Microstructure and Tensile Properties of 1-D Forged (TiB+TiC)/Ti Composite

2013 ◽  
Vol 747-748 ◽  
pp. 926-931 ◽  
Author(s):  
Chang Jiang Zhang ◽  
Fan Tao Kong ◽  
Shu Long Xiao ◽  
Li Juan Xu ◽  
Yuong Chen ◽  
...  
Keyword(s):  
High Temperature ◽  
Aspect Ratio ◽  
Grain Boundaries ◽  
Tensile Properties ◽  
Room Temperature ◽  
Fracture Mechanisms ◽  
Cast Composite ◽  
Temperature Fracture ◽  
Cast Microstructure

In this work, 2.5vol. % (TiB+TiC)/Ti composite was prepared by in situ casting route then 1-D forging. The microstructure and tensile properties were presented and discussed. The results indicate that the as cast microstructure can be significantly modified by 1-D forging. After forging, TiB and TiC segregated at the prior β grain boundaries within the as-cast composite tend to fracture and align perpendicular to forging direction. Reduction in aspect ratio of reinforcements and α lath is also observed. 1-D forging can enhance the strength and elongation of as cast composite significantly. However, the increment in strength is quite limited as strain temperature increases to 700 °C. Additionally, room temperature and high temperature fracture mechanisms are also discussed.

Analyses of Eutectoid Phase Transformations in Nb–SilicideIn SituComposites

2004 ◽  
Vol 10 (4) ◽  
pp. 470-480 ◽  
Author(s):  
B.P. Bewlay ◽  
S.D. Sitzman ◽  
L.N. Brewer ◽  
M.R. Jackson
Keyword(s):  
Crystal Structure ◽  
Phase Transformation ◽  
High Temperature ◽  
Room Temperature ◽  
Bulk Composition ◽  
High Strength ◽  
Eutectoid Decomposition ◽  
Quaternary Alloys ◽  
Temperature Fracture

Nb–silicide in situ composites have great potential for high-temperature turbine applications. Nb–silicide composites consist of a ductile Nb-based solid solution together with high-strength silicides, such as Nb5Si3and Nb3Si. With the appropriate addition of alloying elements, such as Ti, Hf, Cr, and Al, it is possible to achieve a promising balance of room-temperature fracture toughness, high-temperature creep performance, and oxidation resistance. In Nb–silicide composites generated from metal-rich binary Nb-Si alloys, Nb3Si is unstable and experiences eutectoid decomposition to Nb and Nb5Si3. At high Ti concentrations, Nb3Si is stabilized to room temperature, and the eutectoid decomposition is suppressed. However, the effect of both Ti and Hf additions in quaternary alloys has not been investigated previously. The present article describes the discovery of a low-temperature eutectoid phase transformation during which (Nb)3Si decomposes into (Nb) and (Nb)5Si3, where the (Nb)5Si3possesses the hP16 crystal structure, as opposed to the tI32 crystal structure observed in binary Nb5Si3. The Ti and Hf concentrations were adjusted over the ranges of 21 to 33 (at.%) and 7.5 to 33 (at.%) to understand the effect of bulk composition on the phases present and the eutectoid phase transformation.

Grain Boundaries and Interfaces in MoSi2 and MoSi2-SiC Composites and Their Effect on High Temperature Strength

2000 ◽  
Vol 6 (S2) ◽  
pp. 424-425
Author(s):  
R. Mitra ◽  
W.-A. Chiou ◽  
A. Venugopal Rao
Keyword(s):  
High Temperature ◽  
Grain Boundaries ◽  
Weight Fraction ◽  
High Temperature Strength ◽  
High Melting Point ◽  
Temperature Oxidation ◽  
Structural Applications ◽  
Temperature Fracture ◽  
Sic Composites

Molybdenum di-silicides (MoSi2) based materials have a strong potential for high temperature structural applications due to high melting point of 2030°C, outstanding elevated temperature oxidation resistance and limited ductility above a temperature range of 1100-1300°C. The major shortcomings of MoSi2 for structural applications are its poor room temperature fracture toughness and low high temperature strength. Sustained efforts including reinforcing MoSi2 with ceramic reinforcements, alloying and in-situ processing, have been made to improve these properties. The purity of grain boundaries and interfaces, which in turn depends on the processing method plays a significant role in the high temperature properties and this paper aims to show that.Intimately mixed Mo and Si powders (Mo:Si = 63:37 by weight fraction) were reaction hot pressed (“RHP“) in vacuum at 1500°C for 1 h, using a pressure of 26 MPa. During the hot pressing process, Mo and Si reacted to form MoSi2.

Effects of Re Alloying on Mechanical Properties of In-Situ Composites with Base Composition of Nb-18Si-2HfC

2006 ◽  
Vol 306-308 ◽  
pp. 941-946
Author(s):  
Sheng Wu Wang ◽  
Tatsuo Tabaru ◽  
Hisatoshi Hirai ◽  
Hideto Ueno
Keyword(s):  
Mechanical Properties ◽  
Fracture Toughness ◽  
High Temperature ◽  
Base Composition ◽  
Room Temperature ◽  
High Temperature Strength ◽  
Strengthening Effect ◽  
In Situ Composites ◽  
Temperature Fracture

Nb-base in-situ composites with the base composition of Nb-18Si-2HfC were prepared by conventional arc-melting. Their microstructures and mechanical properties, such as high-temperature strength and room temperature fracture toughness, were investigated to elucidate the effects of Re alloying. The in-situ composites predominantly have eutectic microstructures consisting of an Nb solid solution (NbSS) and Nb5Si3. The compressive strength increased with the increasing Re contents at 1470K and not at 1670 K. The strengthening effect observed at 1470 K is higher than that by W and Mo. Re alloying of about 2 % is valuable for improving both the high temperature strength and room temperature fracture toughness of Nb-18Si-2HfC base materials.

Tensile Behaviour of Al-Si Alloy and Al-Si/Graphite Composites at Elevated Temperatures

2012 ◽  
Vol 710 ◽  
pp. 457-462 ◽  
Author(s):  
G. Rajaram ◽  
S. Kumaran ◽  
T Srinivas Rao
Keyword(s):  
High Temperature ◽  
Room Temperature ◽  
Elevated Temperatures ◽  
Matrix Alloy ◽  
Tensile Behaviour ◽  
Fracture Mechanisms ◽  
Strain Hardening Exponent ◽  
Transition Elements ◽  
Softening Effect ◽  
Graphite Composite

The high temperature tensile behaviour of Al-Si alloy and two of its composite systems with graphite as major reinforcement were investigated. The composites were developed by the stir casting method, wherein a mixture of graphite (3 wt %) and Cu / Ni (2 wt% each) were added into the molten Al-Si alloy to fabricate two systems such as Al-Si-Cu/graphite composite and Al-Si-Ni/graphite composite. The properties of composites were better than that of the matrix alloy. Tensile behaviour of alloy and composites were studied at different temperatures from room temperature to 300°C. It is found that the tensile strength of the alloy and composites were decreasing with increase in temperature. The transition elements (Cu / Ni) have played the key role in improving the ultimate tensile and yield strength of the composites over the alloy. The flow stress of the composite is more than that of the alloy. The strain hardening exponent value continuously drops with the increase of tensile temperature due to the thermal softening effect. The % elongation of the alloy is more than that of the composites. Fracture surfaces of the samples are analyzed by scanning electron microscope to understand the fracture mechanisms. Fractography reveals that the fracture behaviour of the alloy changes from cleavage mode at room temperature to complete ductile mode at high temperature.

Effect of High Temperature Caliber Rolling on Microstructure and Room Temperature Tensile Properties of Mg-3Al-1Zn (AZ31) Alloy

2013 ◽  
Vol 209 ◽  
pp. 6-9 ◽  
Author(s):  
Rajendra Doiphode ◽  
S.V.S. Narayana Murty ◽  
Nityanand Prabhu ◽  
Bhagwati Prasad Kashyap
Keyword(s):  
Tensile Strength ◽  
High Temperature ◽  
Yield Strength ◽  
Strain Rate ◽  
Tensile Properties ◽  
Room Temperature ◽  
Tensile Tests ◽  
Az31 Alloy ◽  
Rolling Temperature ◽  
Grain Sizes

Mg-3Al-1Zn (AZ31) alloy was caliber rolled at 250, 300, 350, 400 and 450 °C. The effects of caliber rolling temperature on the microstructure and tensile properties were investigated. The room temperature tensile tests were carried out to failure at a strain rate of 1 x 10-4s-1. The nature of stress-strain curves obtained was found to vary with the temperature employed in caliber rolling. The yield strength and tensile strength followed a sinusoidal behaviour with increasing caliber rolling temperature but no such trend was noted in ductility. These variations in tensile properties were explained by the varying grain sizes obtained as a function of caliber rolling temperature.

scholarly journals Improvement of High Temperature Wear Behavior of In-Situ Cr3C2-20 wt. % Ni Cermet by Adding Mo

Crystals ◽  
2020 ◽  
Vol 10 (8) ◽  
pp. 682
Author(s):  
Liang Sun ◽  
Wenyan Zhai ◽  
Hui Dong ◽  
Yiran Wang ◽  
Lin He
Keyword(s):  
Wear Resistance ◽  
High Temperature ◽  
Wear Mechanism ◽  
Room Temperature ◽  
Wear Behavior ◽  
Ceramic Particle ◽  
High Temperature Wear ◽  
The Coefficient Of Friction ◽  
Mo Content

Cr3C2-Ni cermet is a kind of promising material especially for wear applications due to its excellent wear resistance. However, researches were mainly concentrated on the experiment condition of room temperature, besides high-temperature wear mechanism of the cermet would be utilized much potential applications and also lack of consideration. In present paper, the influence of Mo content on the high-temperature wear behavior of in-situ Cr3C2-20 wt. % Ni cermet was investigated systematically. The friction-wear experiment was carried out range from room temperature to 800 °C, while Al2O3 ceramic was set as the counterpart. According to experimental results, it is indicated that the coefficient of friction (COF) of friction pairs risen at the beginning of friction stage and then declined to constant, while the wear rate of Cr3C2-20 wt. % Ni cermet risen continuously along with temperature increased, which attributes to the converted wear mechanism generally from typical abrasive wear to severe oxidation and adhesive wear. Generally, the result of wear resistance was enhanced for 13.4% (at 400 °C) and 31.5% (at 800 °C) by adding 1 wt. % Mo. The in-situ newly formed (Cr, Mo)7C3 ceramic particle and the lubrication phase of MoO3 can effectively improve the wear resistance of Cr3C2-20 wt. % Ni cermet.

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