scholarly journals Effect of Microwave Sintering Parameters on the Physical and Mechanical Properties of Pure Ti and Blended Elemental Ti Alloys

2018 ◽  
Vol 770 ◽  
pp. 52-59
Author(s):  
Stiliana Raynova ◽  
M. Ashraf Imam ◽  
Hunter Taylor ◽  
Fei Yang ◽  
Leandro Bolzoni
Keyword(s):  
Tensile Properties ◽  
Sintering Temperature ◽  
Microwave Sintering ◽  
Physical And Mechanical Properties ◽  
Porosity Distribution ◽  
Powder Mixtures ◽  
Blended Elemental ◽  
Ti Alloys ◽  
Ti Powder ◽  
Powder Compacts

Microwave sintering (MWS) was used to consolidate hydride de-hydride Ti powder and blended elemental Ti6Al4V, Ti5Fe and Ti5Al5Mo5V3Cr (Ti5553) powder mixtures. The amount of powders used to prepare the powder compacts was scaled up to 500g.The effect of the MWS conditions on the relative density, porosity distribution, microstructure and tensile properties were studied. Furthermore, uniformity in distribution of the alloying elements was checked. For most of the materials considered, a combinations of sintering temperature of 1200oC and 1300oC and holding time of 5 to 30 min resulted in significantly improved density. Nevertheless sintering temperature of at least 1300oC was required for pore coalescence and high tensile properties.

Development of Nano-Structure Cu-Ti Alloys by Mechanical Alloying Process

2013 ◽  
Vol 829 ◽  
pp. 168-172 ◽  
Author(s):  
Ahdie Pourfereidouni ◽  
Gholam Hossein Akbari
Keyword(s):  
Milled Powder ◽  
Lattice Parameter ◽  
X Ray Diffraction ◽  
Powder Mixtures ◽  
Nano Structure ◽  
Cu Alloys ◽  
Ti Alloys ◽  
Alloy Process ◽  
Electrical Conductivities ◽  
Ti Powder

Cu-Ti system with a terminal solution in the Cu-rich portion of equilibrium Cu-Ti phase diagram with a decreasing trend with temperature shows a potential to develop age hardenable alloys with suitable strength and thermal and electrical conductivities. In the present study, the mechanical alloy process has been employed to increase solubility of Ti in Cu matrix to make age hardenable Cu alloys. Cu-Ti powder mixtures with different rations of 1 and 6 wt% of Ti were milled in planetary ball mill for different milling times of 4, 12, 48, 96 and 192 hours. The milled powder mixtures were investigated and characterised by X-ray diffraction (XRD) technique. The results show increasing in lattice parameter of Cu, which indicates that Ti atoms are dissolved in the Cu matrix. Cu crystal sizes showed decreasing trend which were more obvious in the mixture with higher Ti contents. The final crystal sizes were in the range of 17-23 nm after 192 hours of milling.

Hybrid microwave sintering of blended elemental Ti alloys

2019 ◽  
Vol 39 ◽  
pp. 52-57 ◽  
Author(s):  
S. Raynova ◽  
M.A. Imam ◽  
F. Yang ◽  
L. Bolzoni
Keyword(s):  
Microwave Sintering ◽  
Blended Elemental ◽  
Ti Alloys

scholarly journals Effect of Sintering Time on the Densification, Microstructure, Weight Loss and Tensile Properties of a Powder Metallurgical Fe-Mn-Si Alloy

2017 ◽  
Author(s):  
Zhigang Xu ◽  
Michael A. Hodgson ◽  
Peng Cao
Keyword(s):  
Weight Loss ◽  
Tensile Properties ◽  
Isothermal Holding ◽  
Weight Percent ◽  
Depletion Region ◽  
Holding Time ◽  
Uniaxial Pressure ◽  
Nominal Composition ◽  
Powder Mixtures ◽  
Powder Compacts

This work investigated the isothermal holding time dependence of the densification, microstructure, weight loss and tensile properties of Fe-Mn-Si powder compacts. Elemental Fe, Mn and Si powder mixtures with a nominal composition of Fe-28Mn-3Si (in weight percent) were ball milled for 5h and subsequently pressed under a uniaxial pressure of 400 MPa. The compacted Fe-Mn-Si powder mixtures were sintered at 1200 ℃ for 0, 1, 2 and 3 h, respectively. In general, the density, weight loss and tensile properties increased with the increase of isothermal holding time. A significant increase in density, weight loss and tensile properties occurred in the compacts isothermally holding for 1 h, as compared to those with no isothermal holding. However, further extension of isothermal holding time (2 and 3 h) only played a limited role in promoting the density and tensile properties. The weight loss of the sintered compacts was mianly caused by the sublimation of Mn in Mn depletion region on the surface layer of the sintered Fe-Mn-Si compacts. The length of the Mn depletion region increased as isothermal holding time increased. A single α-Fe phase was detected on the surface of all the sintered compacts, and the locations beyond the Mn depletion region were comprised of a dual dominant γ-austenite and minor ε-martensite.

ANSONIA C14500

Alloy Digest ◽  
2008 ◽  
Vol 57 (3) ◽  
Keyword(s):  
Mechanical Properties ◽  
Shear Strength ◽  
Physical Properties ◽  
Tensile Properties ◽  
Pure Copper ◽  
Physical And Mechanical Properties ◽  
Heat Treating

Abstract Ansonia alloy C14500 has unique fabrication properties while maintaining both physical and mechanical properties close to pure copper. The addition of Tellurium makes the alloy free machining. This datasheet provides information on composition, physical properties, hardness, tensile properties, and shear strength. It also includes information on forming, heat treating, machining, and joining. Filing Code: CU-752. Producer or source: Ansonia Copper & Brass Inc.

Development of the Snoek Anelastic Relaxation Correlated with Oxygen in β-Ti Alloys

2019 ◽  
Vol 298 ◽  
pp. 59-63 ◽  
Author(s):  
Zheng Cun Zhou ◽  
J. Du ◽  
S.Y. Gu ◽  
Y.J. Yan
Keyword(s):  
Internal Friction ◽  
Physical And Mechanical Properties ◽  
Peak Height ◽  
Relaxation Peak ◽  
Interstitial Oxygen ◽  
Internal Friction Peak ◽  
Β Phase ◽  
Ti Alloys ◽  
Interstitial Atoms ◽  
The Stability

The β-Ti alloys exhibit excellent shape memory effect and superelastic properties. The interstitial atoms in the alloys have important effect on their physical and mechanical properties. For the interstitial atoms, the internal friction technique can be used to detect their distributions and status in the alloys. The anelastic relaxation in β-Ti alloys is discussed in this paper. β-Ti alloys possesses bcc (body center body) structure. The oxygen (O) atoms in in the alloys is difficult to be removed. The O atoms located at the octahedral sites in the alloys will produce relaxation under cycle stress. In addition, the interaction between the interstitial atoms and substitute atoms, e.g., Nb-O,Ti-O can also produce relaxation. Therefore, the observed relaxational internal friction peak during the measuring of internal friction is widened. The widened multiple relaxation peak can be revolved into Debye,s elemental peaks in Ti-based alloys. The relaxation peak is associated with oxygen movements in lattices under the application of cycle stress and the interactions of oxygen-substitute atoms in metastable β phase (βM) phase for the water-cooled specimens and in the stable β (βS) phase for the as-sintered specimens. The damping peak height is not only associated with the interstitial oxygen, but also the stability and number of βM in the alloys.

scholarly journals Microwave Sintering and Microwave Dielectric Properties of (1–x)Ca0.61La0.26TiO3-xNd(Mg0.5Ti0.5)O3 Ceramics

Materials ◽  
2021 ◽  
Vol 14 (2) ◽  
pp. 438
Author(s):  
Shuwei Yang ◽  
Bingliang Liang ◽  
Changhong Liu ◽  
Jin Liu ◽  
Caisheng Fang ◽  
...  
Keyword(s):  
Dielectric Properties ◽  
Mobile Communications ◽  
Sintering Temperature ◽  
Microwave Sintering ◽  
Microwave Dielectric Properties ◽  
Conventional Heating ◽  
Sintering Process ◽  
Microwave Dielectric ◽  
Sintering Time ◽  
Frequency Temperature

The (1–x)Ca0.61La0.26TiO3-xNd(Mg0.5Ti0.5)O3 [(1–x)CLT-xNMT, x = 0.35~0.60] ceramics were prepared via microwave sintering. The effects of sintering temperature and composition on the phase formation, microstructure, and microwave dielectric properties were investigated. The results show that the microwave sintering process requires a lower sintering temperature and shorter sintering time of (1–x)CLT-xNMT ceramics than conventional heating methods. All of the (1–x)CLT-xNMT ceramics possess a single perovskite structure. With the increase of x, the dielectric constant (ε) shows a downward trend; the quality factor (Qf) drops first and then rises significantly; the resonance frequency temperature coefficient (τf) keeps decreasing. With excellent microwave dielectric properties (ε = 51.3, Qf = 13,852 GHz, τf = −1.9 × 10−6/°C), the 0.65CLT-0.35NMT ceramic can be applied to the field of mobile communications.

Effect of TiO2 and MgO on Microstructure of α-Alumina Ceramics and its Sintering Behavior

2015 ◽  
Vol 1112 ◽  
pp. 519-523 ◽  
Author(s):  
Jarot Raharjo ◽  
Sri Rahayu ◽  
Tika Mustika ◽  
Masmui ◽  
Dwi Budiyanto
Keyword(s):  
Mechanical Properties ◽  
Sintering Temperature ◽  
Physical And Mechanical Properties ◽  
Basic Material ◽  
Sintering Behavior ◽  
Pressureless Sintering ◽  
Alumina Ceramics ◽  
Density Measurements ◽  
Technical Alumina ◽  
Platelet Structure

Observation on the effect of adding titanium oxide (TiO2) and magnesium oxide (MgO) on the sintering of α-alumina (Al2O3) has been performed. In this study, technical alumina used as basic material in which the sample is formed by the pressureless sintering/cold press and sintered at 1500°C which is lower than alumina sintering temperature at 1700°C. Elemental analysis, observation of microstructure, hardness, fracture toughness and density measurements were carried out to determine the physical and mechanical properties of alumina. The results indicate a change in the microstructure where the content of the platelet structure are much more than the equilateral structure. At sintering temperature of 1500°C, neck growth occurs at ceramics grain, supported by the results of the density test which indicate perfect compaction has occurred in this process.

Preparation of ZrO2 Composite Ceramics with High Thermal Shock Resistance

2012 ◽  
Vol 455-456 ◽  
pp. 650-654 ◽  
Author(s):  
He Yi Ge ◽  
Jian Ye Liu ◽  
Xian Qin Hou ◽  
Dong Zhi Wang
Keyword(s):  
Mechanical Properties ◽  
Water Absorption ◽  
Thermal Shock ◽  
Thermal Shock Resistance ◽  
Sintering Temperature ◽  
Fiber Composite ◽  
Physical And Mechanical Properties ◽  
Composite Ceramics ◽  
Shock Resistance ◽  
Absorption Measurements

The physical and mechanical properties of nanometer ZrO2-ZrO2fiber composite ceramics were studied by introduction of ZrO2fiber. ZrO2composite ceramics at different sintering temperature was investigated by porosity and water absorption measurements, flexual strength and thermal shock resistance analysis. Results showed that ZrO2composite ceramics containing 15 wt% ZrO2fiber with sintering temperature of 1650°C exhibited good mechanical properties and thermal shock resistance. The porosity and the water absorption were 8.84% and 1.62%, respectively. The flexual strength was 975 MPa and the thermal shock times reached 31 times. Scanning electron microscope (SEM) was used to analyze the microstructure of ZrO2composite ceramics.

CHARACTERIZATION OF HYDROXYAPATITE/TI6AL4V COMPOSITE POWDER UNDER VARIOUS SINTERING TEMPERATURE

2015 ◽  
Vol 75 (7) ◽  
Author(s):  
Amir Arifin ◽  
Abu Bakar Sulong ◽  
Norhamidi Muhamad ◽  
Junaidi Syarif
Keyword(s):  
Mechanical Properties ◽  
Composite Powder ◽  
Sintering Temperature ◽  
Physical And Mechanical Properties ◽  
Xrd Analysis ◽  
X Ray Diffraction ◽  
Different Temperatures ◽  
Two Phases ◽  
Work Interaction

Hydroxyapatite (HA) has been widely used in biomedical applications due to its excellent biocompatibility. However, Hydroxyapatite possesses poor mechanical properties and only tolerate limited loads for implants. Titanium is well-known materials applied in implant that has advantage in mechanical properties but poor in biocompatibility. The combination of the Titanium alloy and HA is expected to produce bio-implants with good in term of mechanical properties and biocompatabilty. In this work, interaction and mechanical properties of HA/Ti6Al4V was analyzed. The physical and mechanical properties of HA/Ti6Al4V composite powder obtained from compaction (powder metallurgy) of 60 wt.% Ti6Al4V and 40 wt.% HA and sintering at different temperatures in air were investigated in this study. Interactions of the mixed powders were investigated using X-ray diffraction. The hardness and density of the HA/Ti6Al4V composites were also measured. Based on the results of XRD analysis, the oxidation of Ti began at 700 °C. At 1000 °C, two phases were formed (i.e., TiO2 and CaTiO3). The results showed that the hardness HA/Ti6Al4V composites increased by 221.6% with increasing sintering temperature from 700oC to 1000oC. In contrast, the density of the composites decreased by 1.9% with increasing sintering temperature. 

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