MFR High Temperature Profile Control Agent Experimental Evaluation

2012 ◽  
Vol 602-604 ◽  
pp. 1250-1254
Author(s):  
Zhen Zhong Fan ◽  
Li Feng Zhang ◽  
Qing Wang Liu
Keyword(s):  
High Temperature ◽  
Temperature Profile ◽  
Gelation Time ◽  
Salt Resistance ◽  
Control Agent ◽  
Heating Time ◽  
The Core ◽  
Profile Control ◽  
Stable Performance ◽  
Breakthrough Pressure

MFR high temperature profile control agent consisted of 6.5% wood Fortunately sulfonic acid calcium (Ca-LS) and 6.5% crosslinker modified furfural resin (MFR),and the gel solution formed a stable performance gel in the 150~300°C.The higher the temperature, the shorter the gelation time; and the longer the heating time, the higher the gel strength. The gel is very stable at 300°C, and is well in acid and salt resistance. The core experiments showed that the blocking agent's blockage ratio is more than 99% ; the units of the breakthrough pressure was greater than 100 kPa / cm,which the gel solution is a good performance of high-temperature profile control agent.

Improvement Research of Organic Phenolic Gel being Used to be an Organic Deep Profile Control Agent

2014 ◽  
Vol 908 ◽  
pp. 46-50
Author(s):  
Yu Li Liu ◽  
Yi Qin
Keyword(s):  
Crosslinking Agent ◽  
Gelation Time ◽  
High Water ◽  
Salt Resistance ◽  
Control Agent ◽  
Water Soluble ◽  
Water Control ◽  
Profile Control ◽  
Weak Gel ◽  
Deep Profile

Organic phenolic gel is commonly used to be a deep profile control agent which applies to use in the high water cut oilfields where heterogeneity is severe, improve the contradiction of inter-reservoir layer and inner layer, expand water sweeping zone, and achieve the purpose of stable oil production and water control. Organic phenolic weak gel is mainly affected by the concentration of each component and reaction temperature. In this paper, formaldehyde was replaced by urotropin, which is not only delaying the gelation time, but also avoiding pollution. In addition, a water-soluble phenolic resin oligomer has been synthesized by the method of two-step alkali catalysis with appropriate mole ratio as an auxiliary crosslinking agent. Considering the concentration of each reactant as the factor, the orthogonal experiments have been designed to optimize the traditional organic HPAM-phenolic weak gel. We have found that the optimized weak gel has a better stability, longer gelation time, better salt resistance and environment friendly. It can better meet the needs of oilfield deep profile control.

Performance Evaluation for High Temperature Blocking Agent of Tannin Foam System

2012 ◽  
Vol 524-527 ◽  
pp. 1518-1525
Author(s):  
Song Yan Li ◽  
Zhao Min Li
Keyword(s):  
High Temperature ◽  
Temperature Profile ◽  
Blocking Agent ◽  
Control Agent ◽  
Interference Phenomenon ◽  
Cyclic Steam Stimulation ◽  
Profile Control ◽  
New Type ◽  
System Selection ◽  
Steam Stimulation

Cyclic steam stimulation is a kind of recover method for heavy oil. Along with steam stimulation cycles increased, steam channeling interference phenomenon will appear. To solve the problem, one of the most effective methods is high temperature profile control technology. In this paper, a new type of high temperature plugging agent of tannin foam system was researched, and the influencing factors on it were analyzed. Through foam system selection and static evaluation high temperature profile control agent of tannin foam system has been selected. The formula is: foaming agent DHG-1 for 0.5%, tannin for 7.5%, formaldehyde for 4.0%, phenol for 1.0%, CaCl2 for 1000ppm. The tannin foam system can be used in steam stimulation well.

scholarly journals Delayed Crosslinking Amphiphilic Polymer Gel System with Adjustable Gelation Time Based on Competitive Inclusion Method

Polymers ◽  
2019 ◽  
Vol 11 (2) ◽  
pp. 381 ◽  
Author(s):  
Bin Xu ◽  
Huiming Zhang ◽  
He Bian
Keyword(s):  
Gelation Time ◽  
Salt Resistance ◽  
Amphiphilic Polymer ◽  
Polymer Gel ◽  
Polymer Backbone ◽  
Temperature Resistance ◽  
Inclusion Method ◽  
Profile Control ◽  
Resistance Performance ◽  
Gel System

Delayed crosslinking polymer gel systems are widely utilized in deep profile control processes for water production control in oilfields. In this paper, a kind of delayed crosslinking amphiphilic polymer gel system with adjustable gelation time based on competitive inclusion was prepared and its delayed crosslinking gelling properties were studied. The amphiphilic polymer of P(acrylamide (AM)–sodium acrylate (NaA)–N-dodecylacrylamide (DDAM)) was synthesized and it showed much better salt resistance, temperature resistance, and shear resistance performance compared with hydrolyzed polyacrylamide (HPAM). Phenol can be controlled released from the the cavity of β-cyclodextrin (β-CD) ring in the presence of the hydrophobic group used as the competitive inclusion agent in the amphiphilic polymer backbone. Accordingly, the gelation time of the delayed crosslinking amphiphilic polymer gel system is closely related to release rate of the crosslinker from the the cavity of β-CD ring. This study screened an amphiphilic polymer with good salt resistance and temperature resistance performance, which can be used in high temperature and high salinity reservoirs, and provided a feasible way to control the gelation time of the polymer gel system by the competitive inclusion method.

Preparation and Application of J-F Profile Control Agent

2014 ◽  
Vol 962-965 ◽  
pp. 727-730
Author(s):  
Zhan Shuang Xu
Keyword(s):  
Ph Value ◽  
Injection Pressure ◽  
Binary Compound ◽  
Salt Resistance ◽  
Temperature Tolerance ◽  
Economic Benefits ◽  
Control Agent ◽  
Utilization Rate ◽  
Profile Control ◽  
Liaohe Oilfield

In Liaohe oilfield Xing 28 block before and during the alkali/polymer binary compound flooding process, there are heterogeneity contradictions on vertical and plane formation. In order to solve this contradiction, improve the utilization rate of oil displacement agent, J - F profile control agent was developed successfully, the profile control agent is not restricted by formation pH value and gel time, of good resistance to flushing, temperature tolerance and salt resistance. Through the field test, using J-F profile control agent the injection profile changed significantly and the injection pressure increased, a remarkable economic benefits and social benefits are gained.

scholarly journals Development and Performance Evaluation of Steam Channeling Plugging Agent of Thermal Oil Recovery

2015 ◽  
Vol 8 (1) ◽  
pp. 58-63
Author(s):  
Wang Chunsheng ◽  
Sun Yingfan ◽  
He Chenglin ◽  
Zhang Haipeng ◽  
Du Qiuying
Keyword(s):  
Thermal Stability ◽  
High Temperature ◽  
Oil Recovery ◽  
Ph Value ◽  
Control Agent ◽  
Formation Condition ◽  
Cross Linking ◽  
Profile Control ◽  
High Efficient ◽  
And Performance

Under the constraints of high temperature and heterogeneity, the common profile control agent can not effectively plug the steam channeling. To address this issue, it is necessary to develop the high temperature resistance steam channeling plugging agent to improve the steam suction profile in the heavy oil reservoir. This paper used Simple Variable Method to optimize the content of the components of the high temperature resistant plugging agent. Static performances evaluation aims to study the influence rules of the formation condition (temperature, salinity and pH value). Dynamic evaluation is used to study its performance (plugging ratio, residual resistance factor, scouring resistance and thermal stability) in the sand-filled pipe to testify its applicability. The ratio of the component and the injection sequence are shown as follows: 0.03% coagulant +2.2% cross-linking agent I + 1.2% cross-linking II + 6% high efficient main agent. The evaluation experiment results show that the gel can resist at least 280ºC, the plugging ratio is above 93.1%. The plugging ratio only have a 8.43% reduction after scoured by 15 PV steam (280ºC). After a 10-day thermal stability experiment (280 ºC), the plugging ratio is still above 80%. The result indicated that the plugging agent is suitable for the improvement of steam suction profile. The suggested way of injection is also provided.

scholarly journals Preparation and Evaluation of a Profile Control Agent Base on Waste Drilling Fluid

2017 ◽  
Vol 2017 ◽  
pp. 1-7 ◽  
Author(s):  
Xiaoping Qin ◽  
Haiwei Lu ◽  
Yilin Li ◽  
Tong Peng ◽  
Lijie Xing ◽  
...  
Keyword(s):  
Raw Materials ◽  
Drilling Fluid ◽  
Water Injection ◽  
Salt Resistance ◽  
Control Agent ◽  
Injection Wells ◽  
Mild Conditions ◽  
Performance Indexes ◽  
Profile Control ◽  
Preparation And Evaluation

The waste drilling fluid was treated by a flocculant and a pH regulator. And a novel profile control agent base on waste drilling fluid (PCAWDF) was prepared using polymer, formaldehyde, resorcinol, and thiourea as raw materials under mild conditions. PCAWDF was characterized by infrared (IR) spectroscopy and scanning electron microscope (SEM). Compared with the profile control agent prepared by the recirculated water (PCARW), PCAWDF exhibited comparable or better stability, salt resistance, and viscoelasticity. The results of parallel core plugging experiments showed that the profile improvement capability of PCAWDF was stronger than that of PCARW (for 3000 mg/L: 84.6% versus 83.1%; for 5000 mg/L: 91.8% versus 90.2%). The main performance indexes of PCAWDF could meet the need of profile control for the water injection wells. The method could solve the problem of waste drilling fluid treatment in an economic and environmental way.

scholarly journals Experimental Study on Expansion Characteristics of Core-Shell and Polymeric Microspheres

2018 ◽  
Vol 2018 ◽  
pp. 1-9 ◽  
Author(s):  
Pengxiang Diwu ◽  
Baoyi Jiang ◽  
Jirui Hou ◽  
Zhenjiang You ◽  
Jia Wang ◽  
...  
Keyword(s):  
Oil Recovery ◽  
Early Stage ◽  
Average Diameter ◽  
Control Agent ◽  
Field Application ◽  
Experimental Results ◽  
Core Shell ◽  
The Core ◽  
Profile Control ◽  
Polymeric Microsphere

Traditional polymeric microsphere has several technical advantages in enhancing oil recovery. Nevertheless, its performance in some field application is unsatisfactory due to limited blockage strength. Since the last decade, novel core-shell microsphere has been developed as the next-generation profile control agent. To understand the expansion characteristic differences between these two types of microspheres, we conduct size measurement experiments on the polymeric and core-shell microspheres, respectively. The experimental results show two main differences between them. First, the core-shell microsphere exhibits a unimodal distribution, compared to multimodal distribution of the polymeric microsphere. Second, the average diameter of the core-shell microsphere increases faster than that of the polymeric microsphere in the early stage of swelling, that is, 0–3 days. These two main differences both result from the electrostatic attraction between core-shell microspheres with different hydration degrees. Based on the experimental results, the core-shell microsphere is suitable for injection in the early stage to block the near-wellbore zone, and the polymeric microsphere is suitable for subsequent injection to block the formation away from the well. A simple mathematical model is proposed for size evolution of the polymeric and core-shell microspheres.

A New Biopolymer for High-Temperature Profile Control: Part II-Field Results

1989 ◽  
Author(s):  
K. Sampath ◽  
L.G. Jones ◽  
E.T. Strom ◽  
C.H. Phelps ◽  
C.S. Chiou
Keyword(s):  
High Temperature ◽  
Temperature Profile ◽  
Profile Control ◽  
Control Part

Water Shutoff and Profile Control with the Combination of Single Fluid and Double Fluids

2014 ◽  
Vol 962-965 ◽  
pp. 741-745
Author(s):  
Hao Wang
Keyword(s):  
High Temperature ◽  
Temperature Profile ◽  
Field Tests ◽  
Economic Benefits ◽  
Thermal Recovery ◽  
Working Fluids ◽  
Water Shutoff ◽  
Profile Control ◽  
Utilization Ratio ◽  
Chemical Water

Both the single fluid and double-fluid method for water shutoff and profile control have their limitations. If the two kinds of working fluids are used in combination for water shutoff and profile control, each of them exhibits its own plugging capability while they can form plugging materials when they contact and react with each other. This method can be used as a plugging system in the formations, eliminating the low utilization ratio and huge waste of the single or double-fluid chemicals. It can enhance the plugging capability and improve the water shutoff and profile control results. The single and double fluid (SAD) system has been proved satisfactory in the field tests of conventional chemical water shutoff and profile control, high temperature chemical water shutoff and high temperature profile control and channeling-plugging in thermal recovery wells. The economic benefits are remarkable from the field tests of 14 wells.

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