The Microstructure and Compression Behavior of Multi-Step Forging Ti-45Al-8Nb Alloy after Annealing at 1100 °C

2013 ◽  
Vol 747-748 ◽  
pp. 111-114
Author(s):  
Lin Song ◽  
Xiang Jun Xu ◽  
Jun Pin Lin ◽  
Lai Qi Zhang
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Annealing Treatment ◽  
Air Cooling ◽  
Test Machine ◽  
Compressive Properties ◽  
Compression Behavior ◽  
Microstructure Change ◽  
Heat Treated ◽  
Before And After

Effects of annealing treatment on microstructure and the compressive properties of hot-worked Ti-45Al-8Nb-(W, B, Y) alloy were investigated. Microstructure of the extrusion plus multi-step forging pancake before and after heat treatment was analyzed by SEM and TEM, respectively. The annealing was conducted by holding samples at 1100°C for 2hrs, and followed by air cooling and furnace cooling. The mechanical properties were measured by Instron test machine. The microstructure evolution during compressive deformation was analyzed by TEM. The results showed that after the annealing the microstructure change could not be observed under SEM but can be observed under TEM. Many dislocation clusters were removed by heat treatment. The heat treated samples had similar compression behaviors with the pancake. TEM investigation showed that the numerous twin intersections occured in γ matrix during compression. The twin spaces tended to decrease as the deformation and the intersection increasing.

scholarly journals Microstructural Tailoring and Enhancement in Compressive Properties of Additive Manufactured Ti-6Al-4V Alloy through Heat Treatment

Materials ◽  
2021 ◽  
Vol 14 (19) ◽  
pp. 5524
Author(s):  
Byungmin Ahn
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Martensite Phase ◽  
Metal Powders ◽  
Compressive Properties ◽  
Laser Additive Manufacturing ◽  
Heat Treated ◽  
Before And After ◽  
Microstructural Studies ◽  
Compressive Tests

Among laser additive manufacturing, selective laser melting (SLM) is one of the most popular methods to produce 3D printing products. The SLM process creates a product by selectively dissolving a layer of powder. However, due to the layerwise printing of metal powders, the initial microstructure is fully acicular α′-martensitic, and mechanical properties of the resultant product are often compromised. In this study, Ti-6Al-4V alloy was prepared using SLM method. The effect of heat treatment was carried out on as-built SLM Ti-6Al-4V alloy from 650–1000 °C to study respective changes in the morphology of α/α′-martensite and mechanical properties. The phase transition temperature was also analyzed through differential thermal analysis (DTA), and the microstructural studies were undertaken by optical microscopy (OM) and scanning electron microscopy (SEM). The mechanical properties were assessed by microhardness and compressive tests before and after heat treatment. The results showed that heat treated samples resulted in a reduction in interior defects and pores and turned the morphology of the α′-martensite into a lamellar (α + β) structure. The strength was significantly reduced after heat treatment, but the elongation was improved due to the reduction in columnar α′-martensite phase. An optimum set of strength and elongation was found at 900 °C.

Influence of Heat Treatment on Microstrudture and Mechanical Properties of AZ31B Magnesium Alloy Prepared by Solid-State Recycling

2012 ◽  
Vol 271-272 ◽  
pp. 17-20
Author(s):  
Shu Yan Wu ◽  
Ze Sheng Ji ◽  
Chun Ying Tian ◽  
Ming Zhong Wu
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Solid State ◽  
Magnesium Alloy ◽  
Static Recrystallization ◽  
Annealing Treatment ◽  
Az31b Magnesium Alloy ◽  
Heat Treated ◽  
Elongation To Failure ◽  
Strength And Ductility

This work is to study the influence of heat treatment on microstrudture and mechanical properties of AZ31B magnesium alloy prepared by solid -state recycling. AZ31B magnesium alloy chips were recycled by hot extruding. Three different heat treatments were conducted for recycled alloy. Mechanical properties and microstructure of the recycled specimen and heat treated specimen were investigated. 300°C×2h annealing specimen exhibits finer grain due to static recrystallization, and microstructure of 400°C×2h annealing specimen becomes more coarse. 300°C×2h annealing treatment improves obviously strength and ductility of recycled alloy. Ultimate tensile strength of alloy decreases and elongation to failure increases after 400°C×2h annealing. Grain size, dislocation density and bonding of chips have an effect on the elongation of recycled materials. 190°C×8h ageing has no influence on microstructure and mechanical properties of recycled alloy.

scholarly journals The Effect of Cooling Rate on Mechanical Properties of Carbon Steel (St 35)

2014 ◽  
Vol 7 (1) ◽  
pp. 109-118
Author(s):  
Jenan Mohammed Nagie
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Grain Size ◽  
Carbon Steel ◽  
Cooling Rate ◽  
Experimental Results ◽  
Heat Treated ◽  
Before And After ◽  
Water Media ◽  
The Relationship

This paper is aimed to study the effect of cooling rate on mechanical properties of Steel 35. Specimens prepared to apply tensile, torsion, impact and hardness tests.Many prepared specimens heat treated at (850ºC) for one hour and subsequently were cooled by three different media [Water-Air-furnace] to show the effect of Medias cooling rate on mechanical properties. Microstructures of all specimens examined before and after heat treatment by an optical microscopy.To figure the phases obtained after heat treatment and its effect on the mechanical properties Experimental results have shown that the microstructure of steel can be changed and significantly improved by varying line cooling rate thus, improving one property will effect on the others because of the relationship between all properties.In water media tensile, torsion and hardness improved while impact results reduced. Air media contributed in improving most of the mechanical properties because of grain size homogeneity. At furnace media ductility and impact improved

Microstructural Evolution and Mechanical Properties of Modified 9%Cr-1%Mo Steel upon Isothermal Heat-Treatment

2005 ◽  
Vol 475-479 ◽  
pp. 81-84
Author(s):  
Sung Kang Hur ◽  
Kee Sam Shin ◽  
Jung Hoon Yoo ◽  
Ja Min Koo ◽  
Soo Lee ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Mechanical Property ◽  
Microstructural Evolution ◽  
Heat Treating ◽  
Air Cooling ◽  
Isothermal Heat Treatment ◽  
Martensitic Structure ◽  
Heat Treated ◽  
Evolution Of Microstructure

The evolution of microstructure and its effects on the mechanical properties of modified 9%Cr-1%Mo steel during heat-treating at 1050°C for 15 min and then isothermal heat treatment at 380~760°C with subsequent air-cooling have been investigated. For the microstructural and mechanical property analyses, OM, SEM, EDS, XRD, hardness and impact tests were used. In accordance with the severity of the heat-treatment, the microstructure evolved from the untransformed martensite to the partially transformed dual phases of martensite and ferrite, and then fully transformed to ferrite. Impact values at ambient temperature for specimens isothermally heat-treated at 320 - 380°C, predominantly at about 350°C were lower than others’ with similar martensitic structure. The partially transformed specimens with dual phases of martensite and ferrite also showed lower impact values than samples with untransformed with martensitic, and transformed with ferritic structures.

Effect of Postweld Heat Treatment on the Mechanical Properties of Weld in a Medium Carbon Steel

2013 ◽  
Vol 315 ◽  
pp. 6-10 ◽  
Author(s):  
S.M. Manladan ◽  
B.O. Onyekpe
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Carbon Steel ◽  
Postweld Heat Treatment ◽  
Medium Carbon Steel ◽  
Air Cooling ◽  
Shielded Metal Arc Welding ◽  
Medium Carbon ◽  
Before And After ◽  
Postweld Heat

This paper presents the result of an investigation of the effect of postweld heat treatment on the mechanical properties of weld in 0.36%C medium Carbon Steel. Samples were prepared and welded using Shielded Metal Arc Welding (SMAW) process with a low hydrogen electrode. The welded samples were subjected to postweld heat treatment (stress relief) at four different temperatures: 550°C, 600°C, 650°C and 700°C followed by air-cooling. Microstructural examination was carried out to determine the change in microstructure before and after postweld heat treatment. The mechanical properties of the samples were also tested before and after the heat treatment. It was established that a hard microstructure, susceptible to Hydrogen Induced Cracking (HIC), was formed in the heat affected zone of the as-welded samples and that postweld heat treatment improved the mechanical properties of the weld and substantially reduced or eliminated the risk of HIC.

AN APPROXIMATION TO DETERMINE CORROSION AND MECHANICAL BEHAVIOR OF TI-BASED ALLOYS

2020 ◽  
pp. 2150001
Author(s):  
YESIM YILMAZ ◽  
HULYA DEMIROREN
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Corrosion Resistance ◽  
High Corrosion Resistance ◽  
Commercially Pure ◽  
Grade 5 ◽  
Heat Treated ◽  
Before And After ◽  
Mechanical Properties And Corrosion ◽  
Cp Ti

Titanium and its alloys used in biomaterial applications are preferrably the cause of high-corrosion resistance properties in addition to having good mechanical properties. Commercially pure Ti (CP-Ti) (Grade 2), Ti6Al4V (Grade 5) and Ti6Al4V-ELI (Grade 23) samples are used as biomaterials exposed to 750°C and 1060°C for 1[Formula: see text]h. The samples were cooled in air after heat treatment at 750°C, the other samples were cooled in water after heat treatment at 1060°C. The free-heat treatment samples are as producted. Microstructures of heat-treated samples and non-made samples by comparison were evaluated before and after corrosion process microstructures and tensile strengths. Test solution is 0.5[Formula: see text]mol H2SO[Formula: see text][Formula: see text]mol HCl mixture. The corrosion resistance of the titanium samples was evaluated. Microstructure images were monitorized on optical and SEM microscopes. In this paper, the effect of heat treatment was determined on the microstructure, mechanical properties and corrosion resistances of the material. As a result, heat treatment is useful on corrosion resistance of alloyed samples.

Influence of Heat Treatment on Impact, Hardness and Fatigue Strength of 6061 Aluminium Alloy

2015 ◽  
Vol 761 ◽  
pp. 484-488 ◽  
Author(s):  
Nurulhilmi Zaiedah Nasir ◽  
Mohd Ahadlin Mohd Daud ◽  
Omar Bapokutty ◽  
Abdul Talib Din ◽  
Mohd Zulkefli Selamat
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Aluminum Alloy ◽  
Fatigue Strength ◽  
Heat Treated ◽  
Before And After ◽  
Temperature Levels ◽  
Number Of Cycles ◽  
6061 Aluminium Alloy ◽  
Alloy 6061

This paper presents effects of heat treatment on toughness, hardness and fatigue strength of aluminum alloy 6061. The alloy specimens were heat treated in the furnace at different temperature levels and holding times; and then cooled in different media (water and oil). The mechanical properties such as hardness, impact and fatigue were examined using standard method. Result shows that mechanical properties of aluminum alloy can be improved by the heat treatment. It was found that through ageing processes at temperature 160 °C for one, three and five hours, decreased the hardness, while increased the toughness. The fatigue strength was decreased when the number of cycles increased. The fracture surfaces between specimens have a different appearance before and after heat treatment.

Effect of Mg, Sr, Ti and Aging Parameters on the Mechanical Behavior of 319 Alloys in the T5 and T6 Heat Treatment

2012 ◽  
Vol 482-484 ◽  
pp. 2275-2288
Author(s):  
Saleh Alkahtani
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Aging Treatment ◽  
Magnesium Content ◽  
Air Cooling ◽  
Particle Spacing ◽  
Sr Modification ◽  
Heat Treated ◽  
Negative Effect ◽  
Mg Content

In this work, the effect of metallurgical parameters (i.e. alloy chemistry and aging parameters) on the mechanical properties of 319 alloys was investigated, with the aim of adjusting these parameters to produce castings of suitable mechanical properties. An attempt has been made to quantify the effects of alloying elements (Mg, Sr, and Ti) and aging parameters on the mechanical properties of heat-treated (T5 and T6) 319 alloys. Exploring the heat treatment differences between T5 and T6 for 319 alloys would help in selecting the metallurgical conditions required to achieve the optimum and maximum mechanical properties. Aging treatments were carried out for 319 alloys in the T5- and T6-condition at 150°C, 180°C, 200°C, 220°C and 250°C for 4, 8, 16, 24 and 48 h, followed by air cooling. Aging treatment at a lower temperature of 150°C produces fine and dense precipitates having a smaller inter-particle spacing, while at higher aging temperatures, such as 250°C, the precipitates are coarser in size, less dense, and more widely dispersed. For 319 alloys, crack initiate and propagate mainly through the debonding of Si particles from the Al matrix and through the cleavage of β-iron intermetallics. Fracture of intermetallic phases in the interdendritic regions is mostly brittle, with the formation of microcracks at the Si, Cu, Fe-base intermetallics and aluminium interfaces. Experimental correlations of the results obtained from the mechanical properties measurements are analyzed and correlations that relate the alloying additions and heat treatment to the ultimate tensile strength (UTS), yield strength (YS) and total percent elongation (%E) of such alloys are found. Different levels of magnesium content (%Mg), Sr-modification (Sr-ppm), aging parameters (temperature and time) were tested. The effect of alloy additions (Mg, Sr and Ti) and aging heat treatment parameters (Temperature and Time) on the mechanical properties and alloy performance of cast and heat treated 319 alloys are investigated. It was found that the strength of 319 alloys increases with the magnesium content and decreases with the Sr-modification (Sr-ppm) and aging parameters (temperature and time). Increasing the Mg content in primary 319 alloys up to 0.45% enhances the alloy response to heat treatment in the T5 and T6 Tempers, more particularly, the T6 one. Sr-Modification of high Mg content 319 alloy in amounts of ~360 ppm leads to a noticeable decline in alloy strength due to porosity formation which counteracts the beneficial effect of the modification. Sr-modification has a negative effect on the % elongation results of Mg-content 319 alloys due to the Mg-Sr interaction in the aged-T6 conditions. However, grain refining of the Mg and Sr content 319 alloys produce sounder castings with finer grain sizes

Crystallographic Differences of Metastable NI2MO in a NI-MO-AL Superalloy

1980 ◽  
Vol 38 ◽  
pp. 158-159
Author(s):  
Michael M. Kersker ◽  
E. A. Aigeltinger ◽  
J. J. IIren
Keyword(s):  
Mechanical Properties ◽  
Air Cooling ◽  
Solution Treated ◽  
Heat Treated ◽  
Metastable Compounds ◽  
Rapidly Solidified

Ni-rich alloys based on approximate ternary composition Ni-8Mo-15A1 (at%) are presently under investigation in an attempt to study the contribution, if any, of the profusion of Mo-rich NixMo metastable compounds that these alloys contain to their excellent mechanical properties. One of the alloys containing metastable NixMo precipitates is RSR 197 of composition Ni-8.96Mo-15.06A1-1.98Ta-.015Yt. The alloy was prepared at Pratt and Whitney Government Products Division, West Palm Beach, Florida, from rapidly solidified powder. The powder was canned under inert conditions and extruded as rod at 1315°C. The as-extruded rod, after air cooling, was solution treated at 1315°C for two hours, air cooled, and heat treated for one hour at 815°C, followed again by air cooling.

scholarly journals Influence of Post Weld Heat Treatment on the Grain Size, and Mechanical Properties of the Alloy-800H Rotary Friction Weld Joints

Materials ◽  
2021 ◽  
Vol 14 (16) ◽  
pp. 4366
Author(s):  
Saqib Anwar ◽  
Ateekh Ur Rehman ◽  
Yusuf Usmani ◽  
Ali M. Al-Samhan
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Grain Size ◽  
Heat Affected Zone ◽  
Tensile Testing ◽  
Weld Zone ◽  
Alloy 800H ◽  
Weld Joints ◽  
Heat Treated ◽  
Friction Weld

This study evaluated the microstructure, grain size, and mechanical properties of the alloy 800H rotary friction welds in as-welded and post-weld heat-treated conditions. The standards for the alloy 800H not only specify the composition and mechanical properties but also the minimum grain sizes. This is because these alloys are mostly used in creep resisting applications. The dynamic recrystallization of the highly strained and plasticized material during friction welding resulted in the fine grain structure (20 ± 2 µm) in the weld zone. However, a small increase in grain size was observed in the heat-affected zone of the weldment with a slight decrease in hardness compared to the base metal. Post-weld solution heat treatment (PWHT) of the friction weld joints increased the grain size (42 ± 4 µm) in the weld zone. Both as-welded and post-weld solution heat-treated friction weld joints failed in the heat-affected zone during the room temperature tensile testing and showed a lower yield strength and ultimate tensile strength than the base metal. A fracture analysis of the failed tensile samples revealed ductile fracture features. However, in high-temperature tensile testing, post-weld solution heat-treated joints exhibited superior elongation and strength compared to the as-welded joints due to the increase in the grain size of the weld metal. It was demonstrated in this study that the minimum grain size requirement of the alloy 800H friction weld joints could be successfully met by PWHT with improved strength and elongation, especially at high temperatures.

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