Grain Size in Mg Alloys: Recrystallization and Mechanical Consequences

2007 ◽  
Vol 558-559 ◽  
pp. 433-440 ◽  
Author(s):  
Matthew R. Barnett ◽  
Dale Atwell ◽  
Aiden G. Beer
Keyword(s):  
Grain Size ◽  
Dynamic Recrystallization ◽  
Grain Refinement ◽  
Magnesium Alloys ◽  
Mechanical Response ◽  
Deformation Twinning ◽  
Simultaneous Increase ◽  
The Impact ◽  
Strength And Ductility

The present paper examines the development of grain size during the recrystallization of magnesium alloys and the influence the grain size has on the mechanical response. In magnesium alloys grain refinement improves the strength-ductility balance. This simultaneous increase in both strength and ductility is ascribed to the impact the grain size has on deformation twinning. The mechanisms by which the grain size is established during hot working are shown to be conventional dynamic recrystallization followed by post-dynamic recrystallization. The role of alloying addition on both of these reactions is briefly considered.

scholarly journals Novel grain refinement of AZ91E magnesium alloy and the effect on hot tearing during solidfication

2021 ◽  
Author(s):  
Abdallah Elsayed
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Magnesium Alloy ◽  
Grain Refinement ◽  
Magnesium Alloys ◽  
Hot Tearing ◽  
Grain Refining ◽  
Grain Refiner ◽  
Structural Applications ◽  
Hot Tearing Susceptibility

For the A1-5Ti-1B grain refiner, the addition of 0.1 wt.% provided a 68 % reduction in grain size as compared to the unrefined AZ91E alloy at a holding time of five minutes. Grain growth restriction by TiB₂ particles was the source of grain refinement. With the addition of A1-5Ti-1B, only a small reduction in hot tearing susceptibility ws observed because large TiA1₃ particles bonded poorly with the eutectic and blocked feeding channels.The addition of 1.0 wt.% A1-1Ti-3B provided a grain size reduction of 63% as compared to the unrefined AZ91E alloy at a holding time of five minutes. The grain refinement with A1-1Ti-3B addition was attributed to a combination of TiB₂ grain growth restriction and A1B₂ nucleating sites. A significant reduction in hot tearing susceptibility was observed with A1-1Ti-3B addition as a result of a higher cooling rate and shorter local soldification time as compared to the AZ91E alloy. The reduction in hot tearing susceptibility was attributed to the good interface between eutectic and TiB₂ particles. Both grain refiners demonstrated a good resistance to fading during the holding times investigated. In addition, the AZ91E + A1-5Ti-1B and AZ91E + A1-1Ti-3B castings showed much fewer dislocation networks as compared to the untreated AZ91E casting.The development of efficient A1-Ti-B refiners can also improve castability of magnesium alloys. In addition, the fade resistant A1-Ti-B grain refiners can reduce operating costs and maintain productivity on the foundry floor. Thus, magnesium alloy with A1-Ti-B treatment have the potential for more demanding structural applications in the automobile and aerospace industries. Vehicle weight in the aerospace and automotive industries directly impacts carbon emissions and fuel efficiency. An increase in the use of lightweight materials for structural applications will result in lighter vehicles. Low density materials, such as magnesium (1.74 g/cm³) are a potential alternative to aluminium (2.70 g/cm³), to reduce component weight in structural applications.However, current magnesium alloys still do not have adequate mechanical properties and castability to meet the performance specifications of the automotive and aerospace industries. Grain refinement can significantly improve mechanical properties and reduce hot tearing during permanent mould casting. Recently, Al-Ti-B based grain refiners have shown potential in grain refining magnesium-aluminum alloys such as AZ91E. This study investigates the grain refining efficiency and fading of A1-5Ti-1B and A1-1Ti-3B in AZ91E magnesium alloy and their subsequent effect on hot tearing.The grain refiners were added at 0.1, 0.2, 0.5 and 1.0 wt.% levels. For the grain refinement and fading experiments, the castings were prepared using graphite moulds with holding times of 5, 10 and 20 minutes. For the hot tearing experiments, castings were produced representing the optimal addition level of each grain refiner. The castings were prepared using a permanent mould with pouring and mould temperatures of 720 and 180 ºC, respectively. The castings were characterized using SEM, TEM, optical microscopy and thermal analysis.

The Role of Deformation Banding in Grain Refinement under ECAP

2014 ◽  
Vol 783-786 ◽  
pp. 2641-2646 ◽  
Author(s):  
Rustam Kaibyshev ◽  
Sergey Malopheyev ◽  
Vladislav Kulitskiy ◽  
Marat Gazizov
Keyword(s):  
Dynamic Recrystallization ◽  
Grain Refinement ◽  
Lamellar Structure ◽  
True Strain ◽  
High Angle ◽  
Continuous Dynamic Recrystallization ◽  
Angular Pressing ◽  
Deformation Banding ◽  
Continuous Dynamic

The mechanism of grain refinement in an Al-5.4Mg-0.4Mn-0.2Sc-0.09Zr alloy subjected to equal-channel angular pressing (ECAP) at 300°C through route BC is considered. It was shown that the formation of geometrically necessary boundaries (GNB) aligned with a {111} plane at ε≤1 initiates the occurrence of continuous dynamic recrystallization (CDRX). Upon further strain the GNBs transform to low-to-moderate angle planar boundaries that produces lamellar structure. In the strain interval 2-4, 3D arrays of planar boundaries evolve due to inducing the formation of 2nd order and higher orders families of GNBs in new {111} planes. GNBs gradually convert to high-angle boundaries (HAB) with strain. A uniform recrystallized structure is produced at a true strain of ∼8. The role of slip concentration and shearing patterns in the formation of GNBs is discussed.

scholarly journals Effects of Repetitive Upsetting Extrusion on the Microstructure and Texture of GWZK124 Alloy under Different Starting Temperatures

Materials ◽  
2019 ◽  
Vol 12 (15) ◽  
pp. 2437
Author(s):  
Guanshi Zhang ◽  
Zhimin Zhang ◽  
Yingze Meng ◽  
Zhaoming Yan ◽  
Xin Che ◽  
...  
Keyword(s):  
Grain Size ◽  
Dynamic Recrystallization ◽  
Grain Refinement ◽  
Volume Fraction ◽  
Bimodal Microstructure ◽  
Continuous Dynamic Recrystallization ◽  
Average Grain Size ◽  
Second Phases ◽  
Continuous Dynamic ◽  
Weak Texture

The effects of repetitive upsetting extrusion under different starting temperatures on the microstructure and texture of GWZK124 alloy were investigated. The results clearly showed that the particles and second phases induced dynamic recrystallization (DRX), which can be explained by the particle-stimulated nucleation (PSN) mechanism. It was shown that grain refinement during repetitive upsetting extrusion (RUE) is dominated by a complicated combination of continuous dynamic recrystallization and discontinuous dynamic recrystallization. The RUEed alloys under different starting temperatures exhibited a bimodal microstructure comprising fine DRXed grains with weak texture and coarse deformed grains with strong texture. The DRXed grains could weaken the texture. As the RUE starting temperature decreased, the average grain size increased and the volume fraction of DRXed grains decreased.

Hierarchical Microstructure Tailoring of Pure Titanium for Enhancing Cellular Response at Tissue-Implant Interface

2021 ◽  
Vol 17 (1) ◽  
pp. 115-130
Author(s):  
Shokouh Attarilar ◽  
Faramarz Djavanroodi ◽  
Mahmoud Ebrahimi ◽  
Khaled J. Al-Fadhalah ◽  
Liqiang Wang ◽  
...  
Keyword(s):  
Grain Size ◽  
Dynamic Recrystallization ◽  
Grain Refinement ◽  
Cellular Response ◽  
Electron Backscatter Diffraction ◽  
Pure Titanium ◽  
Biological Response ◽  
Surface Mechanical Attrition Treatment ◽  
Meaningful Improvement ◽  
Texture Intensity

The main goal of this research is to scrutinize the effect of texture and grain size on the biological response of hierarchical structured pure titanium (Ti), examining the interrelation between grain refinement mechanisms with texture variation. The hierarchical structure was produced using two methods of severe plastic deformation (SPD). The Ti specimens were first processed up to six passes by equal channel angular pressing (ECAP) and subsequently treated at the top surface using surface mechanical attrition treatment (SMAT). Microstructure examination by Electron backscatter diffraction (EBSD) indicates that the SMAT-treated surface was categorized into three distinct microstructural regions based on the type of grain refinement process involved during SPD: twin induced dynamic recrystallization (TDRX) and geometric dynamic recrystallization (GDRX) in the topmost surface, and continuous (CDRX) and discontinuous dynamic recrystallization (DDRX) in the lower regions of the sample. The biological experiments showed meaningful improvement in the cellular response of SMATed and ECAPed samples. It was demonstrated that grain refinement could have the capability of improving the biological response of Ti surface. In this regard, SMATed + 2ECAPed sample showed the best result although it has not the smallest grain size and the highest texture intensity. It was observed that texture and grain orientation of planes have an important impact on the biological response of pure Ti and dominance of prismatic (1010) texture can improve the cell viability, adhesion and its differentiation. Therefore, microstructure and texture tailoring through combined SPD methods could be a promising strategy for the improvement of the next generation of medical implants.

The Impact of Grain Size on Oxidation Behavior of TP304H Austenitic Stainless Steel at High Temperature in Air

2011 ◽  
Vol 117-119 ◽  
pp. 990-994
Author(s):  
Wei Wei ◽  
Zhi Wu Wang ◽  
Mao Lin Liu
Keyword(s):  
Grain Size ◽  
Stainless Steel ◽  
Austenitic Stainless Steel ◽  
Oxide Scale ◽  
Grain Refinement ◽  
Coarse Grained ◽  
X Ray ◽  
Fine Grained ◽  
Different Grain Size ◽  
The Impact

Exposed to 650°C air, TP304H stainless steel with two different grain size was oxidized at this temperature. At the meantime, comparison of their oxidation was through the oxidation kinetics curves and analysis of the morphology and composition of oxide scale which conducted by SEM and X-ray. The results showed that the oxidation rate of TP304H stainless steel was slowed down by grain refinement and oxide scale of fine-grained TP304H steel was thinner than that of coarse-grained steel. The nucleation and the growth of nuclei of coarse-grained oxide scale were more rapid. In addition, the grain refinement of austenitic stainless steel accelerated the diffusivity of Cr and made for the formation of dense and continuous oxide scale, so that the oxidation of stainless steel can be effectively inhabited.

Research on the Strength Improvement of 7A04 Aluminum Alloy

2012 ◽  
Vol 488-489 ◽  
pp. 19-21
Author(s):  
Chao Jue Yi ◽  
Peng Cheng Zhai ◽  
Li Zhou Dong ◽  
Qi Hao Fu
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Tensile Strength ◽  
Aluminum Alloy ◽  
Grain Refinement ◽  
Cryogenic Treatment ◽  
The Impact ◽  
Strength Improvement

By using cryogenic treatment on 7A04 aluminum alloy tested with micrographic analysis and mechanical properties test, we studied the impact on mechanical properties of 7A04 aluminum alloy The results showed that the strength of 7A04 aluminum alloy could be highly increased and the grain size would be reduced in the process through being treated in 480°C/80min + aging in 120°C/4h + cryogenic treatment + aging at 120°C/16h.7A04 aluminum alloy are more fully recrystallized to grain refinement and the tensile strength of it can be increased to 720Mpa after the treatment.

Grain Evolution Character of Discal Parts by Roll Forming

2013 ◽  
Vol 749 ◽  
pp. 328-336
Author(s):  
Quan Lin Jin
Keyword(s):  
Numerical Simulation ◽  
Grain Size ◽  
Titanium Alloy ◽  
Aluminum Alloy ◽  
Dynamic Recrystallization ◽  
Strain Rate ◽  
Grain Refinement ◽  
Grain Growth ◽  
Roll Forming ◽  
Alloy 6061

A study on grain evolution character of discal parts roll forming was carried out by means of experiment and numerical simulation. The discal part material is aluminum alloy 6061 and titanium alloy TC4. The roll forming temperature is 480-500 and 930-1020 for aluminum alloy 6061 and titanium alloy TC4, respectively. A digital double-sided roll forming machine was used for roll forming experiment of discal parts. The high frequency induction heating was used for disk heating, where the deformation zone is in the state of constant temperature. A numerical simulation of roll forming of the 6061 aluminum alloy disk was carried out. The simulated results include macroscopic deformation and various grain size evolution variables. The dynamic recrystallization, the dynamic and static grain growth were considered in the numerical simulation. The experimental and simulated results showed that there may appear not only the grain refinement due to dynamic recrystallization but also dynamic and static grain growth. It is different that from discal parts integrally forging there are the largest deformation, the highest strain rate and the best recrystallization and grain refinement in the zones contacted with the roll tools. In the zones far from the rollers, the strain rate is very low and average grain size increases until once again contact to the rollers and start new grain refinement.

Study of the Microstructure, Texture and Tensile Properties in as-Extruded AZ91 and ZM21 Magnesium Alloys

2011 ◽  
Vol 702-703 ◽  
pp. 659-662
Author(s):  
M. Thirumurugan ◽  
R. Madhavan ◽  
S. Kumaran ◽  
T. Srinivasa Rao ◽  
Satyam Suwas
Keyword(s):  
Grain Size ◽  
Dynamic Recrystallization ◽  
Tensile Properties ◽  
Structure Formation ◽  
Texture Analysis ◽  
Magnesium Alloys ◽  
Az91 Alloy ◽  
Second Phase ◽  
Mean Grain Size ◽  
The Mean

In this paper, the microstructure, texture and tensile properties of the magnesium alloys AZ91 and ZM21 extruded at 350°C to the ratio 25:1 are investigated. After extrusion, the mean grain size reduces from 400 µm to 30 µm in ZM21 alloy and from 350 µm to 40 µm in AZ91 alloy. Bulk texture analysis indicates the formation of characteristic extrusion texture in both the alloys. The occurrence of dynamic recrystallization, as revealed through necklace structure formation, and the precipitation of second phase (Mg17Al12) particles in the AZ91 alloy are observed.

Strength and Ductility in Electrodeposited Nanocrystalline Nickel

2009 ◽  
Vol 633-634 ◽  
pp. 411-420 ◽  
Author(s):  
Heather W. Yang ◽  
Farghalli A. Mohamed
Keyword(s):  
Grain Size ◽  
Grain Growth ◽  
Annealing Treatment ◽  
Average Grain Size ◽  
Annealing Twins ◽  
Grain Distribution ◽  
Small Grains ◽  
20 Nm ◽  
Strength And Ductility

Electrodeposited nanocrystalline (nc) Ni having an average grain size of 20 nm was annealed at 443 K for different holding times. An examination of the microstructure following annealing showed three important features. First, all annealed samples exhibited abnormal grain growth, which was manifested by the presence of large grains that were surrounded by regions of small grains (bimodal grain distributions). Second, annealing twins existed in the large grains of the samples that showed a bimodal grain distribution. Third, by estimating the density of annealing twin, it was found that annealing nc-Ni at 443 K resulted in a maximum twin density after 5h. Following annealing treatment, specimens with different volume fractions of twins were tested under uniaxial tension at 393 K and a strain rate of 10-4 s-1. The results showed that both strength and ductility in nc-Ni attained maximum values after annealing for 5h. The role of both bimodal grain distributions and annealing twins in enhancing ductility and strength was discussed.

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