Preparation, Characterization of N-Ti-MCM-22 Molecular Sieve and its Photocatalytic Properties

Methylene Blue ◽

High Pressure ◽

Liquid Phase ◽

Molecular Sieve ◽

X Ray Diffraction ◽

X Ray ◽

Nanocrystalline N-doped and Ti-containing MCM-22 catalyst was synthesized by the static hydrothermal method, using sodium azide as nitrogen source for doping, and tetra-n-butyl titanate [Ti(OC4H9)4] as precursors of TiO2. The catalysts were characterized by X-ray diffraction, transmission electron microscopy, and energy-dispersive spectroscopy.During liquid phase photocatalytic degradation of methylene blue (MB) under high-pressure Hg arc lamp irradiation, the asprepared N-doped Ti-MCM-22 exhibited much higher activity than the undoped Ti-MCM-22, attributed to the effect of nitrogen dopant.

Detonation Synthesis of Nano-Size Materials

MRS Proceedings ◽

10.1557/proc-418-439 ◽

1995 ◽

Vol 418 ◽

Cited By ~ 1

Author(s):

J. Forbes ◽

J. Davis ◽

C. Wong

Keyword(s):

Electron Microscopy ◽

Nucleation And Growth ◽

Detonation Synthesis ◽

X Ray Diffraction ◽

Crystalline Materials ◽

X Ray ◽

Transmission Electron ◽

Nano Size

AbstractThe detonation of explosives typically creates 100's of kbar pressures and 1000's K temperatures. These pressures and temperatures last for only a fraction of a microsecond as the products expand. Nucleation and growth of crystalline materials can occur under these conditions. Recovery of these materials is difficult but can occur in some circumstances. This paper describes the detonation synthesis facility, recovery of nano-size diamond, and plans to synthesize other nano-size materials by modifying the chemical composition of explosive compounds. The characterization of nano-size diamonds by transmission electron microscopy and electron diffraction, X-ray diffraction and Raman spectroscopy will also be reported.

Hydrothermal Synthesis and Characterization of BiFeO3 Polyhedral Crystallites

Applied Mechanics and Materials ◽

10.4028/www.scientific.net/amm.174-177.508 ◽

2012 ◽

Vol 174-177 ◽

pp. 508-511

Author(s):

Lin Lin Yang ◽

Yong Gang Wang ◽

Yu Jiang Wang ◽

Xiao Feng Wang

Keyword(s):

Electron Microscopy ◽

Scanning Electron Microscopy ◽

Synthesis And Characterization ◽

X Ray Diffraction ◽

Xrd Pattern ◽

X Ray ◽

Transmission Electron ◽

Scanning Electron

BiFeO3 polyhedrons had been successfully synthesized via a hydrothermal method. The as-prepared products were characterized by power X-ray diffraction (XRD) pattern, scanning electron microscopy (SEM) and transmission electron microscopy (TEM). The possible mechanisms for the formation of BiFeO3 polyhedrons were discussed. Though comparison experiments, it was found that the kind of precursor played a key role on the morphology control of BiFeO3 crystals.

Nanoscale Characterization of Metal Nanoclusters by Means of X-Ray Diffraction (XRD) and Transmission Electron Microscopy (TEM) Techniques

Metal Nanoclusters in Catalysis and Materials Science ◽

10.1016/b978-044453057-8.50008-8 ◽

2008 ◽

pp. 129-147 ◽

Cited By ~ 4

Author(s):

Patrizia Canton ◽

Pier Francesco Fazzini ◽

Carlo Meneghini ◽

Alvise Benedetti ◽

Giulio Pozzi

Keyword(s):

Electron Microscopy ◽

Metal Nanoclusters ◽

X Ray Diffraction ◽

X Ray ◽

Transmission Electron ◽

Nanoscale Characterization

Characterization of Amorphized Zeolite A by Combining High-Energy X-ray Diffraction and High-Resolution Transmission Electron Microscopy

The Journal of Physical Chemistry C ◽

10.1021/jp305359q ◽

2012 ◽

Vol 116 (48) ◽

pp. 25293-25299 ◽

Cited By ~ 12

Author(s):

Kaku Sato ◽

Toru Wakihara ◽

Shinji Kohara ◽

Koji Ohara ◽

Junichi Tatami ◽

...

Keyword(s):

Electron Microscopy ◽

High Resolution ◽

High Energy ◽

Zeolite A ◽

X Ray Diffraction ◽

X Ray ◽

Characterization of CuCl quantum dots grown in NaCl single crystals via optical measurements, X-ray diffraction, and transmission electron microscopy

Journal of Crystal Growth ◽

10.1016/j.jcrysgro.2018.03.010 ◽

2018 ◽

Vol 490 ◽

pp. 84-88 ◽

Cited By ~ 2

Author(s):

Kensuke Miyajima ◽

Tatsuro Akatsu ◽

Ken Itoh

Keyword(s):

Electron Microscopy ◽

Quantum Dots ◽

Single Crystals ◽

Optical Measurements ◽

X Ray Diffraction ◽

X Ray ◽

Microstructural analysis of high-pressure compressed C60

Journal of Materials Research ◽

10.1557/jmr.2001.0268 ◽

2001 ◽

Vol 16 (7) ◽

pp. 1960-1966 ◽

Cited By ~ 8

Author(s):

K. Miyazawa ◽

H. Satsuki ◽

M. Kuwabara ◽

M. Akaishi

Keyword(s):

Electron Microscopy ◽

High Pressure ◽

High Resolution ◽

Microstructural Analysis ◽

X Ray Diffraction ◽

X Ray ◽

Transmission Electron ◽

Hardness Tests ◽

Lattice Planes

The structure and hardness of C60 bulk specimens compressed under 5.5 GPa at room temperature to 600 °C are investigated by high-resolution transmission electron microscopy, x-ray diffraction, and micro-Vickers hardness tests. A strong accumulation of the [1 1 0]tr orientation of high-pressure-treated C60 specimens was developed along the compression axis, and stacking faults and nano-sized deformation twins were introduced into the C60 specimens compressed at 450–600 °C. Curved lattice planes indicating a polymerization of C60 were observed by high resolution transmission electron microscopy (HRTEM). The polymerization of the high-pressure-compressed C60 is also supported by the computer simulation of HRTEM images.

Growth and Characterization of Misostructural Zinc Oxide Tubes

Journal of Metastable and Nanocrystalline Materials ◽

10.4028/www.scientific.net/jmnm.23.293 ◽

2005 ◽

Vol 23 ◽

pp. 293-296

Author(s):

X.W. Sun ◽

C.X. Xu ◽

B.J. Chen ◽

Y. Yang

Keyword(s):

Electron Microscopy ◽

Zinc Oxide ◽

Growth Process ◽

Hexagonal Structure ◽

Metallic Zinc ◽

X Ray Diffraction ◽

X Ray ◽

Zinc oxide (ZnO) microtube has been fabricated by heating the mixture of ZnO and graphite powders in the atmosphere. The ZnO microtubes showed perfect hexagonal profiles with bell-mouth or normal hexagonal tops. Both X-ray diffraction (XRD) and high-resolution transmission electron microscopy (TEM) demonstrated that the product was composed of ZnO with typical hexagonal structure grown predominantly along (002) direction. The growth process was interpreted by means of vaporliquid-solid mechanism combining with the evaporation of metallic zinc.

Comparative Characterization of InGaN/GaN Multiple Quantum Wells by Transmission Electron Microscopy, X-Ray Diffraction and Rutherford Backscattering

Chinese Physics Letters ◽

10.1088/0256-307x/22/10/067 ◽

2005 ◽

Vol 22 (10) ◽

pp. 2700-2703 ◽

Cited By ~ 6

Author(s):

Zhou Sheng-Qiang ◽

Wu Ming-Fang ◽

Yao Shu-De ◽

Zhang Guo-Yi

Keyword(s):

Electron Microscopy ◽

Quantum Wells ◽

Rutherford Backscattering ◽

Multiple Quantum Wells ◽

Multiple Quantum ◽

X Ray Diffraction ◽

X Ray ◽

Preparation and characterization of CuInS2 nanorods and nanotubes from an elemental solvothermal reaction

Journal of Materials Research ◽

10.1557/jmr.2001.0386 ◽

2001 ◽

Vol 16 (10) ◽

pp. 2805-2809 ◽

Cited By ~ 33

Author(s):

Yang Jiang ◽

Yue Wu ◽

Shengwen Yuan ◽

Bo Xie ◽

Shuyuan Zhang ◽

...

Keyword(s):

Electron Microscopy ◽

Photoelectron Spectroscopy ◽

Electron Transfer Reaction ◽

Solvothermal Reaction ◽

X Ray Diffraction ◽

Spectroscopy Analysis ◽

X Ray ◽

A simple and convenient solvothermal reaction has been developed to produce CuInS2 nanorods and nanotubes from the elements in ethylenediamine at 280 °C. The products were characterized by x-ray diffraction, transmission electron microscopy, high-resolution transmission electron microscopy, scanning electron microscopy, and x-ray photoelectron spectroscopy. Analysis shows that the coordinating ability of ethylenediamine and the existence of liquid In may play important roles in the growth of one-dimension nanocrystallites and the electron-transfer reaction. In addition, spherical CuInS2 micrometer particles were obtained at 350 °C.