Effects of Modified Solution Heat Treatment on δ- Phase and Low Cycle Fatigue Properties of Inconel 718 Alloy

2006 ◽  
Vol 118 ◽  
pp. 71-76 ◽  
Author(s):  
Jae Keun Hong ◽  
Ji Hong Park ◽  
Nho Kwang Park ◽  
Seong Jun Kim ◽  
Chung Yun Kang

Effects of solution treatment on the microstructure and mechanical properties in wrought Alloy 718 were investigated. For the improvement of tensile and fatigue properties of wrought Alloy 718, a modified solution heat treatment(MSHT), heating at 1000 for 3 minutes followed by furnace cooling at the rate of 3/minute and holding at 985 for 8 minutes, was proposed. This treatment was performed repeatedly 3 times and the samples were subject to the standard aging treatment. For the purpose of comparison, a standard heat treatment(SHT) was also performed. The microstructures of modified solution heat treated specimens showed that small spherical shaped δ- phases were precipitated without grain growth, and the amount of δ-phases was smaller than that of standard heat treated specimens. However, the δ-phases of the standard heat-treated specimen showed needle-like morphologies. Tensile and low cycle fatigue tests were performed on both modified heat-treated and standard heat-treated specimens at room temperature, 350 and 650. Low cycle fatigue tests on the modified heat treated specimens showed promising results without reduction of strength. However, the tensile properties of modified solution treated specimens was almost the same as those of standard heat treated materials both at room temperature and 650.

Materials ◽  
2021 ◽  
Vol 14 (15) ◽  
pp. 4237
Author(s):  
Takuma Tanaka ◽  
Togo Sugioka ◽  
Tatsuya Kobayashi ◽  
Ikuo Shohji ◽  
Yuya Shimada ◽  
...  

The effect of heat treatment on tensile and low cycle fatigue properties of the oxygen-free copper for electric power equipment was investigated. The heat treatment at 850 °C for 20 min, which corresponds to the vacuum brazing process, caused the grain growth and relaxation of strain by recrystallization, and thus, the residual stress in the oxygen-free copper was reduced. The tensile strength and 0.2% proof stress were decreased, and elongation was increased by the heat treatment accompanying recrystallization. The plastic strain in the heat-treated specimen was increased compared with that in the untreated specimen under the same stress amplitude condition, and thus, the low cycle fatigue life of the oxygen-free copper was degraded by the heat treatment. Striation was observed in the crack initiation area of the fractured surface in the case of the stress amplitude less than 100 MPa regardless of the presence of the heat treatment. With an increase in the stress amplitude, the river pattern and the quasicleavage fracture were mainly observed in the fracture surfaces of the untreated specimens, and they were observed with striations in the fracture surfaces of the heat-treated ones. The result of the electron backscattered diffraction (EBSD) analysis showed that the grain reference orientation deviation (GROD) map was confirmed to be effective to investigate the fatigue damage degree in the grain by low cycle fatigue. In addition, the EBSD analysis revealed that the grains were deformed, and the GROD value reached approximately 28° in the fractured areas of heat-treated specimens after the low cycle fatigue test.


2011 ◽  
Vol 291-294 ◽  
pp. 1106-1109 ◽  
Author(s):  
Grzegorz Golański ◽  
Krzysztof Werner ◽  
Stanisław Mroziński

The report treats of the low cycle fatigue (LCF) behaviour of GX12CrMoVNbN9-1 (GP91) cast steel after heat treatment (1040°C/12h/oil + 760°C/12h/air + 750°C/8h/furnace). Fatigue tests were carried out at room temperature for five levels of the controlled total strain amplitude εac = 0.25, 0.30, 0.35, 0.50 and 0.60 %. The research performed within the scope of LCF has shown in general that the investigated cast steel was subject to strong cyclic weakening, revealing no stabilization period at the same time. At the final stage of fatigue there was quick weakening of the material which proceeded till its destruction. The growth of amplitude εac resulted in reducing the number of cycles till the destruction stage.


Materials ◽  
2020 ◽  
Vol 13 (21) ◽  
pp. 4758
Author(s):  
Zhihao Yao ◽  
Biao Zhou ◽  
Kaijun Yao ◽  
Hongying Wang ◽  
Jianxin Dong ◽  
...  

In this work, the sensitivity zone of microstructure and temperature for precipitation-strengthened nickel-based superalloys, used for turbine applications in aero-engines, has been firstly established. Heat treatment experiments with different solution temperatures were carried out. The microstructure evolution and creep residual strain sensitivity, low cycle fatigue properties, and tensile properties are analyzed, and the essential reason for the fluctuation of the mechanical properties of nickel-based superalloys was revealed. The main results obtained are as follows: following subsolvus solution heat treatment with a temperature of 1020 °C, samples have a high primary γ′I phase content, which is beneficial to low creep residual strain. Above the supersolvus solution temperature of 1040 °C, the creep residual strain value and low cycle fatigue performance fluctuate significantly. The essential reason for the dramatic fluctuation of performance is the presence of γ′ phases in different sizes and quantities, especially following the solution heat treatment in the temperature-sensitive zone of the γ′I phase, which is likely to cause huge fluctuations in the microstructure of tertiary γ′III phases. A zone of particular sensitivity in terms of temperature and microstructure for the γ′I phase is proposed. The range of suitable solution temperatures are discussed. In order to maintain stable mechanical properties without large fluctuations, the influence of the sensitivity within this temperature and microstructure zone on the γ′ phase should be considered.


Author(s):  
Hiroshi Nakamura ◽  
Masahiro Takanashi ◽  
Yu Itabashi ◽  
Hiroshi Kuroki ◽  
Yusuke Ueda

This study investigates the shot peening effect on low cycle fatigue properties of two turbo engine materials, Ti-6Al-4V and Inconel 718, in view of the residual stress relaxation by the cyclic load and the thermal relaxation. Strain controlled fatigue tests for Ti-6Al-4V were carried out at room temperature. The fatigue tests for Inconel 718 were conducted at room temperature and 620C. An X-ray diffraction method was used to measure the residual stresses induced by shot peening. The compressive residual stress of Ti-6Al-4V specimen had retained about 60% after half the number of cycles to failure. It is confirmed that shot peening enhances strain range capability of Ti-6Al-4V at the life between 104 and 105 cycles region about 1.5 times higher than that of non-peened specimen. This result is attributed to the retained compressive layer even after applied cyclic loading. Shot peening enhanced the strain range capability of the Inconel 718 specimen at room temperature, by a factor of 1.3 compared to polished specimen at the life of 104 cycles region. The residual stress near the surface has been relaxed rapidly at turbine engine temperature, however, the residual stresses in the deep subsurface have been retained. The peened specimen tested at 620C tended to be slightly higher strain range than those of polished specimen at the life of 105 cycles.


2015 ◽  
Vol 226 ◽  
pp. 69-74
Author(s):  
Kazimierz J. Ducki ◽  
Marek Cieśla ◽  
Grzegorz Junak ◽  
Lilianna Wojtynek

The paper presents the results of investigations of the microstructure and fatigue behaviour of two newly invented Cr-Ni and Cr-Ni-Mn austenitic steels of 13/13 and 12/8/8 type strengthened through carbide particle precipitation. The specimens of the investigated steels were subjected to tests after heat treatment, i.e. solution heat treatment (1200°C/0.5 h/water) and aged at a temperature of 700°C for 12 h, with cooling in air. The heat treated specimens were then subjected to low-cycle fatigue tests (LCF), carried out at room temperature and at an increased temperature of 600°C. Diagrams of fatigue characteristics of the investigated steels at room temperature as well as at elevated temperature have been worked up. It has been found that during low-cycle fatigue tests, at both temperatures, the investigated austenitic steels indicated a fatigue softening effect. The results of LCF at room temperature showed that the fatigue durability (Nt) of both austenitic steels is located in the range 0.8÷1.3×103 cycles. The results of low-cycle fatigue tests at an increased temperature 600°C indicated that the fatigue durability of the investigated steel was lower, and is located in the range Nt = 0.5÷0.6×103 cycles. It has been pointed out that the investigated austenitic steels are characterized by a stability of structure in conditions of cyclic fatigue.


2010 ◽  
Vol 638-642 ◽  
pp. 455-460 ◽  
Author(s):  
A. Rutecka ◽  
L. Dietrich ◽  
Zbigniew L. Kowalewski

The AlSi8Cu3 and AlSi7MgCu0.5 cast aluminium alloys of different composition and heat treatment were investigated to verify their applicability as cylinder heads in the car engines [1]. Creep tests under the step-increased stresses at different temperatures, and low cycle fatigue (LCF) tests for a range of strain amplitudes and temperatures were carried out. The results exhibit a significant influence of the heat treatment on the mechanical properties of the AlSi8Cu3 and AlSi7MgCu0.5. An interesting fact is that the properties strongly depend on the type of quenching. Lower creep resistance (higher strain rates) and lower stress response during fatigue tests were observed for the air quenched materials in comparison to those in the water quenched. Cyclic hardening/softening were also observed during the LCF tests due to the heat treatment applied. The mechanical properties determined during the tests can be used to identify new constitutive equations and to verify existing numerical models.


Materials ◽  
2021 ◽  
Vol 14 (22) ◽  
pp. 6741
Author(s):  
Grzegorz Junak ◽  
Anżelina Marek ◽  
Michał Paduchowicz

This paper presents the results of tests conducted on the HR6W (23Cr-45Ni-6W-Nb-Ti-B) alloy under low-cycle fatigue at room temperature and at 650 °C. Fatigue tests were carried out at constant values of the total strain ranges. The alloy under low-cycle fatigue showed cyclic strengthening both at room temperature and at 650 °C. The degree of HR6W strengthening described by coefficient n’ was higher at higher temperatures. At the same time, its fatigue life Nf at room temperature was, depending on the range of total strain adopted in the tests, several times higher than observed at 650 °C.


2021 ◽  
Vol 1035 ◽  
pp. 292-296
Author(s):  
Zi Chao Peng ◽  
Jun Ying Sheng ◽  
Xu Qing Wang ◽  
Yue Tang

Low cycle fatigue (LCF) properties of a powder metallurgy(PM) nickel base superalloy FGH720Li were systematically studied in this work, including smooth LCF and notched LCF tested at various temperatures and different stress. The relationship between the fatigue life and applied stress was analyzed both for smooth fatigue and notch fatigue tests. The effects of loading frequency and stress ratio on LCF behavior were also studied. As an important influencing factor of the fatigue life in powder metallurgy superalloy, the effect of inclusions on LCF life was also investigated. The results showed that the fatigue properties of FGH720Li alloy was excellent, when tested at the temperature of 450°C and applied stress of 1230MPa, the fatigue life could exceed 5×104 cycles. When tested at 650°C and 1150MPa, the average fatigue life was still beyond 2×105 cycles.


Sign in / Sign up

Export Citation Format

Share Document