Factors Affecting the Separation of Ti-Al Alloy in the TiPro Process

2013 ◽  
Vol 551 ◽  
pp. 44-54
Author(s):  
Kenneth Sichone ◽  
De Liang Zhang ◽  
Stella Raynova
Keyword(s):  
Powder Particle ◽  
Composite Powder ◽  
Al Alloy ◽  
Composite Powders ◽  
Factors Affecting ◽  
Al Composite ◽  
Al2o3 Phase ◽  
The University ◽  
Solid Liquid ◽  
Solid Liquid Separation

Abstract This paper presents and discusses the factors influencing the yield of Ti-Al alloy in the TiPro process which is a process developed at the University of Waikato for producing titanium alloy powders by mechanically activating Al/TiO2 powder mixtures and subsequently preheating the resultant composite powder in order to ignite a combustion synthesis reaction and separate the liquid Ti-Al alloy by extrusion. In this study, TiO2/Al composite powders with different powder particle microstructures have been produced and used to study the effects of starting composite powder particle microstructure on the solid/liquid separation of TiAl from solid Al2O3 by extrusion. Results obtained so far indicate that maximizing the time the Ti-Al alloy phase is maintained in the liquid state after the reaction between TiO2 and Al is one of the critical factors to increase the yield of Ti-Al alloy produced through the separation of liquid Ti-Al from the solid Al2O3 phase by extruding the mixture of liquid Ti-Al and Al2O3 formed through reactions and heating.

scholarly journals The Study of Optimization of Flocculation and Destabilization Technology of Waste PEM Drilling Fluid in Bohai Oilfield

2021 ◽  
Vol 9 ◽  
Author(s):  
Yang Liu ◽  
Yuchen Zhang ◽  
Tao Xie ◽  
Ming Yue ◽  
Dongsen Wang ◽  
...  
Keyword(s):  
Zeta Potential ◽  
Influence Factor ◽  
Ph Value ◽  
Drilling Fluid ◽  
Mean Value ◽  
Factors Affecting ◽  
Clay Particles ◽  
Liquid Yield ◽  
Solid Liquid ◽  
Solid Liquid Separation

In light of the difficulty of solid-liquid separation of waste PEM drilling fluid in the Bohai oilfield, constructing an inorganic-organic flocculation system is proposed and the processing method of destabilization technology is optimized. The biggest influence factor on the flocculation process of PEM drilling fluid was determined by designing an orthogonal test. The flocculation mechanism was researched through single factor optimization, combined with zeta potential and particle size distribution test. The results showed that the most significant factors affecting the flocculation of waste PEM drilling fluid were the dosage of inorganic flocculant CaCl2 and flocculation pH value. When the dosage of inorganic flocculant CaCl2 was 1.2% (w/v), the dosage of organic flocculant SDYJ-2 was 0.05%, the flocculation pH value was 3, and the flocculation time was 5 min, the flocculation technology reached the optimization and then the liquid yield can reach 70.96%. The mechanism of flocculation and destabilization was as follows: the inorganic flocculant of CaCl2 mainly reduced the zeta potential of clay particles through electric neutralization. 1% CaCl2 could reduce the potential mean value of drilling fluid system from -38.1 mV to -32.5 mV, and then decrease the repulsion among suspensions. Through bridging curling and electric neutralization, the organic flocculant of SDYJ-2 can absorb and wrap the clay particles after flocculation destabilization to form a network spatial structure, which made clay particles aggregate into large flocs and particles. D50 can increase by 21.5 times, when the concentration of SDYJ-2 was 0.15%.

scholarly journals The Ability of Froth Formed without Chemicals to Hold Bacteria

2019 ◽  
Author(s):  
Ghanim Hassan ◽  
Robert G. J. Edyvean
Keyword(s):  
Drinking Water ◽  
Froth Flotation ◽  
Operating Conditions ◽  
Optimum Conditions ◽  
Bacterial Concentration ◽  
Taste And Odor ◽  
Water Taste ◽  
The University ◽  
Solid Liquid ◽  
Solid Liquid Separation

Abstract. Froth flotation is a solid-liquid separation technique that uses hydrophobicity as a driving force. Bacteria and other drinking water microorganisms tend to be hydrophobic and can be removed from water using this application. The biggest limitation against using froth flotation in the drinking water industry is the difficulty of producing froth without chemical frothers and holding bacteria in this froth without chemical collectors which deteriorate water taste and odor. Recently, researchers at the University of Sheffield described a method for producing froth using only water and compressed air. This has enabled froth flotation to be studied as an alternative to biocides for the removal of bacteria from drinking water. This work examines the ability of froth, produced by controlling air pumping through a water column, to hold bacteria. Bacteria are moved to the top of the column and collected in the froth. The operating conditions determine the percentage of bacteria removed. At optimum conditions, froth can hold up to 2×108 cfu/ml of bacteria. It has been found that air pumping at 130 l/min in a 20 cm diameter column will give the highest froth bacterial content. Time to reach stable froth bacterial concentration is decreased by increasing other variables.

EFFECT OF MILLING PARAMETERS ON MICROSTRUCTURE OF Ti/Al COMPOSITE POWDER PRODUCED BY DISCUS MILLING

2006 ◽  
Vol 20 (25n27) ◽  
pp. 4679-4684 ◽  
Author(s):  
S. RAYNOVA ◽  
P. CAO ◽  
B. GABBITAS ◽  
D. ZHANG
Keyword(s):  
Composite Powder ◽  
Single Phase ◽  
Vapour Deposition ◽  
Bulk Material ◽  
Control Agent ◽  
Powder Particle Size ◽  
X Ray Diffraction ◽  
Composite Powders ◽  
Pvd Coating ◽  
Al Composite

The motivation of this research is to develop a process for producing Ti/Al composite powders that enable synthesis of a single-phase TiAl intermetallic bulk material, which is then used as a target for physical vapour deposition (PVD) coating. This study reports the effects of milling time, amount of process control agent (PCA) added as well as the powder-to-medium ratio on the microstructure of the Ti/Al composite powder. Optical microscopy and scanning electron microscopy (SEM) were used to evaluate the level of mixing and the resulting powder particle size. X-ray diffraction analysis and differential thermal analysis were used for determining the phase constituents and the solid state reaction temperature of the as-milled powders.

Structural Model of Service Quality Factors Affecting Loyalty Sustainability

2020 ◽  
Vol 11 (2) ◽  
Author(s):  
Eman Al-erqi ◽  
◽  
Mohd Lizam Mohd Diah ◽  
Najmaddin Abo Mosali ◽  
◽  
...  
Keyword(s):  
International Students ◽  
Service Quality ◽  
Goodness Of Fit ◽  
Structural Model ◽  
Quality Factors ◽  
Factors Affecting ◽  
Measurement Models ◽  
Confirmatory Factor ◽  
The University ◽  
The Impact

This study seeks to address the impact of service quality affecting international student's satisfaction towards loyalty tothe Universiti Tun Hussein Onn Malaysia(UTHM). The aim of thestudy is to develop relationship between service quality factor and loyalty to the university from the international students’ perspectives. The study adopted quantitative approach where data was collected through questionnaire survey and analysed statistically. A total of 246 responses were received and found to be valid. The model was developed and analysed using AMOS-SEM software. Confirmatory factor analysis (CFA) function of the software was to assessed the measurement models and found that all the models achieved goodness of fit. Then path analysis function was used to assessed structural model and found that service qualityfactors have a significant effect on the students’ satisfaction and thus affecting the loyaltyto the university. Hopefully the outcome form this study will benefit the university in providing services especially to the international students.

Nitrogen Removal in a Real-Time Controlled Sequencing Batch Membrane Bioreactor

2010 ◽  
Vol 5 (3) ◽  
Author(s):  
Cheng-Nan Chang ◽  
Li-Ling Lee ◽  
Han-Hsien Huang ◽  
Ying-Chih Chiu
Keyword(s):  
Real Time ◽  
Nitrogen Removal ◽  
Membrane Bioreactor ◽  
Synthetic Wastewater ◽  
Real Time Control ◽  
Time Control ◽  
Cake Layer ◽  
On Line ◽  
Solid Liquid ◽  
Solid Liquid Separation

The performance of a real-time controlled Sequencing Batch Membrane Bioreactor (SBMBR) for removing organic matter and nitrogen from synthetic wastewater has been investigated in this study under two specific ammonia loadings of 0.0086 and 0.0045g NH4+-N gVSS−1 day−1. Laboratory results indicate that both COD and DOC removal are greater than 97.5% (w/w) but the major benefit of using membrane for solid-liquid separation is that the effluent can be decanted through the membrane while aeration is continued during the draw stage. With a continued aeration, the sludge cake layer is prevented from forming thus alleviating the membrane clogging problem in addition to significant nitrification activities observed in the draw stage. With adequate aeration in the oxic stage, the nitrogen removal efficiency exceeding 99% can be achieved with the SBMBR system. Furthermore, the SBMBR system has also been used to study the occurrence of ammonia valley and nitrate knee that can be used for real-time control of the biological process. Under appropriate ammonia loading rates, applicable ammonia valley and nitrate knee are detected. The real-time control of the SBMBR can be performed based on on-line ORP and pH measurements.

Investigations on the filtration of natural aquatic suspensions supported by dosing small amounts of Fe(III)-salts (βFe ≤ 0.1 mg.L-1): mode of action and basic design criteria

2002 ◽  
Vol 2 (2) ◽  
pp. 91-98
Author(s):  
R. Winzenbacher ◽  
R. Schick ◽  
H.-H. Stabel ◽  
M. Jekel
Keyword(s):  
Large Scale ◽  
Suspended Solids ◽  
Iron Hydroxides ◽  
Essential Step ◽  
Iron Salts ◽  
Alkaline Earths ◽  
Co Precipitation ◽  
Solid Liquid ◽  
Solid Liquid Separation

Improved removal of particles during the treatment of natural aquatic suspensions has been achieved by pre-ozonation and the addition of small quantities of iron salts (βFe ≤ 0.1 mg.L-1; “Fe(III)-assisted filtration”) followed by rapid filtration. As shown by investigations on a large-scale installation at Lake Constance Water Supply, this procedure reliably reduces suspended solids by at least 2-3 powers of ten in long-term use. However, the high efficacy of Fe(III)-assisted filtration cannot be explained on the basis of known coagulation mechanisms (like adsorption-charge neutralization, co-precipitation). Instead, the essential step was found to be the conditioning of the filter medium by coating it with colloids containing Fe(OH)3, and this “Fe coating” process occurs only in the presence of alkaline earths (especially Ca2+). According to further experiments, the enhanced solid-liquid separation was ultimately traced to chemical interactions such as the formation of calcium-organic association structures between the iron hydroxides and other solids. For design of Fe(III)-assisted filtration steps, finally, a βCa/DOC ratio above 40 mg.mg-1 and pre-oxidation with ozone dosages not exceeding 2 mg O3/mg DOC was recommended.

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