Multifunctional hybrid nanopapers based on bacterial cellulose and sol–gel synthesized titanium/vanadium oxide nanoparticles

Cellulose ◽  
2013 ◽  
Vol 20 (3) ◽  
pp. 1301-1311 ◽  
Author(s):  
Junkal Gutierrez ◽  
Susana C. M. Fernandes ◽  
Iñaki Mondragon ◽  
Agnieszka Tercjak
Keyword(s):  
Vanadium Oxide ◽  
Bacterial Cellulose ◽  
Sol Gel ◽  
Oxide Nanoparticles ◽  
Titanium Vanadium

STUDY OF THE ELECTRICAL PROPERTIES OF SOL-GEL-DERIVED TITANIUM-VANADIUM OXIDE FILMS

2002 ◽  
Vol 16 (28n29) ◽  
pp. 4465-4468 ◽  
Author(s):  
GAOLING ZHAO ◽  
GAORONG HAN
Keyword(s):  
Solid Solution ◽  
Electrical Properties ◽  
Vanadium Oxide ◽  
Hall Mobility ◽  
Sol Gel ◽  
Oxide Films ◽  
X Ray Diffraction ◽  
Type Semiconductor ◽  
Titanium Vanadium ◽  
Vanadium Oxide Films

Titanium-vanadium oxide films were prepared by the sol-gel method. The effects of vanadium incorporation on the crystallization behavior TiO 2 were investigated by X-ray diffraction analysis. The results showed that anatase and rutile type solid solution Ti 1-x V x O 2 films were obtained for x < 0.15 and x > 0.15 samples, respectively. Anatase and V 2 O 5 were found in x = 0.15 sample. Moreover, it was found that the crystallization of the film increased with increasing amount of vanadium. The electrical properties of Ti 1-x V x O 2 films were studied by measuring their resistance and Hall mobility. It was revealed that the resistivity of Ti 1-x V x O 2 films decreased with increasing x when the solid solution was formed, while the resistivity increased when the crystallization of vanadium oxide precipitated. The Hall constant was negative, indicating that Titanium-vanadium oxide is an n-type semiconductor. The evolution of the resistance and Hall mobility was ascribed to the 3d electrons of vanadium.

Green Synthesis of Cobalt Oxide Nanoparticles by a Starch-Assisted Method

2019 ◽  
Vol 9 (3) ◽  
pp. 362-370 ◽  
Author(s):  
D. Vaya ◽  
Meena ◽  
B.K. Das
Keyword(s):  
Photocatalytic Activity ◽  
Cobalt Oxide ◽  
Sol Gel ◽  
Complex Nature ◽  
Oxide Nanoparticles ◽  
Capping Agent ◽  
Chemical Route ◽  
Gel Method ◽  
Sol Gel Method ◽  
Cobalt Oxide Nanoparticles

Background: The properties of the material are altered when material size shifted towards nano-regime. This feature could be used for wastewater treatment process using model pollutant such as dyes. Recently, nanoparticles are synthesized by a green chemical route using different capping agents. This is the reason we adopt starch as green capping agent along with sol-gel method. Objective: To synthesize cobalt oxide nanoparticles by green chemical route and utilized it in degradation of dyes. Methods: Synthesis of cobalt oxide nanoparticles by sol-gel method using starch as a capping agent. The characteristics of surface modifications were investigated by UV-VIS, TEM, SEM, XRD and FTIR techniques. Results: Cobalt oxide nanoparticles synthesized and inhibited photocatalytic activity. Conclusion: Deactivation of photocatalytic activity due to complex nature of starch. This property can be used elsewhere as in light shielding applications to coat and protect surfaces in order to keep them cool and safe from damage as in the painting of vehicles, roofs, buildings, water tanks, etc.

scholarly journals Yttrium Oxide Nanoparticle Synthesis: An Overview of Methods of Preparation and Biomedical Applications

2021 ◽  
Vol 11 (5) ◽  
pp. 2172
Author(s):  
Govindasamy Rajakumar ◽  
Lebao Mao ◽  
Ting Bao ◽  
Wei Wen ◽  
Shengfu Wang ◽  
...  
Keyword(s):  
Yttrium Oxide ◽  
Metal Oxide Nanoparticles ◽  
Sol Gel ◽  
Antioxidant Properties ◽  
Nanoparticle Synthesis ◽  
Synthetic Methods ◽  
Host Material ◽  
Solid State Reactions ◽  
Oxide Nanoparticles ◽  
Advantages And Disadvantages

Metal oxide nanoparticles demonstrate uniqueness in various technical applications due to their suitable physiochemical properties. In particular, yttrium oxide (Y2O3) nanoparticle is familiar for technical applications because of its higher dielectric constant and thermal stability. It is widely used as a host material for a variety of rare-earth dopants, biological imaging, and photodynamic therapies. Y2O3 has also been used as a polarizer, phosphor, laser host material, and in the optoelectronic fields for cancer therapy, biosensor, and bioimaging. Yttrium oxide nanoparticles have attractive antibacterial and antioxidant properties. This review focuses on the promising applications of Y2O3, its drawbacks, and its modifications. The synthetic methods of nanoparticles, such as sol-gel, emulsion, chemical methods, solid-state reactions, combustion, colloid reaction techniques, and hydrothermal processing, are recapitulated. Herein, we also discuss the advantages and disadvantages of Y2O3 NPs based biosensors that function through various detection modes including colorimetric, electrochemistry, and chemo luminescent regarding the detection of small organic chemicals, metal ions, and biomarkers.

Bimetallic Antimony–Vanadium Oxide Nanoparticles Embedded in Graphene for Stable Lithium and Sodium Storage

2021 ◽  
Author(s):  
Yutong Hao ◽  
Ying Jiang ◽  
Luzi Zhao ◽  
Zhengqing Ye ◽  
Ziheng Wang ◽  
...  
Keyword(s):  
Vanadium Oxide ◽  
Oxide Nanoparticles ◽  
Sodium Storage

scholarly journals Wound Healing Composite Materials of Bacterial Cellulose and Zinc Oxide Nanoparticles with Immobilized Betulin Diphosphate

Nanomaterials ◽  
2021 ◽  
Vol 11 (3) ◽  
pp. 713
Author(s):  
Nina Melnikova ◽  
Alexander Knyazev ◽  
Viktor Nikolskiy ◽  
Peter Peretyagin ◽  
Kseniia Belyaeva ◽  
...  
Keyword(s):  
Wound Healing ◽  
Zinc Oxide ◽  
Bacterial Cellulose ◽  
Zinc Oxide Nanoparticles ◽  
Wound Dressings ◽  
Oxide Nanoparticles ◽  
Burn Wound ◽  
Zno Nps ◽  
Wound Model ◽  
And Oxidative Stress

A design of new nanocomposites of bacterial cellulose (BC) and betulin diphosphate (BDP) pre-impregnated into the surface of zinc oxide nanoparticles (ZnO NPs) for the production of wound dressings is proposed. The sizes of crystalline BC and ZnO NPs (5–25%) corresponded to 5–6 nm and 10–18 nm, respectively (powder X-ray diffractometry (PXRD), Fourier-infrared (FTIR), ultraviolet (UV), atomic absorption (AAS) and photoluminescence (PL) spectroscopies). The biological activity of the wound dressings “BC-ZnO NPs-BDP” was investigated in rats using a burn wound model. Morpho-histological studies have shown that more intensive healing was observed during treatment with hydrophilic nanocomposites than the oleophilic standard (ZnO NPs-BDP oleogel; p < 0.001). Treatment by both hydrophilic and lipophilic agents led to increases in antioxidant enzyme activity (superoxide dismutase (SOD), catalase) in erythrocytes and decreases in the malondialdehyde (MDA) concentration by 7, 10 and 21 days (p < 0.001). The microcirculation index was restored on the 3rd day after burn under treatment with BC-ZnO NPs-BDP wound dressings. The results of effective wound healing with BC-ZnO NPs-BDP nanocomposites can be explained by the synergistic effect of all nanocomposite components, which regulate oxygenation and microcirculation, reducing hypoxia and oxidative stress in a burn wound.

scholarly journals Properties and Biomedical Applications of Hydrothermal method Synthesized of Vanadium Oxide nanoparticles

2021 ◽  
Vol 1963 (1) ◽  
pp. 012043
Author(s):  
Saif Altimime ◽  
Sundus Q. Mohammed ◽  
Majid H. Hassoni ◽  
Ahmed N. Abd
Keyword(s):  
Vanadium Oxide ◽  
Hydrothermal Method ◽  
Biomedical Applications ◽  
Oxide Nanoparticles

Synthesis of Novel Vanadium Oxide Nanotubes and Nanofibers

2002 ◽  
Vol 740 ◽  
Author(s):  
Samuel T. Lutta ◽  
Hong Dong ◽  
Peter Y. Zavalij ◽  
M. Stanley Whittingham
Keyword(s):  
Thermal Analysis ◽  
Vanadium Oxide ◽  
Electrochemical Behavior ◽  
Redox Reactions ◽  
Sol Gel ◽  
Vanadium Oxides ◽  
Organic Polymer ◽  
Fibrous Morphology ◽  
Surfactant Templates ◽  
Vanadium Oxide Nanotubes

ABSTRACTWe are exploring the synthesis and properties of structured vanadium oxides mainly nanotubes and nanorods. Nanotubes initially formed with surfactant templates have been readily exchanged with simple cations without change of the basal-plane structure. These compounds contain d-like vanadium oxide layers with the vanadium in VO6 octahedra. This structure is particularly suitable for redox reactions. In this paper we report on synthesis of vanadium oxide, (NH4)xV2O5-d·nH2O rods using organic polymer as template. This compound has been synthesized by sol-gel reaction and subsequent hydrothermal treatment. TGA, SEM, XRD and FTIR were used to characterize this compound. Thermal analysis of this compound shows that the fibrous morphology is maintained when it is heated in nitrogen and oxygen above 300 °C. However, in both cases the size of the fibers decreases. Performance of this compound as cathode material in secondary electrolyte has been investigated using LiPF6 as electrolyte. A capacity of 140 mAh/g was obtained which remained fairly constant with up to at least 10 cycles. We also investigated electrochemical behavior of thermal products.

Structural, Magnetic and Dielectric Analysis of Higher Magnetic Mn Doped Zn-Cr Oxide Nanoparticles

2021 ◽  
Vol 9 (VI) ◽  
pp. 95-102
Author(s):  
S. D. Balsure
Keyword(s):  
Type Strain ◽  
Sol Gel ◽  
Hexagonal Wurtzite Structure ◽  
Xrd Analysis ◽  
Oxide Nanoparticles ◽  
X Ray Diffraction ◽  
Microstructural Parameters ◽  
Auto Combustion ◽  
Mn Doped ◽  
Combustion Technique

Higher magnetic Mn doped Zn-Cr oxide nanoparticles with general compositional formula MxZn0.95-xCr0.05O have been synthesized by using sol-gel auto combustion technique. Room temperature X-ray diffraction (XRD) technique has been employed to study the structural and microstructural parameters of the as-prepared samples. XRD analysis confirms the phase purity and hexagonal wurtzite structure of all the samples. Replacement of Zn2+ ions by Mn2+ ions shifts peak positions slightly towards the lower angles which in turn expands the lattice lengths ‘a’ from 3.2487 to 3.2528 Å and ‘c’ from 5.2043 to 5.2118 Å. Crystallite size obtained from Scherrer equation was confirmed by Williamson – Hall (W-H) and size – strain plot methods (SSP). Both W-H and SSP methods reveals the tensile type strain for undoped sample and comprehensive type strain for Mn2+ doped samples. Magnetic properties were investigated by using vibrating sample magnetometer. Diluted ferromagnetic behaviour is observed for all the samples and saturation magnetization (MS) increases from 0.0514 to 0.1163 emu/gm. Two-probe technique was employed to understand the dielectric behaviour of the samples as a function of frequency. At lower frequency region, both dielectric constant () and dielectric loss tangent (tan ) shows higher values and decreases with the increasing applied frequency.

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