Phase Transformation Law of Nb Microalloyed Steel at Different Cooling Rates

2021 ◽  
Vol 1035 ◽  
pp. 396-403
Author(s):  
Ping Yu ◽  
Ren Bo Song ◽  
Wen Ming Xiong ◽  
Wei Feng Huo ◽  
Chen Wei ◽  
...  

Through the Gleeble3500 thermal simulation test machine, the phase transformation law of Nb microalloyed steel was studied and tested. After the compression deformation, it was cooled to room temperature at different speeds. Obtain the dynamic continuous cooling transformation diagram and the scanning structure diagram of the test steel, and then analyze the phase composition under different cooling speeds through JMatPro material performance simulation. The results show that: at a lower cooling speed (0.1°C/s), austenite decomposition is a diffusion-type phase change that takes place in a high-temperature region, and carbon atoms can diffuse sufficiently. At a moderate cooling rate (1°C/s), the bainite phase transition is a semi-diffusion phase transition in which carbon atoms are displaced in a non-cooperative thermally activated transition mode. When the cooling rate is high (15°C/s), the martensitic transformation is a non-diffusion-type transformation carried out in the low temperature region, and the atoms are directly transferred from the austenite lattice to the martensite lattice. With the increase of the cooling rate and the decrease of the transition temperature, from low-speed cooling→medium-speed cooling→high-speed cooling, respectively, the diffusion type phase transition→semi-diffusion type phase transition→the non-diffusion type phase transition. At different cooling rates, the continuous cooling transition diagram simulated by JMatPro is basically the same as the phase transition in the dynamic continuous cooling transition diagram of the test steel, which proves that the simulation prediction of the dynamic continuous cooling transition of the test steel by the JMatPro software has high accuracy and applicability.

2011 ◽  
Vol 291-294 ◽  
pp. 786-789
Author(s):  
Lian Sheng Chen ◽  
Yan Hong Leng ◽  
Yan Kai Han ◽  
Jin Ying Song

In the continuous cooling process, when the metal material austenite transition occurs, latent heat is released. Through the thermal-meter can determine the characteristics point of the phase transition. In this paper, by thermal analysis, at the cooling rate of 0.5°C•s-1, 0.8°C•s-1, 40Cr bar is tested to determine the characteristics point of the phase transition, latent heat and the heat capacity in phase transition.


2014 ◽  
Vol 804 ◽  
pp. 281-284
Author(s):  
Yuan She ◽  
Zhao Hui Zhang ◽  
Jian Tao Ju ◽  
Bo Jin

The continuous cooling phase transformation behavior of niobium microalloyed steel was studied by Thermecmastor-Z thermomechanical simulator; the continuous cooling transformation curves (CCT) were established. The change of microstructure under different cooling rates was observed, and the influence of deformation in austenite non-recrystallization region on transformation was discussed. Based on these work, it was possible to know that the phase transformation is retarded and the ferritic grain is refined dramatically as the cooling rate increasing. The deformation in austenite non-recrystallization region caused deformation stored-energy, which improved the grain refinement of transformation to some extent, but not significant.


2012 ◽  
Vol 590 ◽  
pp. 23-27
Author(s):  
Xin Li ◽  
Jie Zhao ◽  
Jun Cheng Bao ◽  
Bao Qun Ning ◽  
Jian Ping Li

To achieve reasonable rolling technology of the novel Nb-V composite microalloyed steel, the continuous cooling transformation (CCT) curve was established by thermal simulation experiment. Microstructure and microhardness at different cooling rates were characterized using an optical microscope (OM) and microhardness tester. The results indicate that the critical quenching speed of Nb-V microalloyed steel is about 23 °C/s. The start and finishing temperatures of phase transformation decreased with the rise of cooling rate. Widmannstatten (W) structure appears at lower cooling rate interval. Microstructure transfers into martensite (M) and bainite (B) with obviously refined grains in higher cooling rate interval. Microhardness improves with the increase of cooling rates. Microhardness value is greatly improved to 298.6 HV at the cooling rate of 11 °C/s, which could be related to the formation of lower bainite during phase transformation process. When the cooling rate is above 29 °C/s, microhardness values remain unchanged basically. This illustrates that the microstructure of Nb-V microalloyed steel consists of martensite and lower bainite.


2013 ◽  
Vol 652-654 ◽  
pp. 947-951
Author(s):  
Hui Li ◽  
Yun Li Feng ◽  
Da Qiang Cang ◽  
Meng Song

The static continuous cooling transformation (CCT)curves of 3.15 Si-0.036 C-0.21 Mn-0.008 S-0.008 N-0.022 Al are measured on Gleeble-3500 thermal mechanical simulator, the evolution of microstructure and the tendency of hardness are investigated by optical microscope (OM) and hardness tester. The results show that there is no evident change in microstructure which mainly are ferrite and little pearlite under different cooling rates, but the transition temperature of ferrite is gradually reduced with the increase of cooling rate. When the cooling rate is increased from 0.5°C/s to 20°C/s, the ending temperatures of phase transformation are decreased by 118°C, when cooling rate reaches to 10, Widmanstatten ferrite appears. The hardness of the steel turns out gradual upward trend with the increase of cooling rate.


2011 ◽  
Vol 228-229 ◽  
pp. 72-76
Author(s):  
J. H. Yang ◽  
Q. Y. Liu

Deformation dilatometry has been used to simulate controlled hot rolling followed by controlled cooling of a Nb microalloyed pipeline steels, the microstructure and transformation characteristics in the steel and the effect of deformation on transformation are studied. According to the results of both dilatometry measurements and microstructure observations, the continuous cooling transformation curves (CCT) of the tested steels are constructed. The results show that Nb content and deformation enhance the formation of acicular ferrite; the microstructure of the steel range from PF, QF to AF with increasing of cooling rates from 0.5 to 50°C /s in a two stages controlled rolling and the microstructure revolution is sensitive to cooling rates when it is lower than 5°C /s, however, when the cooling rate increasing further, the microstructure didn’t change very much but M/A constituents in matrix is refined and dispersed.


2022 ◽  
Vol 905 ◽  
pp. 83-87
Author(s):  
Lu Lu Feng ◽  
Wei Wen Qiao ◽  
Jian Sun ◽  
De Fa Li ◽  
Ping Ping Li ◽  
...  

The continuous cooling transformation behavior of high-carbon pearlitic steel was studied by employing optical microscopy, scanning electron microscopy, and the Vickers hardness test. The results show that the microstructure of the test steel is composed of proeutectoid cementite and lamellar pearlite in the cooling rate range of 0.05–2 °C/s and lamellar pearlite in the range of 2–5 °C/s. Further, martensite appears at 10 °C/s. With the increase in the cooling rate, the Vickers hardness of the test steel first decreases and then increases. In the industrial production of high-carbon pearlite steel, the formation of proeutectoid cementite at a low cooling rate needs to be avoided, and at the same time, the formation of martensite and other brittle-phase at a high cooling rate needs to be avoided.


2004 ◽  
Vol 57 (4) ◽  
pp. 303-311
Author(s):  
Wiliam Regone ◽  
Sérgio Tonini Button

Microalloyed steels are used in the forging of many automotive parts like crankshafts and connecting rods. They are hot worked in a sequence of stages that includes the heating to the soaking temperature, followed by forging steps, and finally the controlled cooling to define the microstructure and mechanical properties. In this work it was investigated the thermomechanical behavior and the microstructural evolution of a Ti-V microalloyed steel in the phase transition region. Torsion tests were done with multiple steps with true strain equal to 0.26 in each step. After each torsion step the samples were continuous cooled for 15 seconds to simulate hot forging conditions. These tests provided results for the temperature at the beginning of the phase transformation, and allowed to analyze the microstructural changes. Also, workability tests were held to analyze the microstructural evolution by optical and scanning electron microscopy. Results from the torsion tests showed that the temperature for the beginning of phase transformation is about 700 ºC. Workability tests held at 700 ºC followed by water-cooling presented microstructures with different regions: strain hardened, and static and dynamic recrystallized. Workability tests at 700 ºC followed by air-cooling showed a complex microstructure with ferrite, bainite and martensite, while tests at 650 and 600 ºC followed by water-cooling showed a microstructure with allotriomorphic ferrite present in the grain boundaries of the previous austenite.


2016 ◽  
Vol 850 ◽  
pp. 916-921
Author(s):  
Pei Pei Xia ◽  
Liu Qing Yang ◽  
Xiao Jiang Guo ◽  
Ye Zheng Li

The microstructural evolution of the high Nb X80 pipeline steel in Continuous Cooling Transformation (CCT) by Gleeble-3500HS thermal mechanical simulation testing system was studied, the corresponding CCT curves were drawn and the influence of some parameters such as deformation and cooling rate on microstructure of high Nb X80 pipeline steel was analyzed. The results show that as cooling rate increased, the phase transformation temperature of high Nb X80 steel decreased, with the microstructure transformation from ferrite-pearlite to acicular ferrite and bainite-ferrite. When cooling rate was between 20°C/s and 30°C/s, the microstructure was comparatively ideal acicular ferrite, thermal deformation accelerates phase transformation notably and made the dynamic CCT curves move upward and the initial temperature of phase transformation increase obviously. Meanwhile the thermal deformation refined acicular ferrite and extended the range of cooling rate accessible to acicular ferrite.


2019 ◽  
Vol 944 ◽  
pp. 303-312
Author(s):  
Li Zhang Li ◽  
He Wei ◽  
Lin Lin Liao ◽  
Yin Li Chen ◽  
Hai Feng Yan ◽  
...  

Gear steel is a ferritic steel. In the rolling process, the ideal structure is ferrite + pearlite, and bainite or martensite is not expected. However, due to the high alloy content, the hardenability is good, and the bainite or martensite structure is very likely to be generated upon cooling after rolling. In this paper, phase transformation rules during continuous cooling of 20CrMnTi with and without deformation were studied to guide the avoidance of the appearance of bainite or martensite in steel. A combined method of dilatometry and metallography was adopted in the experiments, and the dilatometer DIL805A and thermo-simulation Gleeble3500 were used. Both dynamic and static continuous cooling transformation (CCT) diagrams were drawn by using the software Origin. The causes of those changes in starting temperature, finishing temperature, starting time and transformation duration in ferrite-pearlite phase transformation were analyzed, and the change in Vickers hardness of samples with different cooling rate was discussed. The results indicate that with different cooling rate, there are three phase transformation zones: ferrite-pearlite, bainite and martensite. Deformation of austenite accelerates the occurrence of transformation obviously and moves CCT curve to left and up direction. When the cooling rate is lower than 1 °C/s, the phases in samples are mainly ferrite and pearlite, which is the ideal microstructure of experimental steel. As the cooling rate increases, starting temperature of ferrite transformation in steel decreases, starting time reduces, transformation duration gradually decreases, and the Vickers hardness of samples increases. Under the cooling rate of 0.5 °C/s, ferrite transformation in deformed sample starts at 751.67 °C, ferrite-pearlite phase transformation lasts 167.9 s, and Vickers hardness of sample is 183.4 HV.


Metals ◽  
2019 ◽  
Vol 9 (3) ◽  
pp. 334 ◽  
Author(s):  
Samuel Rodrigues ◽  
Fulvio Siciliano ◽  
Clodualdo Aranas ◽  
Eden Silva ◽  
Gedeon Reis ◽  
...  

A five-pass torsion simulation of the roughing passes applied during hot plate rolling was performed in the single-phase austenite region of a Nb-microalloyed steel under continuous cooling conditions. The deformation temperatures were approximately half-way between the Ae3 and the delta ferrite formation temperature (i.e., 250 °C above the Ae3) in which the free energy difference of austenite and ferrite is at maximum. The microstructures in-between passes were analyzed to characterize and quantify the occurrence of deformation-induced dynamic phase transformation. It was observed that about 7% of austenite transforms into ferrite right after the final pass. The results are consistent with the calculated critical strains and driving forces which indicate that dynamic transformation (DT) can take place at any temperature above the Ae3. This mechanism occurs even with the presence of high Nb in the material, which is known to retard and hinder the occurrence of DT by means of pinning and solute drag effects. The calculated cooling rate during quenching and the time–temperature–transformation curves of the present material further verified the existence of dynamically transformed ferrite.


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