decreased dramatically as increasing heat treatment temperature before re-pressing. The higher the heat treatment temperature, the more the yield after re-pressing. Impaction on the abrasion resistance of polycrystalline diamond powder from the preparing process of copper/graphite is smaller.

Study on the Characterization of Zinc Ferrite High-Temperature Coal Gas Desulfurization Agent

2010 ◽  
Vol 129-131 ◽  
pp. 1233-1237
Author(s):  
Hong Yan Xu ◽  
Mei Sheng Liang ◽  
Chun Hu Li
Keyword(s):  
Zinc Ferrite ◽  
Raw Materials ◽  
Particle Diameter ◽  
Textural Properties ◽  
Zinc Nitrate ◽  
Gas Absorption ◽  
Precipitation Method ◽  
Ferric Nitrate ◽  
The One ◽  
Co Precipitation

Using ferric nitrate, zinc nitrate, ammonia liquor and binder as main raw materials, five kinds of zinc ferrite sorbents were prepared by the co-precipitation method. The effects of the different binders on the structure and texture of zinc ferrite sorbents were investigated. The morphology, composite structure, pore properties, and mechanical strength were studied by using modern several physicochemical techniques such as powder X-ray diffraction (XRD), scanning electronic microscopy (SEM), strength tester and gas absorption meter. It is showed that spinel structure ZnFe2O4 is not affected by different binders，and its particle diameter is in micron leve1. The spinel structures are present in the sorbents that have been calcined at 750 0C.. The sorbent employed kaolinite as binder is the best one of the five types of sorbents for desulfurization, while the one employed diatomite is the worst.Different binders modify the textural properties, modifying consequently the sorbent reactivity. Furthermore, the reactivity and sulfur capacity of sorbents are increasing with an increase in the pore volume.

Influence of Zinc Substitution on Hydroxyapatite Structure Prepared by Chemical Precipitation Method

2018 ◽  
Vol 879 ◽  
pp. 3-7 ◽  
Author(s):  
Nisakorn Nuamsrinuan ◽  
Patcharin Naemchanthara ◽  
Pichet Limsuwan ◽  
Kittisakchai Naemchanthara
Keyword(s):  
Heat Treatment ◽  
Fourier Transforms ◽  
Chemical Precipitation ◽  
Zinc Nitrate ◽  
Treatment Temperature ◽  
Chemical Precipitation Method ◽  
Precipitation Method ◽  
Phosphate Phase ◽  
Chicken Eggshell ◽  
Hydroxyapatite Phase

The zinc (Zn) substituted hydroxyapatite were synthesized using a chemical precipitation method. The chemical precursors were prepared from di-ammonium hydrogen orthophosphate, calcium oxide (CaO) derived from chicken eggshell and zinc nitrate (Zn(NO3)2). The Zn(NO3)2contents in the prepared samples were varied from 1 to 25 %wt of CaO. The Zn substituted hydroxyapatite were heated at the various temperatures from 200 to 1300 °C in the furnace with an incremental temperature of 100 °C. The crystal structure, function group and morphology of sample were analyzed by X-ray diffraction (XRD), Fourier transforms infrared spectroscopy (FTIR) and field emission scanning electron microscopy (FESEM), respectively. The results show that the hydroxyapatite doped Zn was a hydroxyapatite phase as well as pure hydroxyapatite. The crystalline size of sample decreased with increasing the Zn content. And, the crystallinity of hydroxyapatite phase was increased following by increasing heat treatment temperature. However, the amount of Zn has the effect on phase transformation of hydroxyapatite phase after heat treatment. Zn concentration accelerates hydroxyapatite transforms to β-tricalcium phosphate phase.

Synthesis of Y3Al5-xFexO12 Nanopowder by the Co-Precipitation Method: Influence of Precipitate Agent

2013 ◽  
Vol 341-342 ◽  
pp. 114-118
Author(s):  
Min Zeng ◽  
Yun Hong Wang
Keyword(s):  
Phase Formation ◽  
Formation Process ◽  
Raw Materials ◽  
Precipitation Method ◽  
Precipitation Technique ◽  
Pure Phase ◽  
Co Precipitation ◽  
Carbonate Precursor ◽  
Phase Formation Process

The Y3Al5-xFexO12 (0x5, YAIG) powders have been prepared by co-precipitation technique in which NH4HCO3 or (NH4)2CO3 is used as a precipitant and Y(NO3)3·6H2O, Al (NO3)3·9H2O and Fe (NO3)3·9H2O as raw materials. The composition of YAIG precursor, the phase formation process of YAIG and the properties of the powders were investigated by means of XRD, SEM, TEM and EDS. The results indicated that the precipitant effects the preparation of pure-phase YAIG powders. AC as precipitant could produce a hydroxide precursor, which transformed to a mixture. AHC as precipitant could produce a loosely agglomerated carbonate precursor. The resultant YAIG powders showed good dispersity and excellent sinterability.

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