scholarly journals Pore-by-pore capillary pressure measurements using X-ray microtomography at reservoir conditions: Curvature, snap-off, and remobilization of residual CO2

2014 ◽  
Vol 50 (11) ◽  
pp. 8760-8774 ◽  
Author(s):  
Matthew Andrew ◽  
Branko Bijeljic ◽  
Martin J. Blunt
2019 ◽  
Vol 89 ◽  
pp. 04005 ◽  
Author(s):  
A Giwelli ◽  
MZ Kashim ◽  
MB Clennell ◽  
L Esteban ◽  
R Noble ◽  
...  

We conducted relatively long duration core-flooding tests on three representative core samples under reservoir conditions to quantify the potential impact of flow rates on fines production/permeability change. Supercritical CO2 was injected cyclically with incremental increases in flow rate (2─14 ml/min) with live brine until a total of 7 cycles were completed. To avoid unwanted fluid-rock reaction when live brine was injected into the sample, and to mimic the in-situ geochemical conditions of the reservoir, a packed column was installed on the inflow accumulator line to pre-equilibrate the fluid before entering the core sample. The change in the gas porosity and permeability of the tested plug samples due to different mechanisms (dissolution and/or precipitation) that may occur during scCO2/live brine injection was investigated. Nuclear magnetic resonance (NMR) T2 determination, X-ray CT scans and chemical analyses of the produced brine were also conducted. Results of pre- and post-test analyses (poroperm, NMR, X-ray CT) showed no clear evidence of formation damage even after long testing cycles and only minor or no dissolution (after large injected pore volumes (PVs) ~ 200). The critical flow rates (if there is one) were higher than the maximum rates applied. Chemical analyses of the core effluent showed that the rock samples for which a pre-column was installed do not experience carbonate dissolution.


2021 ◽  
Author(s):  
Bashar Alramahi ◽  
Qaed Jaafar ◽  
Hisham Al-Qassab

Abstract Classifying rock facies and estimating permeability is particularly challenging in Microporous dominated carbonate rocks. Reservoir rock types with a very small porosity range could have up to two orders of magnitude permeability difference resulting in high uncertainty in facies and permeability assignment in static and dynamic models. While seismic and conventional porosity logs can guide the mapping of large scale features to define resource density, estimating permeability requires the integration of advanced logs, core measurements, production data and a general understanding of the geologic depositional setting. Core based primary drainage capillary pressure measurements, including porous plate and mercury injection, offer a valuable insight into the relation between rock quality (i.e., permeability, pore throat size) and water saturation at various capillary pressure levels. Capillary pressure data was incorporated into a petrophysical workflow that compares current (Archie) water saturation at a particular height above free water level (i.e., capillary pressure) to the expected water saturation from core based capillary pressure measurements of various rock facies. This was then used to assign rock facies, and ultimately, estimate permeability along the entire wellbore, differentiating low quality microporous rocks from high quality grainstones with similar porosity values. The workflow first requires normalizing log based water saturations relative to structural position and proximity to the free water level to ensure that the only variable impacting current day water saturation is reservoir quality. This paper presents a case study where this workflow was used to detect the presence of grainstone facies in a giant Middle Eastern Carbonate Field. Log based algorithms were used to compare Archie water saturation with primary drainage core based saturation height functions of different rock facies to detect the presence of grainstones and estimate their permeability. Grainstones were then mapped spatially over the field and overlaid with field wide oil production and water injection data to confirm a positive correlation between predicted reservoir quality and productivity/injectivity of the reservoir facies. Core based permeability measurements were also used to confirm predicted permeability trends along wellbores where core was acquired. This workflow presents a novel approach in integrating core, log and dynamic production data to map high quality reservoir facies guiding future field development strategy, workover decisions, and selection of future well locations.


2002 ◽  
Vol 57 (8) ◽  
pp. 868-876 ◽  
Author(s):  
H. Oppermann ◽  
M. Zhang-Preße ◽  
P. Schmidt

The pure ternary phases on the line Yb2O3-SeO2 in thermodynamical equilibrium have been synthesized by solid state reaction and characterized using X-ray powder diffraction and IR-spectroscopy. There exist three phases: Yb2SeO5, Yb2Se3O9 and Yb2Se4O11, the last one with a homogeneiety range extending a higher SeO2-content. The thermal decompositions have been determined by total pressure measurements, and the thermodynamical data of the compounds have been derived. The phase diagram and the phase barogram have been established using the results of thermal analysis and total pressure measurements.


2020 ◽  
Vol 22 (34) ◽  
pp. 19282-19298
Author(s):  
Kayane K. Dingilian ◽  
Roope Halonen ◽  
Valtteri Tikkanen ◽  
Bernhard Reischl ◽  
Hanna Vehkamäki ◽  
...  

Small angle X-ray scattering and pressure measurements yield quantitative homogeneous nucleation rates for CO2 near 80 K.


Sign in / Sign up

Export Citation Format

Share Document