Under environmentally friendly and environmental issues, wastewater treatment in laboratories and factories is an important international issue. Among them, wastewater from the chemical industry accounts for a large part of industrial wastewater discharge. The introduction of new technologies to treat chemical wastewater is of great significance. In particular, the amount of wastewater produced by inorganic chemistry experiments is relatively large, and the pollutants are mostly heavy metal salts. According to the characteristics of inorganic chemistry experimental wastewater, such as special nature, small amount, strong discontinuity, high hazard, complex and changeable composition, etc., design a chemical reaction to provide a practical and feasible method to treat wastewater with high efficiency and low cost. This research initially takes Ni+ metal ion waste liquid as the first stage of recycling and treatment to improve the traditional low-concentration non-economic treatment. The preliminary results of this research are neutralization reaction and optimal pH value control of Ni+ waste liquid to generate Ni+ precursors to increase the economic value of recycling will be the basis for providing in-house recycling systems for electroplating plants, panel plants, and semiconductor plants to achieve emission reduction, green chemical industry and green environmental protection.