Determination of Imidacloprid Residues in Chinese Cabbage by UPLC-MS/MS
Keyword(s):
A method for determination of imidacloprid in Chinese Cabbage was established by using UPLCMS/MS. and the samples are extracted with acetontrile,and the extract is cleaned up by Florisil SPE cartridges and evaporated.Choromatographic separation was performed on a C18 column,and determined by UPLC-MS/MS.The external standard calibration curves were used for quantification. The results showed that a good linear correlation was obtained in the range of 0.005-0.1ug/mL. The limit of quantif icat ion w as 0. 008 mg/ kg .The average recoveries and the relative standard deviations were in the range of 84.9 %~92.7 % and 0.9 %~6.2 %, respectively. It is applicable to the determination of imidacloprid redidue in Chinese cabbage.
2012 ◽
Vol 550-553
◽
pp. 1173-1176
2003 ◽
Vol 69
(7)
◽
pp. 3996-3998
◽
1992 ◽
Vol 75
(3)
◽
pp. 379-383
◽
2018 ◽
Vol 2018
◽
pp. 1-12
◽
2001 ◽
Vol 84
(6)
◽
pp. 1818-1827
◽
1991 ◽
Vol 74
(1)
◽
pp. 22-26
◽
2007 ◽
Vol 90
(1)
◽
pp. 225-237
◽
1989 ◽
Vol 72
(5)
◽
pp. 770-774
◽
2007 ◽
Vol 90
(3)
◽
pp. 844-856
◽
2019 ◽
Vol 82
(8)
◽
pp. 1377-1383
◽