Synthesis of Porous Cubic Nickel Oxide Nanostructures and their Electrochemical Property

2012 ◽  
Vol 557-559 ◽  
pp. 628-631
Author(s):  
Shao Mei Wang ◽  
Huan Pang ◽  
Hang Zhang ◽  
Ya Hui Ma ◽  
Xue Xue Li ◽  
...  
Keyword(s):  
Nickel Oxide ◽  
Specific Capacitance ◽  
Electrochemical Property ◽  
Structure Characterization ◽  
Simple Method ◽  
Oxide Nanostructures ◽  
Morphology And Structure

Monodispersed porous cubic nickel oxide nanostructures have been synthesized by a simple method. TEM have been employed for the morphology and structure characterization. Electrochemical data prove that the monodispersed porous cubic nickel oxide nanostructures contain a good specific capacitance.

Cubic-Like Nickel Oxide Nanostructures as Large Specific Capacitance and Long-Life Supercapacitors

2012 ◽  
Vol 516-517 ◽  
pp. 1688-1691 ◽  
Author(s):  
Jia Wei Deng ◽  
Huan Pang ◽  
Shao Mei Wang ◽  
Jiang Shan Zhang
Keyword(s):  
Nickel Oxide ◽  
Specific Capacitance ◽  
High Performance ◽  
Structure Characterization ◽  
Simple Method ◽  
Oxide Nanostructures ◽  
Morphology And Structure ◽  
Long Life ◽  
Charge Discharge

Monodispersed anamorphic cubic NiO materials have been synthesized by a simple method. SEM, TEM and XRD have been employed for the morphology and structure characterization. The calcination conditions have been carefully studied about their effects on supercapacitor properties. Electrochemical data prove that the monodispersed nano anamorphic cubic NiO materials contain a good specific capacitance and excellent specific capacitance retention after 2000 continuous charge-discharge cycles. These results suggest that both the morphology and structure have important effects on the high performance supercapacitors.

scholarly journals Tuning the hierarchical pore structure of graphene oxide through dual thermal activation for high-performance supercapacitor

2021 ◽  
Vol 11 (1) ◽  
Author(s):  
Jeongpil Kim ◽  
Jeong-Hyun Eum ◽  
Junhyeok Kang ◽  
Ohchan Kwon ◽  
Hansung Kim ◽  
...  
Keyword(s):  
Graphene Oxide ◽  
Pore Structure ◽  
Specific Capacitance ◽  
Surface Area ◽  
Thermal Annealing ◽  
High Performance ◽  
Annealing Process ◽  
Supercapacitor Electrode ◽  
Simple Method ◽  
Surface Areas

AbstractHerein, we introduce a simple method to prepare hierarchical graphene with a tunable pore structure by activating graphene oxide (GO) with a two-step thermal annealing process. First, GO was treated at 600 °C by rapid thermal annealing in air, followed by subsequent thermal annealing in N2. The prepared graphene powder comprised abundant slit nanopores and micropores, showing a large specific surface area of 653.2 m2/g with a microporous surface area of 367.2 m2/g under optimized conditions. The pore structure was easily tunable by controlling the oxidation degree of GO and by the second annealing process. When the graphene powder was used as the supercapacitor electrode, a specific capacitance of 372.1 F/g was achieved at 0.5 A/g in 1 M H2SO4 electrolyte, which is a significantly enhanced value compared to that obtained using activated carbon and commercial reduced GO. The performance of the supercapacitor was highly stable, showing 103.8% retention of specific capacitance after 10,000 cycles at 10 A/g. The influence of pore structure on the supercapacitor performance was systematically investigated by varying the ratio of micro- and external surface areas of graphene.

scholarly journals Pore system changes of damaged Brazilian oxisols and nitosols induced by wet-dry cycles as seen in 2-D micromorphologic image analysis

2009 ◽  
Vol 81 (1) ◽  
pp. 151-161 ◽  
Author(s):  
Luiz F. Pires ◽  
Klaus Reichardt ◽  
Miguel Cooper ◽  
Fabio A.M. Cássaro ◽  
Nivea M.P. Dias ◽  
...  
Keyword(s):  
Image Analysis ◽  
Size Distribution ◽  
Soil Structure ◽  
Tropical Soils ◽  
Transport Processes ◽  
Structure Characterization ◽  
Control Treatment ◽  
Simple Method ◽  
Wetting And Drying ◽  
Essential Information

Soil pore structure characterization using 2-D image analysis constitutes a simple method to obtain essential information related to soil porosity and pore size distribution (PSD). Such information is important to infer on soil quality, which is related to soil structure and transport processes inside the soil. Most of the time soils are submitted to wetting and drying cycles (W-D), which can cause important changes in soils with damaged structures. This report uses 2-D image analysis to evaluate possible modifications induced by W-D cycles on the structure of damaged soil samples. Samples of three tropical soils (Geric Ferralsol, GF; Eutric Nitosol, EN; and Rhodic Ferralsol, RF) were submitted to three treatments: 0WD, the control treatment in which samples were not submitted to any W-D cycle; 3WD and 9WD with samples submitted to 3 and 9 consecutive W-D cycles, respectively. It was observed that W-D cycles produced significant changes in large irregular pores of the GF and RF soils, and in rounded pores of the EN soil. Nevertheless, important changes in smaller pores (35, 75, and 150 µm) were also observed for all soils. As an overall consideration, it can be said that the use of image analysis helped to explain important changes in soil pore systems (shape, number, and size distribution) as consequence of W-D cycles.

Ferrous Nitrate–Nickel Oxide (Fe(NO3)2–NiO) Nanospheres Incorporated With Carbon Black and Polyvinylidenefluoride for Supercapacitor Applications

2019 ◽  
Vol 16 (3) ◽  
Author(s):  
Aqib Muzaffar ◽  
Keerthana Muthusamy ◽  
M. Basheer Ahamed
Keyword(s):  
Nickel Oxide ◽  
Specific Capacitance ◽  
Double Layer ◽  
Electrochemical Impedance ◽  
Maximum Efficiency ◽  
Potential Range ◽  
Double Layer Capacitance ◽  
Hydrothermal Route ◽  
Sem Images ◽  
Charge Discharge

Ferrous nitrate/nickel oxide {Fe(NO3)2–NiO} nanocomposite was synthesized via two-step facile hydrothermal route. The nanocomposite exhibits crystalline structure as unveiled by X-ray diffraction (XRD) pattern, while as the scanning electron microscope (SEM) images divulge spherical morphologies for both Fe(NO3)2 as well as NiO nanoparticles differentiating from each other in size. Cyclic voltammetry (CV), galvanostatic charge–discharge (GCD), and electrochemical impedance spectroscopy (EIS) techniques were used to investigate supercapacitive behavior of the symmetrically fabricated nanocomposite electrode configuration using aqueous KOH as the electrolyte. The CV analyses demonstrate dominant electrical double layer capacitance (EDLC) behavior in the potential range of 0–1 V. From charge–discharge curves, the maximum specific capacitance calculated was 460 F g−1 corresponding to the energy density of 16 W h kg−1 at a high power density of 250 W kg−1. EIS data affiliate well with the CV and GCD results justifying the maximum contribution of specific capacitance due to double layer capacitance. The nanocomposite retained 84% of its original capacitance after 1000 cycles and yielded maximum efficiency of 78%.

A Facile Synthesis of NiFe2O4 with High Specific Capacitance as Supercapacitor Electrode Material

2018 ◽  
Vol 281 ◽  
pp. 854-858
Author(s):  
Xi Cheng Gao ◽  
Jian Qiang Bi ◽  
Wei Li Wang ◽  
Guo Xun Sun ◽  
Xu Xia Hao ◽  
...  
Keyword(s):  
Particle Size ◽  
Specific Capacitance ◽  
Electrochemical Property ◽  
Electrode Materials ◽  
High Specific Capacitance ◽  
Constant Current ◽  
X Ray Diffraction ◽  
Supercapacitor Electrode ◽  
Constant Current Charge ◽  
Supercapacitor Electrode Materials

NiFe2O4 powders were synthesized by a facile hydrothermal method at 180°C followed by a thermal treatment at 300°C. The phase composition and morphology were analyzed by X-ray diffraction (XRD) and scanning electron microscope (SEM). The results showed that the NiFe2O4 powders were well-crystallized, and they possessed a particle size in the range of 50-100 nm. The electrochemical property was characterized via cyclic voltammetry (CV) and constant current charge-discharge method. Encouragingly, the NiFe2O4 powders had an excellent electrochemical property, whose specific capacitance reached 266.84 F/g at the electric current density of 1 A/g due to the small particle size. Compared with other Fe-based metal compound oxides, NiFe2O4 has a better electrochemical performance, which can be widely used in the supercapacitor electrode materials.

Tailoring of pyramid cobalt doped nickel oxide nanostructures by composite-hydroxide-mediated approach

2020 ◽  
Vol 239 ◽  
pp. 122036 ◽  
Author(s):  
Aurang Zeb ◽  
Muhammad Arfan ◽  
Tauseef Shahid ◽  
Taha Bin Masood ◽  
Abdul Ghafar Wattoo ◽  
...  
Keyword(s):  
Nickel Oxide ◽  
Oxide Nanostructures
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