Long-Term Creep and Impact Strength of Biocompatible 3D-Printed PLA-Based Scaffolds

2017 ◽  
Vol 13 ◽  
pp. 15-20 ◽  
Author(s):  
Kirill V. Niaza ◽  
Fedor S. Senatov ◽  
Andrey Stepashkin ◽  
Natalia Yu. Anisimova ◽  
Mikhail V. Kiselevsky
Keyword(s):  
Mechanical Properties ◽  
Charpy Impact ◽  
Bone Defects ◽  
Porous Scaffolds ◽  
Fabrication Method ◽  
Fused Filament Fabrication ◽  
3D Printed ◽  
Term Creep ◽  
Small Bone

In the present work porous scaffolds for trabecular bone defects replacement were studied. PLA and PLA/HA сomposites were obtained by extrusion. Scaffolds were obtained by 3D-printing by fused filament fabrication method. Long-term creep and Charpy impact tests show that PLA/HA scaffolds with the maximum force for destruction at impact of 119 N can function under a load of up to 10 MPa without shape changing and loss of mechanical properties. In vivo tests were used to investigate biocompatibility of scaffolds. The scaffolds may be used as implants for unloaded small bone defects replacement

Temperature-compensated constitutive model of fused filament fabrication 3D printed PLA materials with full extrusion temperatures

2021 ◽  
Vol ahead-of-print (ahead-of-print) ◽  
Author(s):  
Kaiyang Zhu ◽  
Zichen Deng ◽  
Shi Dai ◽  
Yajun Yu
Keyword(s):  
Mechanical Properties ◽  
Thermal Decomposition ◽  
Constitutive Model ◽  
Polylactic Acid ◽  
Extrusion Temperature ◽  
Fused Filament Fabrication ◽  
Printing Process ◽  
Content Type ◽  
3D Printed ◽  
Interlayer Bonding

Purpose This study aims to focus on the effect of interlayer bonding and thermal decomposition on the mechanical properties of fused filament fabrication-printed polylactic acid specimens at high extrusion temperatures. Design/methodology/approach A printing process, that is simultaneous manufacturing of contour and specimen, is used to improve the printing accuracy at high extrusion temperatures. The effects of the extrusion temperature on the mechanical properties of the interlayer and intra-layer are evaluated via tensile experiments. In addition, the microstructure evolution affected by the extrusion temperature is observed using scanning electron microscopy. Findings The results show that the extrusion temperature can effectively improve the interlayer bonding property; however, the mechanical properties of the specimen for extrusion temperatures higher than 270°C may worsen owing to the thermal decomposition of the polylactic acid (PLA) material. The optimum extrusion temperature of PLA material in the three-dimensional (3D) printing process is recommended to be 250–270°C. Originality/value A temperature-compensated constitutive model for 3D printed PLA material under different extrusion temperatures is proposed. The present work facilitates the prediction of the mechanical properties of specimens at an extrusion temperature for different printing temperatures and different layers.

Stiffness prediction of 3D printed fiber-reinforced thermoplastic composites

2019 ◽  
Vol 26 (3) ◽  
pp. 549-555
Author(s):  
Jin Young Choi ◽  
Mark Timothy Kortschot
Keyword(s):  
Mechanical Properties ◽  
Extrusion Direction ◽  
Analytical Models ◽  
Thermoplastic Composites ◽  
Fiber Reinforced ◽  
Flat Plates ◽  
Fused Filament Fabrication ◽  
Element Analysis ◽  
Content Type ◽  
3D Printed

Purpose The purpose of this study is to confirm that the stiffness of fused filament fabrication (FFF) three-dimensionally (3D) printed fiber-reinforced thermoplastic (FRP) materials can be predicted using classical laminate theory (CLT), and to subsequently use the model to demonstrate its potential to improve the mechanical properties of FFF 3D printed parts intended for load-bearing applications. Design/methodology/approach The porosity and the fiber orientation in specimens printed with carbon fiber reinforced filament were calculated from micro-computed tomography (µCT) images. The infill portion of the sample was modeled using CLT, while the perimeter contour portion was modeled with a rule of mixtures (ROM) approach. Findings The µCT scan images showed that a low porosity of 0.7 ± 0.1% was achieved, and the fibers were highly oriented in the filament extrusion direction. CLT and ROM were effective analytical models to predict the elastic modulus and Poisson’s ratio of FFF 3D printed FRP laminates. Research limitations/implications In this study, the CLT model was only used to predict the properties of flat plates. Once the in-plane properties are known, however, they can be used in a finite element analysis to predict the behavior of plate and shell structures. Practical implications By controlling the raster orientation, the mechanical properties of a FFF part can be optimized for the intended application. Originality/value Before this study, CLT had not been validated for FFF 3D printed FRPs. CLT can be used to help designers tailor the raster pattern of each layer for specific stiffness requirements.

scholarly journals Effect of Porosity and Crystallinity on 3D Printed PLA Properties

Polymers ◽  
2019 ◽  
Vol 11 (9) ◽  
pp. 1487 ◽  
Author(s):  
Yuhan Liao ◽  
Chang Liu ◽  
Bartolomeo Coppola ◽  
Giuseppina Barra ◽  
Luciano Di Maio ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Additive Manufacturing ◽  
3D Printing ◽  
Polylactic Acid ◽  
Complex Geometry ◽  
Fused Filament Fabrication ◽  
3D Printed ◽  
Physical Changes ◽  
Crystalline Forms

Additive manufacturing (AM) is a promising technology for the rapid tooling and fabrication of complex geometry components. Among all AM techniques, fused filament fabrication (FFF) is the most widely used technique for polymers. However, the consistency and properties control of the FFF product remains a challenging issue. This study aims to investigate physical changes during the 3D printing of polylactic acid (PLA). The correlations between the porosity, crystallinity and mechanical properties of the printed parts were studied. Moreover, the effects of the build-platform temperature were investigated. The experimental results confirmed the anisotropy of printed objects due to the occurrence of orientation phenomena during the filament deposition and the formation both of ordered and disordered crystalline forms (α and δ, respectively). A heat treatment post-3D printing was proposed as an effective method to improve mechanical properties by optimizing the crystallinity (transforming the δ form into the α one) and overcoming the anisotropy of the 3D printed object.

Investigation of future 3D printed brace design parameters: evaluation of mechanical properties and prototype outcomes

2019 ◽  
Vol 3 (4) ◽  
pp. 171-184
Author(s):  
Kenwick JL Ng ◽  
Kajsa Duke ◽  
Edmond Lou
Keyword(s):  
Mechanical Properties ◽  
Mechanical Characteristics ◽  
Treatment Effectiveness ◽  
Design Parameters ◽  
Wear Comfort ◽  
Polypropylene Material ◽  
Spinal Brace ◽  
3D Printed ◽  
Opening And Closing

Aim: Spinal brace wear time affects treatment effectiveness of adolescent idiopathic scoliosis but remains challenging with the brace’s bulkiness. This study aims to determine the appropriate material and thickness to improve wear comfort. Materials & methods: Thirty-one specimens were tested with 13 ULTEM1010 and 13 Nylon12 potential materials and 5 standard polypropylene material in 2.5, 3.25 and 4 mm thicknesses to evaluate mechanical properties. Donning tests of ULTEM1010 and Nylon12 printed braces were conducted. Results: Nylon12 with 2.5–3.25 mm thickness had higher flexibility and the closest mechanical characteristics as 4-mm thick polypropylene. ULTEM1010 brace fractured after 615-times and Nylon12 brace handled 2920-times of opening and closing. Conclusion: Nylon12, 2.5–3.25 mm are appropriate design parameters. Further clinical study can validate long term brace effectiveness.

Mechanical properties and shape memory effect of 3D-printed PLA-based porous scaffolds

2016 ◽  
Vol 57 ◽  
pp. 139-148 ◽  
Author(s):  
F.S. Senatov ◽  
K.V. Niaza ◽  
M.Yu. Zadorozhnyy ◽  
A.V. Maksimkin ◽  
S.D. Kaloshkin ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Shape Memory ◽  
Shape Memory Effect ◽  
Memory Effect ◽  
Porous Scaffolds ◽  
3D Printed

Shape Recovery Characteristics of 3D Printed Soft Polymers and Their Composites

2016 ◽  
Author(s):  
Wenbo Liu ◽  
Nan Wu ◽  
Kishore Pochiraju
Keyword(s):  
High Resolution ◽  
Shape Memory ◽  
Recovery Time ◽  
Shape Recovery ◽  
Recovery Process ◽  
Hot Water ◽  
Recovery Ratio ◽  
3D Printed ◽  
Term Creep

Shape memory polymers can be triggered to assume memorized shapes from temporarily deformed forms using thermal stimuli. This paper focuses on the characterization of the shape memory behaviors observed in selected 3D printable photo-cured polymer parts and filament with specified fillers. The shape recovery ratio and recovery time were analyzed using 3D printed specimens with 90° bends. Parts with the mixture of selected commercially available polymers — a rigid polymer (RP) and two digitally mixed polymer blends (DB-A and DB-B) were 3D-printed on a multi-material 3D printer capable of producing digital materials with variable mix ratios. The recovery ratios were determined after thermal triggering and after long-term creep (self-recovery) without thermal triggering. The 3D printed parts were heated to above their glass transaction temperature to train temporary shapes and the recovery of original shapes after a thermal trigger was monitored using a high-resolution camera. Long-term self-recovery (non-triggered) was also studied by observing the parts after temporary shape has been trained, as the try to regain their original shape over several days of slow recovery. The recovery of bending angles was quantitatively recorded from the images taken during the shape recovery process. The recovery due to thermal triggers was monitored under a high resolution microscope by reheating with hot water at 90°C. Experiments of long-term self-recovery at room temperature included monitoring of several parts by taking periodic images of the specimens using a resolution camera. The effect of inclusion of fillers on the shape recovery characteristics was also investigated. Silicon Carbide (SiC) with different weight fractions were mixed into PLA powders. Continuous filaments were extruded using a single screw extruder. The recovery time of thermal activation recovery was then characterized to determine the effect of addition of the fillers. The effect of material-mix ratio, initial printed orientation, filler type on the recovery ratio and recovery time are described in this paper.

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