X-Ray Probe with Collimation of the Secondary Beam

1962 ◽  
pp. 516-526 ◽  
Author(s):  
Kurt F. J. Heinrich
Keyword(s):  
2003 ◽  
Vol 36 (6) ◽  
pp. 1324-1333 ◽  
Author(s):  
Gunnar Thorkildsen ◽  
Helge B. Larsen ◽  
Edgar Weckert ◽  
Dag Semmingsen

An original functional description of the intensity perturbation of the two-beam diffracted power caused by an interfering three-beam interaction has been developed. By using this approach in the analysis of measured three-beam profiles of α-oxalic acid dihydrate, parameters related to the Darwin mosaic model are refined. The final results indicate an anisotropy in both the mean domain size, measured along the secondary beam, and the block orientation, measured as the angular spread in the location of the three-beam point. The presented method relies on a procedure for merging the contributions to the perturbation originating from dynamical (coherent) and kinematical (incoherent) scattering processes.


1998 ◽  
Vol 30 (3-4) ◽  
pp. 133-143 ◽  
Author(s):  
K. Van Acker ◽  
P. Van Houtte

An X-ray texture goniometer equipped with a vertical Soller slit and a monochromator in the secondary beam in combination with Cu radiation is found to be useful for pole figure measurements on different materials, e.g. Al and Fe, as well as for low incident beam angle measurements on thin coatings. The obtained ODF's are less sensitive to errors in the procedure used for background correction of the pole figures than obtained with the classical setup used for pole figure measurements. The reason for that is the drastically ameliorated Intensity/Background (I/B) ratio by the use of the monochromator. Examples for cold rolled Fe and Al are presented. One of the merits of the new setup is that pole figures of Al, Cu, Ti, Fe can all be measured by using Cu Kα radiation, thus avoiding frequent and time-consuming exchanges of X-ray tubes.


1961 ◽  
Vol 5 ◽  
pp. 447-456
Author(s):  
Eugene P. Bertin ◽  
Rita J. Longobucco

AbstractVarious sample-mounting devices are described for use with a commercial flat-crystal X-ray fluorescence spectrometer having conventional (i.e., not inverted) geometry: (1) a sample drawer with two sample “spinners,” one for rotation of flat samples in their own plane, the other for rotation of cylindrical or filamentary samples about an axis normal to the plane defined by the directions of the primary and secondary X-ray beams; (2) rotatable mounting stages for filter paper disks and various very small samples; (3) a sample drawer for selected area operation with pinhole or slit apertures in the primary beam or pinhole apertures in the secondary beam; (4) a liquid cell with 0.00025-in. Mylar window (the cell is inexpensive, easily filled and rinsed, and usable 20-50 times before the window must be replaced); (5) three types of cell for powder samples (one has a 0.00025-in, Mylar window and is filled through a port in the top; the other types are open on both sides and are filled by placing them on glass plates and introducing the powder from the back; one of these back-loading cells permits rotation of the powder sample); (6) rotatable stages for briquetted powder samples; (7) mounting devices for wire samples on small spools (one of these devices permits rotation of the spool).These devices were designed and made at the X-ray laboratory of the RCA plant at Harrison, N. J., and have been used there successfully with a wide variety of samples for several years.


1995 ◽  
Vol 39 ◽  
pp. 87-94 ◽  
Author(s):  
Rainer Stabenow ◽  
Alfried Haase

Grazing incidence diffraction (GID) is a powerful tool for the structural characterization of thin films. Unlike traditional Bragg-Brentano geometry (divergent X-ray beam, focusing geometry), GID experiments are enhanced by a parallel beam of high intensity. Classical conditioning of the X-ray beam is done by using small slits on the primary beam side and a long Soller slit in combination with a flat crystal (e.g. graphite, lithium fluoride or germanium) or an energy dispersive detector on the secondary beam side. However, new alternatives for beam conditioners are becoming available which promise increased performance. X-ray beam optics using either planar or graded parabolically curved multilayer mirrors of high reflectivity have been constructed for the primary beam side as well as for the secondary beam side.


1961 ◽  
Vol 5 ◽  
pp. 516-526 ◽  
Author(s):  
Kurt F. J. Heinrich

AbstractAn attachment to a commercial flat-crystal X-ray fluorescent goniometer permits analysis of small areas. The selection of the sample area is achieved by collimating the secondary beam. The geometry of the probe, its stage, and counting statistics applied to the probe are discussed. Experimental data are shown referring to determination of spot size, counting rates obtained, and both qualitative and quantitative applications.


In a paper on “Polarised Röntgen Radiation,” the writer gave an account of experiments which demonstrated the partial polarisation of a beam of X-rays proceeding from the antikathode of an X-ray focus-tube, and verified the theory previously given of the production of secondary X-rays in light substances. In that paper it was shown that the secondary radiation proceeding in a direction perpendicular to that of propagation of the primary radiation from certain substances placed in that primary beam should, according to the theory put forward, be plane polarised. From gases, however, the secondary radiation was not sufficiently intense to produce a tertiary of measurable intensity, and thus the polarisation of the secondary from them was not verifiable. On the other hand, though heavy metals were found to emit secondary radiation of sufficient intensity and ionising power to produce appreciable tertiary effects, in these metals the production of secondary radiation is a more complex phenomenon, and evidence of polarisation of the secondary beam is not to be expected from experiments upon them.


1964 ◽  
Vol 36 (2) ◽  
pp. 441-443 ◽  
Author(s):  
E. P. Berlin
Keyword(s):  

1994 ◽  
Vol 144 ◽  
pp. 275-277
Author(s):  
M. Karlický ◽  
J. C. Hénoux

AbstractUsing a new ID hybrid model of the electron bombardment in flare loops, we study not only the evolution of densities, plasma velocities and temperatures in the loop, but also the temporal and spatial evolution of hard X-ray emission. In the present paper a continuous bombardment by electrons isotropically accelerated at the top of flare loop with a power-law injection distribution function is considered. The computations include the effects of the return-current that reduces significantly the depth of the chromospheric layer which is evaporated. The present modelling is made with superthermal electron parameters corresponding to the classical resistivity regime for an input energy flux of superthermal electrons of 109erg cm−2s−1. It was found that due to the electron bombardment the two chromospheric evaporation waves are generated at both feet of the loop and they propagate up to the top, where they collide and cause temporary density and hard X-ray enhancements.


1994 ◽  
Vol 144 ◽  
pp. 1-9
Author(s):  
A. H. Gabriel

The development of the physics of the solar atmosphere during the last 50 years has been greatly influenced by the increasing capability of observations made from space. Access to images and spectra of the hotter plasma in the UV, XUV and X-ray regions provided a major advance over the few coronal forbidden lines seen in the visible and enabled the cooler chromospheric and photospheric plasma to be seen in its proper perspective, as part of a total system. In this way space observations have stimulated new and important advances, not only in space but also in ground-based observations and theoretical modelling, so that today we find a well-balanced harmony between the three techniques.


1994 ◽  
Vol 144 ◽  
pp. 82
Author(s):  
E. Hildner

AbstractOver the last twenty years, orbiting coronagraphs have vastly increased the amount of observational material for the whitelight corona. Spanning almost two solar cycles, and augmented by ground-based K-coronameter, emission-line, and eclipse observations, these data allow us to assess,inter alia: the typical and atypical behavior of the corona; how the corona evolves on time scales from minutes to a decade; and (in some respects) the relation between photospheric, coronal, and interplanetary features. This talk will review recent results on these three topics. A remark or two will attempt to relate the whitelight corona between 1.5 and 6 R⊙to the corona seen at lower altitudes in soft X-rays (e.g., with Yohkoh). The whitelight emission depends only on integrated electron density independent of temperature, whereas the soft X-ray emission depends upon the integral of electron density squared times a temperature function. The properties of coronal mass ejections (CMEs) will be reviewed briefly and their relationships to other solar and interplanetary phenomena will be noted.


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