Structure and Phase Composition of a Ti Film–Al Substrate System Irradiated with an Intense Pulsed Electron Beam

2018 ◽  
Vol 781 ◽  
pp. 101-107
Author(s):  
Yurii Ivanov ◽  
Olga V. Krysina ◽  
Pavel Moskvin ◽  
Elizaveta A. Petrikova ◽  
Olga V. Ivanova ◽  
...  
Keyword(s):  
Wear Resistance ◽  
Electron Beam ◽  
High Surface ◽  
Pure Titanium ◽  
Surface Hardness ◽  
Vacuum Arc ◽  
High Wear Resistance ◽  
Commercially Pure Titanium ◽  
Plasma Cathode ◽  
Commercially Pure

Commercially pure A7 aluminum was exposed to surface modification in a single vacuum cycle which included vacuum arc evaporation and deposition of commercially pure titanium and intense electron beam irradiation and melting of the film–substrate system using a plasma-cathode pulsed electron source. The deposited Ti film thickness was 0.5 and 1 μm. The irradiated Ti–Al system revealed a multilayer multiphase structure consisting of submicro-and nanosized elements with intermetallic inclusions Al3Ti, Al2Ti, and TiAl3. The Ti film during irradiation broke up into fragments with their immersion in the molten Al surface layer to a depth of 20 μm. The modified material surpassed the initial aluminum in wear resistance by a factor of 2.4 and in microhardness by a factor larger than 4. The main cause for the high surface hardness and high wear resistance of the modified aluminum was likely the formation of both the intermetallic particles and the Ti-hardened transition layer.

Multicycle Surface Alloying of Aluminum with Titanium: Structure and Properties

2018 ◽  
Vol 781 ◽  
pp. 131-136
Author(s):  
Yurii Ivanov ◽  
Nikolay Koval ◽  
Olga V. Krysina ◽  
Pavel Moskvin ◽  
Elizaveta A. Petrikova ◽  
...  
Keyword(s):  
Intermetallic Layer ◽  
Pure Titanium ◽  
Vacuum Arc ◽  
Commercially Pure Titanium ◽  
Plasma Cathode ◽  
Mechanical And Tribological Properties ◽  
Commercially Pure ◽  
Film Substrate ◽  
Titanium Structure ◽  
Rapidly Solidified

Commercially pure A7 aluminum was surface alloyed with commercially pure titanium on COMPLEX equipment under unified vacuum conditions through vacuum arc evaporation and deposition of a thin Ti film and intense electron beam irradiation of the film–substrate system using a plasma-cathode pulsed electron source. The number of deposition–irradiation cycles was 20. The Ti film thickness in each cycle was 0.5 μm. After multicycle alloying, a modified surface layer of up to 60 μm thick was formed representing a multiphase structure of rapidly solidified submicro-and nanograins. The microhardness of the Ti–Al surface alloy (irradiation at 15 J/cm2, 50 μs, 10 pulses) was more than 8 times the microhardness of A7 aluminum, and its wear resistance and friction coefficient were respectively 45 times higher and 1.2 times lower than the values in the initial material. The chief cause for the improved mechanical and tribological properties of commercially pure A7 aluminum is the formation of an extended intermetallic layer.

Influence of Duplex Treatment on Structural and Tribological Properties of Commercially Pure Titanium

2017 ◽  
Vol 36 (1) ◽  
pp. 63-68 ◽  
Author(s):  
Ilhan Çelik
Keyword(s):  
Wear Resistance ◽  
Tribological Properties ◽  
Physical Vapor Deposition ◽  
Plasma Nitriding ◽  
Pure Titanium ◽  
Surface Hardness ◽  
Compound Layer ◽  
Commercially Pure Titanium ◽  
Wear Properties ◽  
Commercially Pure

AbstractTitanium and its alloys are widely used in many fields, including aerospace and the chemical and biomedical industries. This is due to their mechanical properties, excellent corrosion resistance, and biocompatibility although they do have poor wear resistance. In this study, a duplex layer was successfully formed on the commercially pure titanium surface by duplex treatments (plasma nitriding and physical vapor deposition (PVD)). In the initial treatment, plasma nitriding was performed on the pure titanium samples and in the second treatment, the nitrided samples were coated with CrN by PVD. The friction and wear properties of the duplex-treated samples were investigated for tribological applications. Surface morphology and microstructure of the duplex-treated samples were analyzed by X-ray diffraction (XRD) and scanning electron microscopy (SEM). In addition, the tribological properties were investigated using pin-on-disc tribometer. A compound layer composed of ε-Ti2N and δ-TiN phases and a diffusion layer formed under the compound layer were obtained on the surface of pure titanium after the nitriding treatments. CrN coated on the nitrided surface provided an increase in the surface hardness and in the wear resistance.

The Influence of Laser Irradiation Parameters on Tribological Behaviour of Commercially Pure Titanium for Dental Prostheses

2016 ◽  
Author(s):  
Karibeeran Shanmuga Sundaram ◽  
Gurusami Kiliyappan ◽  
Senthil Kumaran Selvadurai
Keyword(s):  
Surface Roughness ◽  
Wear Resistance ◽  
Pure Titanium ◽  
Laser Surface ◽  
Commercially Pure Titanium ◽  
Laser Shock ◽  
Micro Hardness ◽  
Dental Prostheses ◽  
Commercially Pure ◽  
Cp Ti

Laser shock peening (LSP) is one of the innovative technique that produces a compressive residual stress on the surface of metallic materials, thereby significantly increasing its fatigue life in applications where failure is caused by surface-initiated cracks. The specimens were treated with laser shock waves with different processing parameters, and characterization studies were made on treated specimens. The purpose of the present study was to investigate the influence of Nd:YAG laser on commercially pure titanium (CP-Ti) used in prosthetic dental restorations. The treatment influenced change in microstructure, micro hardness, surface roughness, and wear resistance characteristics. Though CP-Ti is considered as an excellent material for dental applications due to its outstanding biocompatibility, it is not suitable when high mastication forces are applied. In the present study, pulsed Nd:YAG laser surface treatment technique was adopted to improve the wear resistance of CP-Ti. The wear test pin specimens of CP-Ti were investment cast with centrifugal titanium casting machine. The wear properties of specimens were evaluated after LSP on a “pin-on-disc” wear testing tribometer, as per ASTM G99-05 standards. The results of the wear experiment showed that the treated laser surface has higher wear resistance, micro hardness, and surface roughness compared to as-cast samples. The improvement of wear resistance may be attributed due to grain refinement imparted by LSP processes. The microstructure, wear surfaces, wear debris, and morphology of the specimen were analyzed by using optical electron microscope, scanning electron microscope, and X-ray diffraction (XRD). The data were compared using ANOVA and post-hoc Tukey tests. The characteristic change resulted in increase in wear resistance and decrease in wear rate. Hence, it is evident that the more reliable and removable partial denture metal frameworks for dental prostheses may find its applications.

Regularities of the formation and the role of secondary structures in the improvement of the wear resistance of commercially pure titanium VT1-0

2012 ◽  
Vol 33 (3) ◽  
pp. 184-189 ◽  
Author(s):  
B. P. Gritsenko ◽  
Yu. F. Ivanov ◽  
N. N. Koval’ ◽  
K. V. Krukovskii ◽  
N. V. Girsova ◽  
...  
Keyword(s):  
Wear Resistance ◽  
Pure Titanium ◽  
Secondary Structures ◽  
Commercially Pure Titanium ◽  
Commercially Pure

Comparison of Commercially Pure Titanium Surface Hardness Improvement by Plasma Nitrocarburizing and Ion Implantation

2013 ◽  
Vol 789 ◽  
pp. 347-351 ◽  
Author(s):  
Agung Setyo Darmawan ◽  
Waluyo Adi Siswanto ◽  
Tjipto Sujitno
Keyword(s):  
Ion Implantation ◽  
Elevated Temperatures ◽  
Pure Titanium ◽  
Surface Hardness ◽  
Commercially Pure Titanium ◽  
Hardness Tester ◽  
Hardness Number ◽  
Commercially Pure ◽  
Hardness Tests ◽  
Plasma Nitrocarburizing

Commercially pure (cp) titanium has a relative soft hardness property. In particular usage such as sliding, the improvement of the surface hardness will be required. In this study, surface hardness improvement of cp titanium by Plasma Nitrocarburizing and Ion Implantation are compared. Plasma Nitrocarburizing processes are conducted at different elevated temperatures with different duration processes, i.e. at 350 °C for 3, 4, and 5 hours, and at 450 °C for 2, 3, and 4 hours respectively, while Ion Implantation processes are conducted at room temperature and process durations are varied as 2.3 hours, 4.7 hours, and 9.3 hours. Nitrogen ions are used to implant the material. Hardness tests are then performed on each specimen by using Micro Vickers Hardness Tester. The surface hardness number (HV) for specimens of the Plasma Nitrocarburizing processes at temperature of 350 °C for process duration of 3 hours, 4 hours, and 5 hours are 74.16, 92.25 and 94.41, respectively while those at temperature of 450 °C for duration process of 2 hours, 3 hours, and 4 hours are 103.70, 121.31 and 126.17, respectively. The processes of Ion Implantation produce the surface hardness number (HV) of 88.97, 125.51, and 130.2, for duration processes of 2.3 hours, 4.7 hours, and 9.3 hours. The process of Ion Implantation produce higher surface hardness number than the Plasma Nitrocarburizing process at temperature 350 °C but the surface hardness number is lower when compared to the Plasma Nitrocarburizing at a temperature of 450 °C. For the duration processes 4 hours and more, the process of Ion Implantation produces the same surface hardness number with the Plasma Nitrocarburizing at temperature of 450 °C.

scholarly journals Porous SiO2/HAp Coatings on Cp-Titanium Grade 1 Surfaces Produced by Electrophoretic Deposition

2016 ◽  
Vol 61 (4) ◽  
pp. 2177-2182 ◽  
Author(s):  
T. Moskalewicz ◽  
A. Babkiewicz ◽  
B. Dubiel ◽  
M. Kot ◽  
A. Radziszewska ◽  
...  
Keyword(s):  
High Surface ◽  
Pure Titanium ◽  
Commercially Pure Titanium ◽  
Porous Hydroxyapatite ◽  
Commercially Pure ◽  
Nanocrystalline Hydroxyapatite ◽  
Porous Sio2 ◽  
Surface Development ◽  
Titanium Grade ◽  
Increase Corrosion Resistance

Abstract Porous hydroxyapatite doped SiO2 coatings were electrophoretically deposited (EPD) on commercially pure titanium. The influence of EPD parameters on coatings quality was investigated. Microstructural observation was done using transmission and scanning electron microscopy as well as X-ray diffractometry. The coatings consisted of spherical micro and nanocrystalline hydroxyapatite (HAp) as well as amorphous SiO2 nanoparticles. The coatings exhibited open porosity with pore diameter up to 1 μm and due to presence of nanoparticles high surface development. It was found that application of SiO2/HAp coating increase corrosion resistance of titanium in Ringer’s solution.

L. KLEIN TITAN GRADE 2

Alloy Digest ◽  
2021 ◽  
Vol 70 (4) ◽  
Keyword(s):  
Wear Resistance ◽  
Corrosion Resistance ◽  
Physical Properties ◽  
Pure Titanium ◽  
Heat Treating ◽  
Commercially Pure Titanium ◽  
Commercially Pure ◽  
Continuous Service ◽  
Titanium Grade ◽  
Service Environments

Abstract L. Klein Titan Grade 2 is an unalloyed, commercially pure titanium grade. It is the most widely used commercially pure titanium grade. It offers a combination of moderate strength and good ductility, with outstanding corrosion resistance in many challenging service environments. L. Klein Titan Grade 2 can operate in continuous service up to 425 °C (800 °F) and in intermittent service up to 540 °C (1005 °F). This datasheet provides information on composition, physical properties, and tensile properties. It also includes information on corrosion resistance and wear resistance as well as forming, heat treating, machining, and joining. Filing Code: Ti-177. Producer or source: L. Klein SA.

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