scholarly journals EFFECT OF ETCHING TECHNIQUES ON THE SHEAR BOND STRENGTH OF ADHESIVE PRECOATED BRACKETS BONDED IN VITRO

Author(s):  
Elsanuse Saied Abdelmegeed Bilgasem

This study was designed to compare shear bond strength durability of two etching techniques namely conventional etching and self-etching primer techniques, when using Adhesive pre-coated brackets (APCII). Thirty extracted premolars were divided into two equal groups (group 1: etched with 37% Phosphoric acid and group 2: bonded with transbond plus self-etching primer), each group was further subdivided into three subgroups each of them contains five teeth, at different storage times: 24 hours, 30 days and 3 months. Universal testing machine was used to measure shear bond strength. T-test revealed that there was no significant difference in shear bond strength between the two etching techniques at 24 hours and 30 days, while showed a highly significant difference (P ≤ 0.01) at 3 months. For the three storage times, self-etching primer showed less adhesive remnant on the teeth than that of Phosphoric acid etching. It can be concluded that self-etching primer provided shear bond strength Comparable to that of phosphoric acid, and it has less adhesive remnant than conventional etching technique.

2014 ◽  
Vol 39 (6) ◽  
pp. E250-E260 ◽  
Author(s):  
TA Imbery ◽  
T Gray ◽  
F DeLatour ◽  
C Boxx ◽  
AM Best ◽  
...  

SUMMARY Objective Repairing composite restorations may be a more conservative treatment than replacing the entire restoration. The objective of this in vitro study was to determine the best repair method by measuring flexural, diametral tensile, and shear bond strength of repaired composites in which the surfaces were treated with chemical primers (Add & Bond or Silane Bond Enhancer), a bonding agent (Optibond Solo Plus [OBSP]), or mechanical retention with a bonding agent. Methods Filtek Supreme Ultra shade B1B was placed in special molds to fabricate specimens that served to test the flexural, diametral tensile, or shear strength of the inherent resin substrate. The same molds were modified to make specimens for testing repair strength of the resin. Repairs were made immediately or after aging in deionized water at 37°C for seven days. All repair sites were finished with coarse Sof-Lex discs to simulate finishing new restorations or partially removing aged restorations. Repair surfaces were treated with one of the following: 1) phosphoric-acid etching and OBSP; 2) Add & Bond; 3) phosphoric-acid etching, Silane Bond Enhancer, and OBSP; or 4) quarter round bur, phosphoric-acid etching, and OBSP. Specimens were placed back in the original molds to fabricate specimens for diametral tensile or flexural testing or in an Ultradent jig to make specimens for shear bond testing. Composite resin in shade B5B was polymerized against the treated surfaces to make repairs. Two negative control groups for the three testing methods consisted of specimens in which repairs were made immediately or after aging without any surface treatments. Controls and experimental repairs were aged (water 37°C, 24 hours) before flexural, diametral tensile, or shear testing in an Instron Universal testing machine at a crosshead speed of 0.5 mm/min. Results Experimental flexural repair strengths ranged from 26.4% to 88.6% of the inherent substrate strength. Diametral tensile repair strengths ranged from 40% to 80% of the inherent substrate strength, and shear bond strength repairs ranged from 56% to 102%. Geometric means were statistically analyzed with two-way analysis of variance on their log-transformed values. Significant differences were determined using Tukey honestly significant difference (p<0.05). Conclusions Depending on the mechanical property being tested, surface treatments produced different results. OBSP produced more consistent results than chemical primers.


2018 ◽  
Vol 7 (2) ◽  
pp. 28-31
Author(s):  
Varunjeet Chaudhary ◽  
Sanad Singh Solanki ◽  
Varsha Yadav ◽  
Seema Lahoti

Objective: To evaluate the shear bond strength of stainless steel brackets bonded with fluoride-releasing composite resins, comparing effect of adhesion booster and conventional primer.Materials & Method: Sixty extracted premolars were subjected to bracket bonding with fluoride-releasing composite resin; which were bonded by randomly divided into two groups of bonding agents: Group 1- conventional primer as control group, Group 2- adhesion booster. After bonding, the samples were thermocycled (500 cycles) at 5ºC and 55ºC temperatures. After 48 hours they were subjected to shear bond strength testing in occluso-gingival direction, using an MTS 810 Universal Testing Machine with load speed of 0.5 mm/min.Result: Mean shear bond strength was significantly more in samples bonded with adhesion booster (14.792±3.805 Mpa) as compared to conventional primers (11.327±4.047 Mpa). There was statistically significant difference in shear bond strength between the groups (p=0.001).Conclusion: The use of the adhesion booster significantly increased the bond strength of bracket bonded with fluoride-releasing composite.


2007 ◽  
Vol 77 (4) ◽  
pp. 701-706 ◽  
Author(s):  
Rodney G. Northrup ◽  
David W. Berzins ◽  
Thomas Gerard Bradley ◽  
William Schuckit

Abstract Objective: To evaluate and compare the shear bond strengths of two adhesives using two types of brackets: a conventional and a self-ligating bracket system. Materials and Methods: Sixty extracted human premolars were collected. The premolars were randomly divided into three groups of 20 teeth. All three groups were direct bonded. Groups 1 and 2 used light-cured adhesive and primer (Transbond XT) with a conventional (Orthos) and a self-ligating bracket (Damon 2), respectively. Group 3 used a light-cured primer (Orthosolo) and a light-cured adhesive (Blūgloo) with a self-ligating bracket (Damon 2). The specimens were stored in distilled water at 37°C for 40 ± 2 hours, after which they were debonded and inspected for Adhesive Remnant Index (ARI) scoring. Results: The mean shear bond strength was 15.2 MPa for group 1, 23.2 MPa for group 2, and 24.8 MPa for group 3. A one-way analysis of variance and post hoc Tukey test showed significant differences in bond strength (P < .001) between group 1 and groups 2 and 3 but no significant difference (P > .05) between groups 2 and 3. A Weibull analysis demonstrated that all three groups provided sufficient bond strength with over 90% survival rate at normal masticatory and orthodontic force levels. A Kruskal-Wallis test showed no significant difference (P > .05) in ARI scores among all three groups. Conclusions: All three groups demonstrated clinically acceptable bond strength. The Damon 2 self-ligating bracket exhibited satisfactory in vitro bond strength with both adhesive systems used.


2021 ◽  
Vol 58 (1) ◽  
pp. eUJ3657
Author(s):  
Germano Brandão ◽  
◽  
Liliana Ávila Maltagliati ◽  
Ana Carla Raphaelli Nahás-Scocate ◽  
Murilo Matias ◽  
...  

The objective of this in vitro study was to assess and compare the shear bond strength of conventional and modified orthodontic tubes bonded to the surface of dry and saliva-contaminated enamel. The sample consisted of 40 human teeth, which were randomly divided into four groups according to attachment base and presence or absence of saliva contamination as follows: Group CB, conventional orthodontic tubes without salivary contamination; Group CB-S, conventional orthodontic tubes with salivary contamination; Groups BM, orthodontic tubes modified by welding a metal mesh to their base without salivary contamination; and Group BM-S, modified orthodontic tubes with salivary contamination. Shear bond strength test was performed in a universal testing machine and analysis of the adhesive remnant index (ARI) by optical microscopy. Two-way ANOVA was used, followed by Tukey’s test at a statistical significance level of 5%. The ARI results were analysed descriptively. There was statistically significant difference between the groups regarding the shear bond strength values, with conventional tubes presenting significantly higher values (P < 0.05). In addition, the presence of salivary contamination interfered negatively with the behaviour of conventional tubes only (P < 0.05). Shear bond strength was not improved by increasing the area of the orthodontic tubes. Moreover, salivary contamination influenced negatively the SBS values, but only when conventional tubes were used.


BDJ Open ◽  
2020 ◽  
Vol 6 (1) ◽  
Author(s):  
Yasser R. Souror ◽  
Tayseer Maaly ◽  
Mohammed Sameer Khawandanah

Abstract To evaluate a fixed-space maintainer made of light-cure acrylic resin (LCAR) for its flexural and shear bond strength using different bonding systems to the enamel. 45 extracted primary teeth were selected. They were randomly divided into three equal groups (n = 15) along with the type of adhesive system (Tetric Flow, Transbond XT, and Fuji Ortho LC) used for bonding (LCAR) to the tooth surface. Surfaces were treated; LCAR was attached to the treated surfaces using a split Teflon mold. For flexural strength testing, ten bars of LCAR were made using another Teflon-split mold. Shear bond strength and mean flexural strength values were evaluated by a universal testing machine. The highest values of bond strength were recorded for Transbond XT, followed by Tetric Flow, while the lowest values were for Fuji Ortho LC. Various groups had a significant difference as investigated by ANOVA. ARI scores showed no significant difference in debond sites. Mean value and standard deviation of flexural strength for LCAR were 82.83  ± 5.2. LCAR has superior mechanical properties and could be an alternative to currently-in-use space maintainer though in vivo and in vitro trials are needed to progress the ultimate design of LCAR.


2014 ◽  
Vol 1025-1026 ◽  
pp. 385-390
Author(s):  
Niwat Anuwongnukroh ◽  
Surachai Dechkunakorn ◽  
Jirawat Arunakol ◽  
Wassana Wichai

One of the problems that often occurred during orthodontic treatment is bracket failure. This is usually the result either of the patient’s accidentally, applying inappropriate forces to the bracket or of a poor bonding technique. Thus, a significant number of teeth have to be rebonded in an orthodontic practice. Objective: The aim of this study was to evaluate the in vitro initial repeated shear bond strength of the three adhesive systems at two and five minutes after placement of a bracket. Materials and Methods: The three bonding agent adhesives are System1+, Rely-a-bond, Unite. Two hundred and forty human premolar teeth were divided into two groups, a control and an experimental group. Each group was further divided into three subgroups for bonding brackets with the three different adhesives. Only the teeth in the experimental group were sequentially bonded and debonded two times with the same adhesive. The teeth in control and experimental groups were tested for shear bond strength (at two and five minutes after the bracket was bonded) with an Instron testing machine. Results: The studies were found that : (1) there were differences between the shear bond strength of each adhesive in the control and experimental group. Unite had the highest shear bond strength followed by Rely-a-bond and System1+ at two minutes and five minutes, (2) the experiment group ( rebonded brackets) had higher shear bond strength than control group and Unite had in significant difference (p<0.05) of initial repeated bond strength with System1+ and Rely-a-bond at two minutes and five minutes and (3) there were mostly significant difference (p<0.05) between repeated shear bond strength at two minutes and repeated shear bond strength at five minutes. Conclusion: There were significant difference of the initial repeated shear bond strength of each adhesive. The orthodontists should be aware of applying force for tooth movement into the repeated bonding brackets.


2015 ◽  
Vol 2015 ◽  
pp. 1-7 ◽  
Author(s):  
Gisele Lima Bezerra ◽  
Carlos Rocha Gomes Torres ◽  
Mateus Rodrigues Tonetto ◽  
Alvaro Henrique Borges ◽  
Milton Carlos Kuga ◽  
...  

The objective of this study is to assess,in vitro, the shear bond strength of orthodontic brackets fixed with remineralizing adhesive systems submitted to thermomechanical cycling, simulating one year of orthodontic treatment. Sixty-four bovine incisor teeth were randomly divided into 4 experimental groups (n=16):XT: Transbond XT,QC: Quick Cure,OL: Ortholite Color, andSEP: Transbond Plus Self-Etching Primer. The samples were submitted to thermomechanical cycling simulating one year of orthodontic treatment. Shear bond strength tests were carried out using a universal testing machine with a load cell of 50 KgF at 0.5 mm/minute. The samples were examined with a stereomicroscope and a scanning electron microscope (SEM) in order to analyze enamel surface and Adhesive Remnant Index (ARI). Kruskal-Wallis and Mann-Whitney (with Bonferroni correction) tests showed a significant difference between the studied groups (p<0.05). Groups XT, QC, and SEP presented the highest values of adhesive resistance and no statistical differences were found between them. The highest frequency of failures between enamel and adhesive was observed in groups XT, QC, and OL. Quick Cure (QC) remineralizing adhesive system presented average adhesive resistance values similar to conventional (XT) and self-etching (SEP) adhesives, while remineralizing system (OL) provided the lowest values of adhesive resistance.


Author(s):  
Shubhangi Mani ◽  
Darshan Deepak Shah ◽  
Narendra Manwar ◽  
Rushabh Malde

ABSTRACT Aim To compare the shear bond strength of Tetric N Bond (Ivoclar Vivadent) and Single Bond Universal Adhesive (3M ESPE, MN, USA) on ground enamel and dentin. Materials and methods A total of 30 extracted human maxillary and mandibular molars and premolars were used for this study and divided into two groups which were treated with Tetric N Bond (Ivoclar Vivaden) t- and Single Bond Universal Adhesive (3M ESPE, MN, USA). The shear bond strength was tested on Universal testing machine (Instron). Results There was statistically significant difference in the shear bond strength among the two groups. Conclusion Based on the results (Tetric N Bond, Ivoclar Vivadent) had higher bond strength than Single Bond Universal Adhesive (3M ESPE, MN, USA) on ground enamel and dentin. How to cite this article Shah DD, Chandak M, Manwar N, Mani S, Mani A, Saini R, Malde R. Comparing Shear Bond Strength of Two Step vs One Step Bonding Agents on Ground Enamel and Dentin: An in vitro Study. Int J Experiment Dent Sci 2014;3(1):1-3.


2012 ◽  
Vol 10 (2) ◽  
pp. 98-104
Author(s):  
P Mazumdar ◽  
U Kumar Das ◽  
R Kundu

Introduction: Composite resins have become one of the most commonly used direct restorative materials for anterior and posterior teeth.Objectives: To observe and analyze the gap at the resin dentin interface in class II cavities restored with light cure composite resin in four experimental groups employing 37% phosphoric acid or self etching monomers and restored with /without light cure flowable composite resin.Methods: 40 sound maxillary first premolars, extracted due to orthodontic reasons was taken, distoproximal cavities were prepared and divided into 4 groups. Teeth of Group 1 was etched by 37% Phosphoric acid and light cure flowable composite resin was used, in group 2 ,two coats of self etching acidic monomer were applied and light cure flowable composite resin was used. Teeth of group 3 was etched with 37% phosphoric acid and restored without light cure flowable composite resin and in group 4, two coats of self etching acidic monomer were applied and restored without using light cure flowable composite resin material. Thermocycling was done after finishing and polishing and viewed under scanning electron microscope to observe and analyze the gap between tooth and the restoration.Result: Gap was observed at dentin-composite resin interface in all 4 groups. Results were evaluated by F-test and Manwhitney U test. No statistically significant difference was found.Conclusion: Use of flowable composite resin liner and the etching technique do not have any influence on the gap.DOI: http://dx.doi.org/10.3126/hren.v10i2.6571 Health Renaissance 2012; Vol 10 (No.2); 98-104


Author(s):  
Mohammad Moslem Imani ◽  
Farzaneh Aghajani ◽  
Nafiseh Momeni ◽  
Mohammad Sadegh Ahmad Akhoundi

Objectives: In clinical conditions, orthodontic brackets are exposed to periodic stresses mainly induced by mastication and intraoral forces. The objective of the present study was to evaluate the effects of cyclic loading to simulate masticatory forces on shear bond strength (SBS) of metal brackets bonded to teeth using self-etch and total-etch bonding systems. Materials and Methods: Eighty-four caries- and crack-free bovine mandibular incisors were selected and randomly assigned to two groups based on the type of bonding system. After bonding, all samples were thermocycled (500 cycles) followed by cyclic loading of the half of the specimens in each group by applying 40 N load with 2 Hz frequency for 10,000 cycles. The SBS was measured using a universal testing machine. The adhesive remnant index (ARI) score was calculated subsequently. Data were analyzed using Kolmogorov-Smirnov test, two-way ANOVA and Mann-Whitney test. Results: The SBS was 10.09±3.78 MPa and 14.44±6.06 MPa for self-etch and total-etch bonding systems in cyclic loading group, respectively. The SBS was 9.43±5.3 MPa and 11.31±5.42 MPa in self-etch and total-etch groups without cyclic loading, respectively. Cyclic loading did not cause any significant difference in SBS (P>0.05). The ARI scores of the groups were significantly different (P<0.05). Conclusions: The present results demonstrated that low masticatory forces at 10,000 cycles did not have a significant impact on bracket-adhesive SBS; however, they significantly changed the ARI score. Even though the total-etch bonding system yielded higher SBS than the self-etch system, the performance of both was clinically acceptable.


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