A New Constitutive Model for Work Hardening Based on Gain Boundary Energy Density

2009 ◽  
Vol 633-634 ◽  
pp. 249-259
Author(s):  
Ji Luo ◽  
Zhi Rui Wang

Recently, the necessity to grade grain size to ultrafine and nano scale for understanding the mechanical behavior of these materials has been recognized. However, the nature of such classification has remained unclear. As an example, ultrafine (100 nm -1 μm) and nano (<100 nm) grained FCC metals, compared to their coarse grained counterparts, exhibit a grain size strengthening that may deviate from the Hall-Petch relationship. To explain the mechanism of such deviation, previous dislocation theories seem insufficient. To solve this problem, a critical grain size criterion governing the shift of deformation mechanism is proposed in this work. This model employs an energetic approach; it relates the grain boundary energy density to certain critical energy values; and it permits, for the first time, a quantitative grading of grain sizes. Predictions based on this model were evaluated. The prediction on copper polycrystals of various grain sizes showed a very good agreement with experimental results. It is thus wished that the grain size theory on plastic deformation mechanism could be unified with the dislocation theory. In this study, such unification is attempted by using a parameter defined as the defect energy density. The possibility of such generalization is further reasoned upon the fact that the defect energy approach should be a unique but common form applicable for both dislocations and grain boundaries.

Materials ◽  
2020 ◽  
Vol 13 (14) ◽  
pp. 3223 ◽  
Author(s):  
Abdelrahim Husain ◽  
Peiqing La ◽  
Yue Hongzheng ◽  
Sheng Jie

In the present study, molecular dynamics simulations were employed to investigate the effect of strain rate on the plastic deformation mechanism of nanocrystalline 316 L stainless-steel, wherein there was an average grain of 2.5–11.5 nm at room temperature. The results showed that the critical grain size was 7.7 nm. Below critical grain size, grain boundary activation was dominant (i.e., grain boundary sliding and grain rotation). Above critical grain size, dislocation activities were dominant. There was a slight effect that occurred during the plastic deformation mechanism transition from dislocation-based plasticity to grain boundaries, as a result of the stress rate on larger grain sizes. There was also a greater sensitive on the strain rate for smaller grain sizes than the larger grain sizes. We chose samples of 316 L nanocrystalline stainless-steel with mean grain sizes of 2.5, 4.1, and 9.9 nm. The values of strain rate sensitivity were 0.19, 0.22, and 0.14, respectively. These values indicated that small grain sizes in the plastic deformation mechanism, such as grain boundary sliding and grain boundary rotation, were sensitive to strain rates bigger than those of the larger grain sizes. We found that the stacking fault was formed by partial dislocation in all samples. These stacking faults were obstacles to partial dislocation emission in more sensitive stress rates. Additionally, the results showed that mechanical properties such as yield stress and flow stress increased by increasing the strain rate.


1981 ◽  
Vol 32 (6) ◽  
pp. 935 ◽  
Author(s):  
DR Hudson ◽  
RA Hunter ◽  
DW Peter

Grain size of elemental selenium is a major factor controlling the long-term effectiveness of intraruminal selenium pellets. Microscope studies of polished sections of new and used selenium pellets showed that two commercially manufactured pellets contained selenium with average grain sizes about 4 and 40 �m respectively. Plasma selenium concentrations in sheep treated with pellets containing the coarse-grained selenium were maintained at higher levels over longer periods of time than those measured for sheep treated with pellets with fine-grained selenium. Pellets removed from sheep after 2, 4, 8, 16 and 28 days showed a progressive increase in the degree of alteration of selenium to a compound of average composition (g/100 g) iron, 33.7; selenium, 51.3 ; oxygen, 15.0. After 28 days only a small percentage of elemental selenium remained in pellets with fine-grained selenium, whereas about 50% remained in pellets with coarse-grained selenium. CSIRO prototype pellets, for which long-term effectiveness had been established, also contained coarse-grained selenium, and remnants of selenium were found in pellets that had been in sheep for periods up to 3 years. Selenium, administered in gelatin capsules or as sachets containing glass-selenium mixtures, was stable under the pH-Eh conditions of the rumen, but was rendered unstable in selenium pellets or iron-selenium mixtures by the presence of iron. It is probable that the most rapid release of selenium to the sheep occurs as a result of a chemical reaction involving the oxidation of iron and concomitant alteration of elemental selenium to iron selenide.


MRS Advances ◽  
2016 ◽  
Vol 1 (12) ◽  
pp. 811-816 ◽  
Author(s):  
Myeong-heom Park ◽  
Akinobu Shibata ◽  
Nobuhiro Tsuji

ABSTRACTIt is well-known that dual phase (DP) steels composed of ferrite and martensite have good ductility and plasticity as well as high strength. Due to their excellent mechanical properties, DP steels are widely used in the industrial field. The mechanical properties of DP steels strongly depend on several factors such as fraction, distribution and grain size of each phase. In this study, the grain size effect on mechanical properties of DP steels was investigated. In order to obtain DP structures with different grain sizes, intercritical heat treatment in ferrite + austenite two-phase region was carried out for ferrite-pearlite structures having coarse and fine ferrite grain sizes. These ferrite-pearlite structures with coarse and fine grains were fabricated by two types of heat treatments; austenitizing heat treatment and repetitive heat treatment. Ferrite grain sizes of the specimens heat-treated by austenitizing and repetitive heat treatment were 47.5 µm (coarse grain) and 4.5 µm (fine grain), respectively. The ferrite grain sizes in the final DP structures fabricated from the coarse-grained and fine-grained ferrite-pearlite structures were 58.3 µm and 4.1µm, respectively. The mechanical behavior of the DP structures with different grain sizes was evaluated by an uniaxial tensile test at room temperature. The local strain distribution in the specimens during tensile test was obtained by a digital image correlation (DIC) technique. Results of the tensile test showed that the fine-grained DP structure had higher strength and larger elongation than the coarse-grained DP structure. It was found by the DIC analysis that the fine-grained DP structure showed homogeneous deformation compared with the coarse-grained DP structure.


2018 ◽  
Vol 2018 ◽  
pp. 1-6 ◽  
Author(s):  
Renjie Wen ◽  
Cai Tan ◽  
Yong Wu ◽  
Chen Wang

Biaxial compression tests with the same specimen size and different maximum grain sizes were simulated for coarse-grained soils using the discrete element method to study the influence of grain size on the mechanical properties and force chain. The maximum grain sizes were 40, 20, 10, and 5 mm, respectively. The grading with self-similar fractal structure in mass is designed to ensure the same pore structure for soils. The shear strength increased with the increase in maximum grain size. Evident increase in shear strength and significant size effect were observed when the ratio of the specimen diameter to maximum grain size was less than five. The shear dilation of coarse-grained soils increases with the increase in maximum grain size. The contact force distribution was uniform when maximum grain size was small but tends to be uneven with the increase in maximum grain size, thereby causing the increase in shear strength by stable strong force chains. This finding demonstrates size effect on the mechanical properties and force chain of cohesionless coarse-grained soils under the biaxial compression condition.


2010 ◽  
Vol 654-656 ◽  
pp. 294-297 ◽  
Author(s):  
Ghasem Dini ◽  
Rintaro Ueji ◽  
Abbas Najafizadeh

The effect of grain size on the flow stress in TWinning Induced Plasticity (TWIP) steel was investigated via the X-ray diffraction (XRD) measurements of dislocation density. The results indicated that the hardening behavior of fine grained samples (mean grain sizes in the range of 2.1-3.8μm) can be described as typical dislocation interactions. However in coarse grained samples (mean grain sizes in the range of 4.7-38.5μm) where extensive mechanical twinning occurs, another strengthening mechanism is required. Consequently, the effect of grain size on the flow stress parameters of the proposed equation was considered and it was found that in the fine grained samples, the Holloman analysis can describe the hardening behavior. However, in coarse grained samples, a second hardening term due to the strengthening effect of mechanical twin boundaries needs to be added to the Holloman equation.


Author(s):  
Alina Vattai ◽  
Nikoletta Rozgonyi-Boissinot

AbstractThe effects of grain size and different multi-stage shearing techniques on shear strength along discontinuities were analyzed in this study. Laboratory direct shear tests were carried out on plaster mortar with maximum grain sizes of 0.5 mm and 1.0 mm. All specimen surfaces were essentially similar, copied from the same natural, Hungarian coarse-grained sandstone joint with a low joint roughness coefficient (JRC = 8). Tests within two different normal stress ranges (σn = 0.25–0.5 and 0.5–1.5 MPa) were performed simultaneously. Specimens tested using the technique involving modified shearing with repositioning were sheared three times while being subjected to the same degree of normal stress (shearing sequence n = 1, 2, 3) and those with multi-stage technique without repositioning were subjected to shearing once at three different degrees of normal stress. The changing values of the peak friction angle calculated from the resulting peak shear strength-normal stress data pairs (τp − σn) were examined. Failure curves were estimated using linear regression, according to the Mohr–Coulomb failure criterion. The differences between the various peak friction angles obtained from experiments in which different multi-stage shearing techniques were used tend to increase in significance with the increasing number of shearing sequences. Peak friction angle values vary according to grain size of the material, though further investigations using more grain sizes are required to establish the extent of the effect on shear strength along discontinuities.


2014 ◽  
Vol 37 ◽  
pp. 27-39 ◽  
Author(s):  
L. Guerit ◽  
L. Barrier ◽  
C. Narteau ◽  
F. Métivier ◽  
Y. Liu ◽  
...  

Abstract. In gravel-bed rivers, sediments are often sorted into patches of different grain-sizes, but in braided streams, the link between this sorting and the channel morpho-sedimentary elements is still unclear. In this study, the size of the bed sediment in the shallow braided gravel-bed Urumqi River is characterized by surface-count and volumetric sampling methods. Three morpho-sedimentary elements are identified in the active threads of the river: chutes at flow constrictions, which pass downstream to anabranches and bars at flow expansions. The surface and surface-layer grain-size distributions of these three elements show that they correspond to only two kinds of grain-size patches: (1) coarse-grained chutes, coarser than the bulk river bed, and (2) finer-grained anabranches and bars, consistent with the bulk river bed. In cross-section, the chute patches are composed of one coarse-grained top layer, which can be interpreted as a local armour layer overlying finer deposits. In contrast, the grain size of the bar-anabranch patches is finer and much more homogeneous in depth than the chute patches. Those patches, which are features of lateral and vertical sorting associated to the transport dynamics that build braided patterns, may be typical of active threads in shallow gravel-bed rivers and should be considered in future works on sorting processes and their geomorphologic and stratigraphic results.


2002 ◽  
Vol 750 ◽  
Author(s):  
Nian Zhang ◽  
Changjin Xie ◽  
Wei Tong

ABSTRACTEffects of the indent depth, the distance between the indent and the grain boundary, grain sizes, and crystallographic orientations on the microhardness of annealed coarse-grained polycrystalline α-brass were investigated using a Vickers indenter with indents much smaller than the α-brass grains (ranging from 80 μm to 550 μm). It is found that the microhardness of α-brass crystals shows a strong dependence on the indentation depth when it is smaller than 5 μm and a very weak dependence on both the distance between the indent and the grain boundary and the grain size when the indentation depth is about 5 μm and more. No significant dependence of the microhardness on the crystallographic orientations was observed in the fourteen grains of different orientations studied in this investigation.


Materials ◽  
2019 ◽  
Vol 12 (23) ◽  
pp. 3956 ◽  
Author(s):  
Baturin ◽  
Lotkov ◽  
Grishkov ◽  
Rodionov ◽  
Kabdylkakov ◽  
...  

The analysis presented here shows that in B2-phase of Ti49.1Ni50.9 (at%) alloy, hydrogenation with further aging at room temperature decreases the temperatures of martensite transformations and then causes their suppression, due to hydrogen diffusion from the surface layer of specimens deep into its bulk. When hydrogen is charged, it first suppresses the transformations B2↔B19′ and R↔B19′ in the surface layer, and when its distribution over the volume becomes uniform, such transformations are suppressed throughout the material. The kinetics of hydrogen redistribution is determined by the hydrogen diffusion coefficient DH, which depends on the grain size. In nanocrystalline Ti49.1Ni50.9 (at%) specimens, DH is three times greater than its value in coarse-grained ones, which is likely due to the larger free volume and larger contribution of hydrogen diffusion along grain boundaries in the nanocrystalline material. According to thermal desorption spectroscopy, two states of hydrogen atoms with low and high activation energies of desorption exist in freshly hydrogenated Ti49.1Ni50.9 (at%) alloy irrespective of the grain size. On aging at room temperature, the low-energy states disappear entirely. Estimates by the Kissinger method are presented for the binding energy of hydrogen in the two states, and the nature of these states in binary hydrogenated TiNi-based alloys is discussed.


Author(s):  
Jie Lian ◽  
Javier Garay ◽  
Junlan Wang

Mechanical properties of fully yttria stabilized zirconia (F-YSZ) with different grain sizes were investigated using instrumented indentation. While the grain size effect on the yield strength was performed on both the coarse-grained and fine-grained F-YSZ, the grain boundary effect was studied on the coarse-grained F-YSZ by performing nanoindentation within the grains and on/near the grain boundaries. Little variations were observed on mechanical properties such as hardness and reduced modulus, interesting results were obtained on the grain boundary effect on the yielding load for the course-grained F-YSZ.


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