The Effect of Sizing Additives for Carbon Fiber on the Mechanical Properties of Polyetherimide Composites

2020 ◽  
Vol 869 ◽  
pp. 488-493
Author(s):  
Aues A. Beev ◽  
Svetlana Yu. Khashirova ◽  
Azamat L. Slonov ◽  
Ismel V. Musov ◽  
Azamat Zhansitov ◽  
...  

The article presents the results of sizing of discrete carbon fibers with various substances and their effect on the properties of polyetherimide composites. As sizing agents, 1,3-diaminobenzene, 4,4'-dihydroxy-2,2-diphenylpropane, polyetherimide and oligoetherether sulfone were used. The study of physical and mechanical properties showed that all the substances used increase the properties of the carbon-filled composite based on polyetherimide. The highest mechanical properties are demonstrated by a composite containing carbon fibers treated with 1,3-diaminobenzene, which indicates improved compatibility of the filler and the polymer matrix and enhanced intermolecular interactions.

2021 ◽  
Vol 899 ◽  
pp. 309-316
Author(s):  
Ismel V. Musov ◽  
Azamat L. Slonov ◽  
Azamat A. Zhansitov ◽  
Zhanna I. Kurdanova ◽  
Svetlana Yu. Khashirova

The influence of the multiplicity of extrusion and melt viscosity on the residual length of discrete carbon fibers in composites based on polyetherimide for 3D-printing is estimated. A technique for measuring the residual length of carbon fibers in composites is proposed. The residual length of carbon fibers in composites containing from 10 to 40% fibrous filler with different initial linear dimensions has been determined. It was found that the addition of a melt viscosity modifier to a carbon-filled composite helps to maintain the linear dimensions of the fiber filler particles, thereby increasing the physical and mechanical properties of the material.


2021 ◽  
Vol 899 ◽  
pp. 540-547
Author(s):  
Aues A. Beev ◽  
Dzhul’etta A. Beeva ◽  
M.U. Shokumova ◽  
M.R. Tlenkopachev ◽  
Muaed M. Oshkhunov

The paper investigates the processes of carbon fiber surface treatment and their influence on the properties of polyetheretherketone composites. It has been shown that preliminary thermal activation of carbon fiber followed by treatment with a dressing agent - polyhydroxyether makes it possible to create polyetheretherketone composite carbon-filled materials with an increased level of physical and mechanical properties.


Materials ◽  
2021 ◽  
Vol 14 (6) ◽  
pp. 1512
Author(s):  
Chiara Morano ◽  
Ran Tao ◽  
Marco Alfano ◽  
Gilles Lubineau

Adhesive bonding of carbon-fiber-reinforced polymers (CFRPs) is a key enabling technology for the assembly of lightweight structures. Surface pretreatment is necessary to remove contaminants related to material manufacturing and ensure bond reliability. The present experimental study focuses on the effect of mechanical abrasion on the damage mechanisms and fracture toughness of CFRP/epoxy joints. The analyzed CFRP plates were provided with a thin layer of surface epoxy matrix and featured enhanced sensitivity to surface preparation. Various degrees of morphological modification and fairly controllable carbon fiber exposure were obtained using sanding with emery paper and grit-blasting with glass particles. In the sanding process, different grit sizes of SiC paper were used, while the grit blasting treatment was carried by varying the sample-to-gun distance and the number of passes. Detailed surveys of surface topography and wettability were carried out using various methods, including scanning electron microscopy (SEM), contact profilometry, and wettability measurements. Mechanical tests were performed using double cantilever beam (DCB) adhesive joints. Two surface conditions were selected for the experiments: sanded interfaces mostly made of a polymer matrix and grit-blasted interfaces featuring a significant degree of exposed carbon fibers. Despite the different topographies, the selected surfaces displayed similar wettability. Besides, the adhesive joints with sanded interfaces had a smooth fracture response (steady-state crack growth). In contrast, the exposed fibers at grit-blasted interfaces enabled large-scale bridging and a significant R-curve behavior. While it is often predicated that quality composite joints require surfaces with a high percentage of the polymer matrix, our mechanical tests show that the exposure of carbon fibers can facilitate a remarkable toughening effect. These results open up for additional interesting prospects for future works concerning toughening of composite joints in automotive and aerospace applications.


2021 ◽  
Vol 36 (4) ◽  
pp. 417-422
Author(s):  
Y. Hamid ◽  
P. Svoboda

Abstract Ethylene-butene copolymer (EBC)/carbon-fiber (CF) composites can be utilized as an electromechanical material due to their ability to change electric resistance with mechanical strain. The electro-mechanical properties and thermal conductivity of ethylene butene copolymer (EBC) composites with carbon fibers were studied. Carbon fibers were introduced to EBC with various concentrations (5 to 25 wt%). The results showed that carbon fibers’ addition to EBC improves the electric conductivity up to 10 times. Increasing the load up to 2.9 MPa will raise the electric resistance change by 4 500% for a 25% fiber sample. It is also noted that the EBC/CF composites’ electric resistance underwent a dramatic increase in raising the strain. For example, the resistance change was around 13 times higher at 15% strain compared to 5% strain. The thermal conductivity tests showed that the addition of carbon fibers increases the thermal conductivity by 40%, from 0.19 to 0.27 Wm–1K–1.


2018 ◽  
Vol 225 ◽  
pp. 01022
Author(s):  
Falak O. Abasi ◽  
Raghad U. Aabass

Newer manufacturing techniques were invented and introduced during the last few decades; some of them were increasingly popular due to their enhanced advantages and ease of manufacturing over the conventional processes. Polymer composite material such as glass, carbon and Kevlar fiber reinforced composite are popular in high performance and light weight applications such as aerospace and automobile fields. This research has been done by reinforcing the matrix (epoxy) resin with two kinds of the reinforcement fibers. One weight fractions were used (20%) wt., Epoxy reinforced with chopped carbon fiber and second reinforcement was epoxy reinforced with hybrid reinforcements Kevlar fiber and improved one was the three laminates Kevlar fiber and chopped carbon fibers reinforced epoxy resin. After preparation of composite materials some of the mechanical properties have been studied. Four different fiber loading, i.e., 0 wt. %, 20wt. % CCF, 20wt. % SKF, AND 20wt. %CCF + 20wt. % SKF were taken for evaluating the above said properties. The thermal and mechanical properties, i.e., hardness load, impact strength, flexural strength (bending load), and thermal conductivity are determined to represent the behaviour of composite structures with that of fibers loading. The results show that with the increase in fiber loading the mechanical properties of carbon fiber reinforced epoxy composites increases as compared to short carbon fiber reinforced epoxy composites except in case of hardness, short carbon fiber reinforced composites shows better results. Similarly, flexural strength test, Impact test, and Brinell hardness test the results show the flexural strength, impact strength of the hybrid composites values were increased with existence of Kevlar fibers, while the hardness was decrease. But the reinforcement with carbon fibers increases the hardness and decreases other tests.


BioResources ◽  
2015 ◽  
Vol 11 (1) ◽  
Author(s):  
Djamila Kada ◽  
Sébastien Migneault ◽  
Ghezalla Tabak ◽  
Ahmed Koubaa

2010 ◽  
Vol 4 (4) ◽  
pp. 329-337
Author(s):  
Fabio Pereira ◽  
◽  
Fabiana Vieira ◽  
Luiz de Castro ◽  
Ricardo Michel ◽  
...  

In this work the influence of different configurations in the sample preparation process on commercial polyacrylonitrile-based carbon fibers mechanical tests were studied. Mechanical properties, such as tensile strength, Young’s modulus, elongation and Weibull modulus, were evaluated. The results showed that all sample preparation steps may have strong influence on the results.


Author(s):  
Р. Ш. Іскандаров ◽  
Н. В. Сова ◽  
Б. М. Савченко ◽  
І. І. П'ятничук ◽  
В. А. Татаренко

Study of the FFF additive manufacturing process of composite material based on L – polylactide (PLLA) with ultra-short carbon fibers. Tensile strength and elongation at break for all test specimens were determined according to ISO 527. Tensile modulus - ASTM D638-10, specimen density - PN-EN ISO 1183, microscopic examination - according to ASTM E2015 - 04 (2014). Charpy Shock Tests ISO 179 and ASTM D256. Bending test method ISO 178 and ASTM D 790. The rational modes of FFF additive manufacturing (AM) of carbon fiber composite based on PLLA was established. Properties of carbon fiber PLLA and unfilled PLLA was determinated for AM formed samples and injection molded samples. Carbon fiber composites have significantly higher flexural and tensile module us values compared to the original L-polylactide, which is due to the effect of polymer matrix reinforcement by the fibrous component. However, finished products obtained by AM PLLA carbon composite have a lower impact strength and tensile strength, which is likely to be due to the fact that the carbon fibers are short (50-60 mkm) and have a cavitations effect during injection molding and AM. Density of carbon fiber filled PLLLA was lower the theoretically calculated value for filament material as well for injection molded and AM formed samples. Density reduction probably the main cause of impact properties deterioration due to cavity forming around carbon fibers. Density and tensile properties of AM formed samples can be changed by AM slicing parameter – extrusion multiplier. Cavitation effect for carbon fiber composites observed for PLLA composite in form AM filament, injection molded parts and AM formed samples. Cavity forming was confirmed by optical microscopy and density measurement. Possible reason for cavity forming is orientation deformation of the fiber in polymer matrix during the formation of the filament. The effect of cavitation also persists in the AM of products from carbon composites due to the passage of the orientation at the exit of the printer nozzle.  The possibility of regulating the density and physical and mechanical properties of carbon composite products obtained by the additive manufacturing method has been established. Selection of rational values of the extrusion multiplier and the direction of the layers in the additive molding allows you to create products with the desired complex of properties.


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