scholarly journals Hierarchical creep cavity formation in an ultramylonite and implications for phase mixing

Solid Earth ◽  
2017 ◽  
Vol 8 (6) ◽  
pp. 1193-1209 ◽  
Author(s):  
James Gilgannon ◽  
Florian Fusseis ◽  
Luca Menegon ◽  
Klaus Regenauer-Lieb ◽  
Jim Buckman
Keyword(s):  
Grain Size ◽  
Grain Boundary ◽  
Grain Boundaries ◽  
Finite Strain ◽  
Grain Boundary Sliding ◽  
Large Strains ◽  
Cavity Formation ◽  
Phase Mixing ◽  
Transient Phenomena ◽  
Boundary Sliding

Abstract. Establishing models for the formation of well-mixed polyphase domains in ultramylonites is difficult because the effects of large strains and thermo-hydro-chemo-mechanical feedbacks can obscure the transient phenomena that may be responsible for domain production. We use scanning electron microscopy and nanotomography to offer critical insights into how the microstructure of a highly deformed quartzo-feldspathic ultramylonite evolved. The dispersal of monomineralic quartz domains in the ultramylonite is interpreted to be the result of the emergence of synkinematic pores, called creep cavities. The cavities can be considered the product of two distinct mechanisms that formed hierarchically: Zener–Stroh cracking and viscous grain-boundary sliding. In initially thick and coherent quartz ribbons deforming by grain-size-insensitive creep, cavities were generated by the Zener–Stroh mechanism on grain boundaries aligned with the YZ plane of finite strain. The opening of creep cavities promoted the ingress of fluids to sites of low stress. The local addition of a fluid lowered the adhesion and cohesion of grain boundaries and promoted viscous grain-boundary sliding. With the increased contribution of viscous grain-boundary sliding, a second population of cavities formed to accommodate strain incompatibilities. Ultimately, the emergence of creep cavities is interpreted to be responsible for the transition of quartz domains from a grain-size-insensitive to a grain-size-sensitive rheology.

scholarly journals Hierarchical creep cavity formation in an ultramylonite and implications for phase mixing

2017 ◽  
Author(s):  
James Gilgannon ◽  
Florian Fusseis ◽  
Luca Menegon ◽  
Klaus Regenauer-Lieb ◽  
Jim Buckman
Keyword(s):  
Grain Size ◽  
Grain Boundary ◽  
Grain Boundaries ◽  
Finite Strain ◽  
Grain Boundary Sliding ◽  
Cavity Formation ◽  
Phase Mixing ◽  
Creep Cavity ◽  
Boundary Sliding

Abstract. The dispersal of monomineralic quartz domains in a quartzofeldspathic ultramylonite is interpreted to be the result of the emergence of syn-kinematic pores, called creep cavities. The cavities can be considered the product of two distinct mechanisms that formed hierarchically: Zener-Stroh cracking and viscous grain boundary sliding. In initially thick and coherent quartz ribbons deforming by grain size-insensitive creep, cavities were generated by the Zener-Stroh mechanism on grain-boundaries aligned with the YZ plane of finite strain. The opening of creep cavities promoted the ingress of fluids to sites of low stress. The local addition of a fluid lowered the adhesion and cohesion of grain-boundaries and promoted viscous grain boundary sliding. With the increased contribution of viscous grain boundary sliding, a second population of cavities formed to accommodate strain incompatibilities. Ultimately, the emergence of creep cavities is interpreted to be responsible for the transition of quartz domains from a grain size-insensitive, to a grain size-sensitive rheology.

Ductile strain partitioning in micritic limestones, Calabria, Italy: the roles and mechanisms of intracrystalline and intercrystalline deformation

2007 ◽  
Vol 44 (11) ◽  
pp. 1587-1602 ◽  
Author(s):  
S Vitale ◽  
J C White ◽  
A Iannace ◽  
S Mazzoli
Keyword(s):  
Electron Microscopy ◽  
Grain Size ◽  
Grain Boundary ◽  
Finite Strain ◽  
Grain Boundary Sliding ◽  
Strain Partitioning ◽  
Grain Sizes ◽  
Reference Sections ◽  
Boundary Sliding ◽  
Mechanical Twins

The Apennine Pollino–Ciagola limestone unit in northern Calabria is characterized by subgreenschist, heterogeneous ductile strain localized along narrow deformation zones at several stratigraphic levels. Paleogene conglomerates and Jurassic calcareous breccias and ooidal packstones have been analyzed with the aim of characterizing the deformation of limestone as a function of the strain recorded by sedimentary markers. Reference sections parallel to principal finite strain planes were prepared at each locality for the study of specific parameters. Image analysis of polished sections by scanning electron microscopy (SEM) was used to obtain the finite strain of calcite grains by Rf/ϕ, harmonic mean and normalized Fry methods. For the range of grain sizes analyzed (1–10 µm), the ellipticity of calcite grains varies as a function of grain size according to a power-law relationship, from which the size of isometric grains is empirically predicted. The finite strain (ellipticity) determined from single calcite grains shows consistently lower values than the corresponding rock strain. For a fixed grain size, grain ellipticity initially increases with rock strain; however for larger strain, scattered ellipticity values are recorded, probably because of dynamic recrystallization. Comparison of bulk strain with grain strain suggests that intercrystalline deformation involving grain boundary sliding contributes 50%–80% of the total strain, for grain sizes in the range of 2–10 µm, increasing to 90% or more for smaller grain sizes. Microstructures (optical, SEM, transmission electron microscopy) are consistent with dominant grain boundary sliding accommodated by dislocation processes. The weakly deformed samples (Rs <4) exhibit straight and subsidiary curved mechanical twins in large grains (d >10 µm), with well-developed glide dislocation substructures in both coarse and micrite grains. In the moderately to highly deformed samples (Rs >4), large grains show curved, thick, and patchy twins, with the development of undulose extinction and subgrains. Subwalls are formed from dislocation networks and relate to subgrain rotation recrystallization in the coarsest grains. Both large and small grains exhibit complex dislocation substructures comprising dislocation networks indicative of concurrent intercrystalline and intracrystalline deformation, whereby grain boundary sliding is accommodated by dislocation processes. Integration of tectonic constraints, field observations, finite strain data, microstructures, and experimental data is consistent with natural deformation at 250 °C, 15–50 MPa, and bulk shear strain rates on the order of 10–13 s–1 to 10–12 s–1.

scholarly journals The role of grain size evolution in the rheology of ice: implications for reconciling laboratory creep data and the Glen flow law

2021 ◽  
Vol 15 (9) ◽  
pp. 4589-4605
Author(s):  
Mark D. Behn ◽  
David L. Goldsby ◽  
Greg Hirth
Keyword(s):  
Grain Size ◽  
Grain Boundary ◽  
Stress Exponent ◽  
Ice Sheets ◽  
Grain Boundary Sliding ◽  
Dislocation Creep ◽  
Ice Flow ◽  
Size Evolution ◽  
Boundary Sliding ◽  
Flow Law

Abstract. Viscous flow in ice is often described by the Glen flow law – a non-Newtonian, power-law relationship between stress and strain rate with a stress exponent n ∼ 3. The Glen law is attributed to grain-size-insensitive dislocation creep; however, laboratory and field studies demonstrate that deformation in ice can be strongly dependent on grain size. This has led to the hypothesis that at sufficiently low stresses, ice flow is controlled by grain boundary sliding, which explicitly incorporates the grain size dependence of ice rheology. Experimental studies find that neither dislocation creep (n ∼ 4) nor grain boundary sliding (n ∼ 1.8) have stress exponents that match the value of n ∼ 3 in the Glen law. Thus, although the Glen law provides an approximate description of ice flow in glaciers and ice sheets, its functional form is not explained by a single deformation mechanism. Here we seek to understand the origin of the n ∼ 3 dependence of the Glen law by using the “wattmeter” to model grain size evolution in ice. The wattmeter posits that grain size is controlled by a balance between the mechanical work required for grain growth and dynamic grain size reduction. Using the wattmeter, we calculate grain size evolution in two end-member cases: (1) a 1-D shear zone and (2) as a function of depth within an ice sheet. Calculated grain sizes match both laboratory data and ice core observations for the interior of ice sheets. Finally, we show that variations in grain size with deformation conditions result in an effective stress exponent intermediate between grain boundary sliding and dislocation creep, which is consistent with a value of n = 3 ± 0.5 over the range of strain rates found in most natural systems.

Research on Micro-Mechanism of Nanocomposite Ceramic in Two-Dimensional Ultrasound Grinding

2007 ◽  
Vol 359-360 ◽  
pp. 344-348 ◽  
Author(s):  
Bo Zhao ◽  
Yan Wu ◽  
Guo Fu Gao ◽  
Feng Jiao
Keyword(s):  
Grain Boundary ◽  
Grain Boundaries ◽  
Deformation Mechanism ◽  
Ground Surface ◽  
Grain Boundary Sliding ◽  
Second Phase ◽  
Two Dimensional ◽  
Composite Ceramics ◽  
Nano Composite ◽  
Boundary Sliding

Surface microstructure of nano-composite ceramics prepared by mixed coherence system and machined by two-dimensional ultrasonic precision grinding was researched using TEM, SEM, XRD detector and other equipments. Structure, formation mechanism and characteristic of metamorphic layer of ground surface of nano-composite ceramics were researched. The experiment shows micro deformation mechanism of ceramic material in two-dimensional ultrasound grinding is twin grain boundary and grain-boundary sliding for Al2O3, and it is crystal dislocation of enhanced phase, matrix grain boundary sliding, coordination deformation of intergranular second phase as well as its deformation mechanism for nano-composite ceramics. The fracture surfaces of nano-composite materials with different microscopic structure were observed using TEM and SEM. Research shows that ZrO2 plays an important influence on the generation and expansion of crack, and enhances the strength of grain boundaries. When grain boundaries is rich in the ZrO2 particles, the crack produced in grinding process will be prevented, and the surface with plastic deformation will be smooth. The results shows nanoparticles dispersed in grain boundary prevents crack propagation and makes materials fracture transgranularly which makes the processed surface fine.

Mechanical Properties of Novel Nanocrystalline Materials

2001 ◽  
Author(s):  
J. Narayan ◽  
H. Wang ◽  
A. Kvit
Keyword(s):  
Grain Size ◽  
Grain Boundary ◽  
Nanocrystalline Materials ◽  
High Surface ◽  
Grain Boundary Sliding ◽  
Boundary Shear ◽  
Functionally Gradient ◽  
Boundary Sliding ◽  
First Time ◽  
Critical Grain Size

Abstract We have synthesized nanocrystalline thin films of Cu, Zn, TiN, and WC having uniform grain size in the range of 5 to 100 nm. This was accomplished by introducing a couple of manolayers of materials with high surface and have a weak interaction with the substrate. The hardness measurements of these well-characterized specimens with controlled microstructures show that hardness initially increases with decreasing grain size following the well-known Hall-Petch relationship (H∝d−½). However, there is a critical grain size below which the hardness decreases with decreasing grain size. The experimental evidence for this softening of nanocrystalline materials at very small grain sizes (referred as reverse Hall-Petch effect) is presented for the first time. Most of the plastic deformation in our model is envisioned to be due to a large number of small “sliding events” associated with grain boundary shear or grain boundary sliding. This grain-size dependence of hardness can be used to create functionally gradient materials for improved adhesion and wear among other improved properties.

scholarly journals Grain Boundary Sliding and Atomic Structures in Alumina Bicrystals with [0001] Symmetric Tilt Grain Boundaries

2002 ◽  
Vol 43 (7) ◽  
pp. 1561-1565 ◽  
Author(s):  
Tsuyoshi Watanabe ◽  
Hidehiro Yoshida ◽  
Yuichi Ikuhara ◽  
Taketo Sakuma ◽  
Hiroyuki Muto ◽  
...  
Keyword(s):  
Grain Boundary ◽  
Grain Boundaries ◽  
Grain Boundary Sliding ◽  
Atomic Structures ◽  
Symmetric Tilt ◽  
Boundary Sliding

Strain localisation during diffusion creep: influence of grain coarsening and grain boundary sliding

2020 ◽  
Author(s):  
John Wheeler ◽  
Lynn Evans ◽  
Robyn Gardner ◽  
Sandra Piazolo
Keyword(s):  
Grain Size ◽  
Grain Boundary ◽  
Earth Pressure ◽  
Grain Boundary Sliding ◽  
Mechanical Anisotropy ◽  
Limited Attention ◽  
Diffusion Creep ◽  
Pressure Solution ◽  
Grain Coarsening ◽  
Boundary Sliding

&lt;p&gt;Diffusion creep and the wet low temperature version, pressure solution, are major deformation mechanisms in the Earth. Pressure solution operates in many metamorphosing systems in the crust and may contribute to slow creep on fault surfaces. Diffusion creep prevails in areas of the upper mantle deforming slowly, and possibly in most of the lower mantle. Both mechanisms contribute to localisation since small grain sizes can deform faster.&lt;/p&gt;&lt;p&gt;However, there has been limited attention paid to the evolution of microstructure during diffusion creep. In some experiments grains coarsen; in some but not all experiments grains remain rather equant. We have developed a grain-scale numerical model for diffusion creep, which indicates that those processes are very important in influencing evolving strength. Our models illustrate three behaviours.&lt;/p&gt;&lt;ol&gt;&lt;li&gt;Strain localises along slip surfaces formed by aligned grain boundaries on all scales. This affects overall strength.&lt;/li&gt; &lt;li&gt;Diffusion creep is predicted to produce elongate grains and then the overall aggregate has intense mechanical anisotropy. Thus strength during diffusion creep, and localisation on weak zones, is influenced not just by grain size but by other aspects of microstructure.&lt;/li&gt; &lt;li&gt;Grain coarsening increases grain size and strength. Our most recent work shows how it interacts with ongoing deformation. In particular grain growth can lead to particular grain shapes which are directly related to strain rate, and influence strength. Consequently, understanding localisation during diffusion creep must encompass the effects of diffusion itself, grain boundary sliding and grain coarsening.&lt;/li&gt; &lt;/ol&gt;

Characterization of Zinalco Alloy Superplastically Deformed Using Orientation Imaging Microscopy

2009 ◽  
Vol 1242 ◽  
Author(s):  
Ramos A. Mitsuo ◽  
Martínez F. Elizabeth ◽  
Negrete S. Jesús ◽  
Torres-Villaseñor G.
Keyword(s):  
Grain Size ◽  
Grain Boundary ◽  
Grain Boundaries ◽  
Superplastic Deformation ◽  
Orientation Imaging Microscopy ◽  
Grain Boundary Sliding ◽  
Boundary Misorientation ◽  
Average Grain Size ◽  
Grain Boundary Misorientation ◽  
Misorientation Angles

ABSTRACTZinalco alloy (Zn-21mass%Al-2mass%Cu) specimens were deformed superplastically with a strain rate (ε) of 1×10-3 s-1 at homologous temperature (TH) of 0.68 (5 ). It was observed neck formation that indicate nonhomegeneus deformation. Grain size and grain boundaries misorientation changes, due superplastic deformation, were characterized by Orientation Imagining Microscopy (OIM) technique. It was studied three regions in deformed specimens and the results were compared with the results for a specimen without deformation. Average grain size of 1 mm was observed in non-deformed specimen and a fraction of 82% for grain boundary misorientation angles with a grain boundaries angles between 15° and 55° was found. For deformed specimen, the fraction of angles between 15° and 55° was decreced to average value of 75% and fractions of low angle (<5°) and high angle (>55°) misorientations were 10% and 15% respectively. The grain size and high fraction of grain boundary misorientation angles between 15° and 55° observed in the alloy without deformation, are favorable for grain rotation and grain boundary sliding (GBS) procces. The changes observed in the fraction of favorable grain boundary angles during superplastic deformation, shown that the superplastic capacity of Zinalco was reduced with the deformation.

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